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Kumar, Shiv,Khan, S.A.,Alam, Ozair,Azim, Rizwan,Khurana, Atul,Shaquiquzzaman, M.,Siddiqui, Nadeem,Ahsan, Waquar Korean Chemical Society 2011 Bulletin of the Korean Chemical Society Vol.32 No.7
4-Chlorotetrazolo[1,5-a]quinoxaline (III) was synthesized by azide (2+3) cycloaddition of 2,3-dichloroquinoxaline (II). Compound (III) on further refluxing with hydrazine hydrate furnished 4-hydrazinotetrazolo[1,5-a]quinoxaline (IV). Further refluxing of (IV) with different aromatic aldehydes in methanol yielded corresponding Schiff's bases V(a-j). Various 4-aminotetrazolo[1,5-a]quinoxaline based azetidinones VII(a-j) were synthesized by stirring the compounds V(a-j), at low temperature, with equimolar mixture of chloroacetylchloride & triethylamine in dry benzene, while 4-aminotetrazolo[1,5-a]quinoxaline based thiazolidinones VIII(a-j) were synthesized by refluxing Schiff's bases V(a-j) with thioglycolic acid in oil-bath. The structures of all the compounds were confirmed on the basis of $^1H$-NMR & FT-IR spectral data. All the newly synthesized compounds were screened for in-vitro antimicrobial activity against E. coli, S. aureus, K. pneumoniae & P. aeruginosa & antifungal activity against C. albicans. Few of them have exhibited the promising activity.
Shiv Kumar,S. A. Khan,Ozair Alam,Rizwan Azim,Atul Khurana,M. Shaquiquzzaman,Nadeem Siddiqui,Waquar Ahsan 대한화학회 2011 Bulletin of the Korean Chemical Society Vol.32 No.7
4-Chlorotetrazolo[1,5-a]quinoxaline (III) was synthesized by azide (2+3) cycloaddition of 2,3-dichloroquinoxaline (II). Compound (III) on further refluxing with hydrazine hydrate furnished 4-hydrazinotetrazolo[1,5-a]quinoxaline (IV). Further refluxing of (IV) with different aromatic aldehydes in methanol yielded corresponding Schiff’s bases V(a-j). Various 4-aminotetrazolo[1,5-a]quinoxaline based azetidinones VII(a-j) were synthesized by stirring the compounds V(a-j), at low temperature, with equimolar mixture of chloroacetylchloride & triethylamine in dry benzene, while 4-aminotetrazolo[1,5-a]quinoxaline based thiazolidinones VIII(a-j) were synthesized by refluxing Schiff’s bases V(a-j) with thioglycolic acid in oil-bath. The structures of all the compounds were confirmed on the basis of ^1H-NMR & FT-IR spectral data. All the newly synthesized compounds were screened for in-vitro antimicrobial activity against E. coli, S. aureus, K. pneumoniae & P. aeruginosa & antifungal activity against C. albicans. Few of them have exhibited the promising activity.
Reliability Assessment of HFRC Slabs Against Projectile Impact
Nadeem A. Siddiqui,Yousef A. Al?Salloum,Tarek H. Almusallam,Aref A. Abadel,Husain Abbas 한국콘크리트학회 2018 International Journal of Concrete Structures and M Vol.12 No.6
In the present study, a probabilistic procedure is presented for estimating the reliability of hybrid fiber reinforced concrete (HFRC) slabs against the impact of hemispherical nose projectiles considering uncertainties involved in the material, geometric and impact parameters. The influence of hybrid fibers in improving the safety level of reinforced concrete slabs against impact loads has also been studied on a parametric basis. The failure of the HFRC slabs was assumed to occur when the impact velocity of the projectile exceeds the ballistic limit of the slab i.e. perforates the slab. To illustrate the procedure, a probabilistic analysis was carried out on the impact test results of HFRC slabs containing different proportions of hooked-end steel, polypropylene and Kevlar fibers, recently published by the authors. Reliability assessment was performed for a range of applied nominal impact loads by varying the impact velocity of the given projectile. Reliability analysis yields the safety level of all the HFRC slabs against the impact of the above projectile. Effect of fibers, especially steel fibers, and slab thickness on the reliability of HFRC slabs are also investigated on a parametric basis.
