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Ab Initio and Experimental Studies on Dibenzothiazyl-Disulfide
Jian, Fang-Fang,Zhang, Ke-Jie,Zhao, Pu-Su,Zheng, Jian Korean Chemical Society 2006 Bulletin of the Korean Chemical Society Vol.27 No.7
Ab initio calculations of the structure, atomic charges and natural bond orbital (NBO) have been performed at HF/6-311G** and B3LYP/6-311G** levels for the title compound of dibenzothiazyl-disulfide. The calculated results show that the two nitrogen atoms have the biggest negative charges and they are the potential sites to react with the metallic ions, which make the title compound become a di-dentate ligand. Vibrational frequencies of the title compound have been obtained and compared with the experimental value and the comparison indicates that B3LYP/6-311G** level is better than HF/6-311G** level to predict the vibrational frequencies for the system studied here. For the title compound, electronic absorption spectra calculated by time?ependent density functional theory (TD-DFT) are more accurate than Hartree-Focksingle-excitation CI (CI-Singles) method. NBO analyses show that the electronic transitions are mainly derived from the contribution of bands $\pi\rightarrow\pi^{*}$. Thermodynamic calculated results show that the formation of the title compound from 2-mercaptobenzothiazole is a spontaneous process at room temperature with the change of free Gibbs being negative value.
Jian, Fang-Fang,Zhao, Pu-Su,Wang, Huan-Xiang,Lu, Lu-De Korean Chemical Society 2004 Bulletin of the Korean Chemical Society Vol.25 No.5
The tetranuclear copper(II) cluster compound $[Cu_4OCl_6(C_{14}H_{12}N_2)_4]$ has been synthesized by hydrothermal reaction and studied by X-ray diffraction. The four copper(II) atoms locate four capsheaves of a tetrahedral skeletal structure and a oxygen atom as interstitial atom occupies the center position of the same tetrahedron, and each edge of the Cu-Cu tetrahedron is bridged by one ${\mu}_2$-Cl anion. The copper atom possesses slightly distorted trigonal bipyramidal geometry with three ${\mu}_2$-Cl atoms in equatorial position and the interstitial O atom and one N atom from 3-benzyl-benzimidazole ligand occupying axial position. The Cu-Cu distances are in the range of 3.0986-3.1162 ${\AA}$. The EPR spectrum suggested that the copper(II) ground state $d_{x2-y2}$ and the coordination geometry was trigonal bipyramidal.
Jiang Wan-Zhu,Yao Fang-Jie,Lu Li-Xin,Fang Ming,Wang Peng,Zhang You-Min,Meng Jing-Jing,Lu Jia,Ma Xiao-Xu,He Qi,Shao Kai-Sheng 한국미생물학회 2021 The journal of microbiology Vol.59 No.1
Gloeostereum incarnatum is an edible medicinal mushroom widely grown in China. Using the whole genome of G. incarnatum, simple sequence repeat (SSR) markers were developed and synthetic primers were designed to construct its first genetic linkage map. The 1,048.6 cm map is composed of 10 linkage groups and contains 183 SSR markers. In total, 112 genome assembly sequences were anchored, representing 16.43 Mb and covering 46.41% of the genome. Selfing populations were used for quantitative trait loci (QTL) targeting, and the composite interval mapping method was used to co-localize the mycelium growth rate (potato dextrose agar and sawdust), growth period, yield and fruiting body length, and width and thickness. The 14 QTLs of agronomic traits had LOD values of 3.20–6.51 and contribution rates of 2.22– 13.18%. No linkage relationship was found between the mycelium growth rate and the growth period, but a linkage relationship was observed among the length, width and thickness of the fruiting bodies. Using NCBI’s BLAST alignment, the genomic sequences corresponding to the QTL regions were compared, and a TPR-like protein candidate gene was selected. Using whole-genome data, 138 candidate genes were found in four sequence fragments of two SSR markers located in the same scaffold. The genetic map and QTLs established in this study will aid in developing selective markers for agronomic traits and identifying corresponding genes, thereby providing a scientific basis for the further gene mapping of quantitative traits and the marker-assisted selection of functional genes in G. incarnatum breeding programs.
Illumination Invariant Chinese Chessboard Reconstruction Based on Color Image
Jianjun Fang,N.Kondo,Jiying Yin,Xiuhong Liu,Kexian Xiao 제어로봇시스템학회 2009 제어로봇시스템학회 국제학술대회 논문집 Vol.2009 No.8
This paper introduces a new approach based on binarized Gabor filters and Hough transform to reconstruct Chinese chessboard by computation. Firstly, Gabor transform is performed directly on an original color image of chessboard to obtain Gabor filters in which only interested lines are kept by selecting appropriate parameters. Secondly, Gabor filters image is binarized and thinned and then lines are detected by Hough transform. Thirdly, a binarized Gabor filters’image is affine rectified and three parameters which dominate reconstruction of chessboard are measured and coordinates of any crossing points in the chessboard can be calculated based on priori information and measured data. Finally, experiments have been conducted to verify illumination invariant feature of proposed approach. Results reveal that this new approach is more robust to illumination change. Comparing to conventional method, it is obviously superior and has been applied in a robust machine vision system for Chinese chess playing robot.
