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- 저자 : Pargat Singh (검색결과 2 건)
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J. S. Dureja,Ranjit Singh,Talwinder Singh,Pargat Singh,Manu Dogra,Manpreet S. Bhatti 한국정밀공학회 2015 International Journal of Precision Engineering and Vol.2 No.2
The benefits of cutting fluids in machining are well known, but their use is accompanied by health and environment hazards. Moreover, strict environmental regulations make the manufacturers to switch over to dry turning, which is not feasible during machining of sticky material like stainless steel and Inconel etc. Therefore, the use of minimal quantities of lubricant (MQL) can be regarded as an alternative solution and a step towards green machining. In the present investigation an attempt has been made to explore the potential of MQL turning of stainless steel with coated carbide cutting tool. Turning under MQL conditions has shown superior results (in terms of flank wear and machined surface roughness) over wet and dry turning. Signal to noise (S/N) ratio as per Taguchi design revealed speed and MQL as significant parameters for minimizing flank wear and surface roughness, whereas feed can be set within range. The optimum combination of parameters are cutting speed (58 m/min), feed rate (0.06 mm/rev.) and MQL flow rate (100 mL/h) for flank wear and cutting speed (23 m/min), feed rate (0.07 mm/rev.) and MQL flow rate (150 mL/h) for surface roughness. Taguchi optimized conditions were validated through multiple response optimization using desirability function.
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Mishra Neeraj Kumar,Rakshit Amitava,문경원,Singh Pargat,김인수 대한화학회 2024 Bulletin of the Korean Chemical Society Vol.45 No.2
The synthesis and functionalization of privileged nitrogen heterocycles has emerged as a central topic in drug discovery and material science. In this context, the tandem C–H functionalization and intramolecular annulation has received prodigious attention, as it is able to expedite the construction of heteroaromatic frameworks beyond conventional C–H functionalization. In general, significant effort has been made to develop the [3 + 2] dipolar cycloaddition of azomethine imines with π‐unsaturated compounds. Moreover, the [3 + 3], [4 + 3], [3 + 2 + 2], and [5 + 3] cycloaddition reactions of azomethine imines with various dipolarophiles have been demonstrated. To date, however, the combination of catalytic C–H functionalization and intramolecular cyclization using azomethine imines as both directing groups and dipolar units has been less explored. This review focuses on recent progress toward the catalytic tandem C–H functionalization and dipolar cycloaddition of azomethines imines with a range of coupling partners. The synthesis and functionalization of privileged nitrogen heterocycles has emerged as a central topic in drug discovery and material science. In this context, the tandem C–H functionalization and intramolecular annulation has received prodigious attention, as it is able to expedite the construction of heteroaromatic frameworks beyond conventional C–H functionalization. In general, significant effort has been made to develop the [3 + 2] dipolar cycloaddition of azomethine imines with π-unsaturated compounds. Moreover, the [3 + 3], [4 + 3], [3 + 2 + 2], and [5 + 3] cycloaddition reactions of azomethine imines with various dipolarophiles have been demonstrated. To date, however, the combination of catalytic C–H functionalization and intramolecular cyclization using azomethine imines as both directing groups and dipolar units has been less explored. This review focuses on recent progress toward the catalytic tandem C–H functionalization and dipolar cycloaddition of azomethines imines with a range of coupling partners.
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