Reliability assessment of RC shear wall-frame buildings subjected to seismic loading
Ahmet Tuken,Mohamed A. Dahesh,Nadeem A. Siddiqui 사단법인 한국계산역학회 2017 Computers and Concrete, An International Journal Vol.20 No.6
A considerable research is available on the seismic response of Reinforced Concrete (RC) shear wall-frame buildings, but the studies on the reliability of such buildings, with the consideration of human error, are limited. In the present study, a detailed procedure for reliability assessment of RC shear wall-frame building subjected to earthquake loading against serviceability limit state is presented. Monte Carlo simulation was used for the reliability assessment. The procedure was implemented on a 10-story RC building to demonstrate that the shear walls improve the reliability substantially. The annual and life-time failure probabilities of the studied building were estimated by employing the information of the annual probability of earthquake occurrence and the design life of the building. A simple risk-based cost assessment procedure that relates both the structural life-time failure probability and the target reliability with the total cost of the building was then presented. The structural failure probability (i.e., the probability of exceeding the allowable drift) considering human errors was also studied. It was observed that human error in the estimation of total load and/or concrete strength changes the reliability sharply.
SBC-based Assessment of Shear Wall Quantity in Moment Resisting Frame Buildings
Ahmet Tuken,Nadeem A. Siddiqui 대한토목학회 2015 KSCE JOURNAL OF CIVIL ENGINEERING Vol.19 No.1
According to Saudi Building Code (SBC) and almost all other seismic codes of the world, Reinforced Concrete (RC) shear wallmomentresisting frame buildings must satisfy the requirements of strength, stiffness and ductility if they have to be constructed inseismic prone areas. In the present study, a simple-to-apply analytical method based on “dual system” concept and SBC provisions isproposed to determine the amount of shear walls which can satisfy the strength, stiffness and ductility requirements imposed by theSBC on RC moment resisting frame buildings. The method also outlines a detailed procedure for the assessment of displacement andcurvature ductility of RC shear wall-moment resisting frame buildings. This formulation is based on plastic analysis and theassumption that the plastic hinge forms at the base of the shear wall. The proposed methodology was then applied to a 10-storey RCbuilding containing shear walls. It was shown that the amount of shear walls which is enough to satisfy the strength requirements alsofulfills the stiffness criteria (i.e., story drift limitation) required by the SBC. It was also proved that the ductility requirements imposedby the SBC can easily be satisfied by using the same quantity of shear walls.
Effect of rebar spacing on the behavior of concrete slabs under projectile impact
Husain Abbas,Nadeem A. Siddiqui,Tarek H. Almusallam,Aref A. Abadel,Hussein Elsanadedy,Yousef A. Al-Salloum 국제구조공학회 2021 Structural Engineering and Mechanics, An Int'l Jou Vol.77 No.3
In this paper, the effect of different steel bar configurations on the quasi-static punching and impact response of concrete slabs was studied. A total of forty RC square slab specimens were cast in two groups of concrete strengths of 40 and 63 MPa. In each group of twenty specimens, ten specimens were reinforced at the back face (singly reinforced), and the remaining specimens were reinforced on both faces of the slab (doubly reinforced). Two rebar spacing of 25 and 100 mm, with constant reinforcement ratio and effective depth, were used in both singly and doubly reinforced slab specimens. The specimens were tested against the normal impact of cylindrical projectiles of hemispherical nose shape. Slabs were also quasi-statically tested in punching using the same projectile, which was employed for the impact testing. The experimental response illustrates that 25 mm spaced rebars are effective in (i) decreasing the local damage and overall penetration depth, (ii) increasing the absorption of impact energy, and (iii) enhancing the ballistic limit of RC slabs. The ballistic limit was predicted using the quasi-static punching test results of slab specimens showing a strong correlation between the dynamic perforation energy and the energy required for quasi-static perforation of slabs.
Experimental Investigation on Vulnerability of Precast RC Beam-column Joints to Progressive Collapse
Tarek H. Almusallam,Hussein M. Elsanadedy,Yousef A. Al-Salloum,Nadeem A. Siddiqui,Rizwan A. Iqbal 대한토목학회 2018 KSCE JOURNAL OF CIVIL ENGINEERING Vol.22 No.10
The multi-story buildings are susceptible to progressive collapse in the event of the removal of one or more columns due to the exposure to blast loads. The lack of structural continuity in precast concrete buildings makes these buildings more vulnerable to progressive collapse as compared to the regular cast-in-situ concrete buildings. This study presents experiments involving two types of detailing of precast beam-column joints using half-scale test specimens when the middle column is suddenly removed. The test specimens represent the most prevalent precast beam-column joints. One conventional cast-in-situ test specimen, having continuous top and bottom beam rebars, was used for comparison. The progressive collapse scenario was simulated by removing the central column support and applying a sudden vertical load on this column at a rate of 100 mm/s until failure. Test results helped in developing better understanding about the progressive collapse potential in the existing precast buildings. This study highlights the need for the rehabilitation of beam-column connections in existing precast buildings and necessitates the need for innovative beamcolumn connections for improving the progressive collapse resistance.