Laguerre characterization of some hypersurfaces
Jianbo Fang,Fengjiang Li 대한수학회 2016 대한수학회보 Vol.53 No.3
Let $x$ : ${M}^{n-1}\rightarrow{\mathbb R}^{n}$ $(n\geq4)$ be an umbilical free hypersurface with non-zero principal curvatures. Then $x$ is associated with a Laguerre metric $\mathbf{g}$, a Laguerre tensor $\mathbf{L}$, a Laguerre form $\mathbf{C}$, and a Laguerre second fundamental form $\mathbf{B}$, which are invariants of $x$ under Laguerre transformation group. We denote the Laguerre scalar curvature by $R$ and the trace-free Laguerre tensor by $\tilde{\mathbf{L}}:={\mathbf{L}}-\frac{1}{n-1}tr({\mathbf{L}})\mathbf{g}$. In this paper, we prove a local classification result under the assumption of parallel Laguerre form and an inequality of the type $$\|\tilde{\mathbf{L}}\|\leq cR,$$ where $c=\frac{1}{(n-3)\sqrt{(n-2)(n-1)}}$ is appropriate real constant, depending on the dimension.
Life history responses of the cabbage beetle Colaphellus bowringi to temperature change
Jian‐Jun Tang,Hai-Min HE,Ting GENG,Shu FU,Fang-Sen XUE 한국곤충학회 2016 Entomological Research Vol.46 No.6
Temperature is considered one of the most important mediators of phenotypic plasticity in ectotherms. Here, we investigated life history traits of the cabbage beetle, Colaphellus bowringi Baly (Coleoptera: Chrysomelidae), at a wide range of temperatures (16, 19, 22, 24, 26 and 28°C). The larval and pupal times were significantly decreased with increasing rearing temperature and growth rate was positively correlated with temperature. However, the relationship between body size and rearing temperature in C. bowringi did not follow the temperature–size rule; both males and females reached the highest body weight at 19°C. Females were significantly larger than males at all temperatures. Male pupae lost significantly more weight at metamorphosis compared to females. However, diapausing males gained significantly higher weight after feeding compared to diapausing females at higher temperatures of 22, 24, 26 and 28°C. Body weight tended to decrease with increasing rearing temperature, whereas sexual size dimorphism (SSD) tended to increase with increasing rearing temperature; thus, Rensch's rule is upheld. The degree to which SSD changed with temperature varied with different development stages. SSD was lowest in pupae, highest in newly emerged adults and intermediate in diapausing adults.
( Jian Rong Xue ),( Hong Zhong ),( Shuai Wang ),( Chang Xin Li ),( Jin Zhong Li ),( Fang Fang Wu ) 한국화학공학회 2015 Korean Chemical Engineering Research(HWAHAK KONGHA Vol.53 No.4
We investigated the reduction leaching process of manganese dioxide ore using black locust as reductant in sulfuric acid solution. The effect of parameters on the leaching efficiency of manganese was the primary focus. Experimental results indicate that manganese leaching efficiency of 97.57% was achieved under the optimal conditions: weight ratio of black locust to manganese dioxide ore (WT) of 4:10, ore particle size of 63 μm, 1.7 mol·L-1 H2SO4, liquid to solid ratio (L/S) of 5:1, leaching time of 8 h, leaching temperature of 368 K and agitation rate of 400 r·min-1. The leaching rate of manganese, based on the shrinking core model, was found to be controlled by inner diffusion through the ash/inert layer composed of associated minerals. The activation energy of reductive leaching is 17.81 kJ·mol-1. To conclude the reaction mechanism, XRD analysis of leached ore residue indicates manganese compounds disappear; FTIR characterization of leached residue of black locust sawdust shows hemicellulose and cellulose disappear after the leaching process.
Jianguang Yue,Hua Fang,Yuefei Xia,Hongquan Wang,Kai Wu 한국강구조학회 2020 International Journal of Steel Structures Vol.20 No.6
The damage evolutions of square concrete-fi lled steel tubular (CFT) columns were experimentally studied by the axial compression cyclic loading test and the acoustic emission (AE) monitoring technique. Based on the mechanical analysis and damage observations, the limit damage states, i.e. inner concrete cracking, confi nement of steel tube, yielding and buckling of steel tube, weld seam splitting and inner concrete spalling were verifi ed. The released strain energy due to the damage of CFT column was monitored by the AE technique and analyzed by the peak frequency classifi cation method. The results show that the buckling of steel tube is the damage state with the maximum load carrying capacity for CFT columns. Most of the released strain energy were detected by the AE signals with the peak frequency between 30 and 75 kHZ and most of the strain energy were released after the buckling of the steel tube.