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Preparation and characterization of epoxidized microbial oil
Xinde Chen,Dan Yang,Lian Xiong,Bo Wang,Xuefang Chen,Can Wang,Hairong Zhang,Haijun Guo 한국화학공학회 2016 Korean Journal of Chemical Engineering Vol.33 No.3
The potential of microbial oil derived from yeasts through fermentation using crops biomass for the formation of plasticizers was investigated. Plasticizers were formed via epoxidation reaction. Five factors of the orthogonal experiment (reaction temperature, time, weight ratio of H2O2/MO, H2SO4/MO, and HCOOH/MO) have been used for optimization of parameters. To further enhance the iodine value of microbial oil and increase the epoxy value of the epoxide, an amount of soybean oil was added. The products were characterized by FTIR, 13C-NMR and 1H-NMR. Under the optimum condition, the epoxy value and the iodine value of epoxide product were 6.21% and 1.8 g I2/100 g with a yield of 91.86% at an oil conversion of 98.43%. This study successfully demonstrated the conversion of crops biomass into value-added chemicals using simple and conventional chemical reactions.
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Yinyin Chen,Xinde Zheng,Hang Jin,Shengming Deng,Daoyuan Ren,Andreas Greiser,Caixia Fu,Hongxiang Gao,Mengsu Zeng 대한영상의학회 2019 Korean Journal of Radiology Vol.20 No.1
Objective: The purpose of this study was to prospectively investigate the value of the myocardial extracellular volume fraction (ECV) in predicting myocardial functional outcome after revascularization of coronary chronic total occlusion (CTO). Materials and Methods: Thirty patients with CTO underwent cardiovascular magnetic resonance (CMR) before and 6 months after revascularization. Three baseline markers of functional outcome were evaluated in the dysfunctional segments assigned to the CTO vessels: ECV, transmural extent of infarction (TEI), and unenhanced rim thickness (RIM). At the global level, the ECV values of the whole myocardium with and without a hyperenhanced region (global and remote ECV) were respectively measured. Results: In per-segment analysis, ECV was superior to TEI and RIM in predicting functional recovery (area under receiver operating characteristic curve [AUC]: 0.86 vs. 0.75 and 0.73, all p values < 0.010), and it emerged as the only independent predictor of regional functional outcome (odds ratio [OR] = 0.83, 95% confidence interval [CI]: 0.77–0.89; p < 0.001) independent of collateral circulation. In per-patient analysis, global baseline ECV was indicative of ejection fraction (EF) at the follow-up examination (β = -0.61, p < 0.001) and changes in EF (β = -0.57, p = 0.001) in multivariate regression analysis. A patient with global baseline ECV less than 30.0% (AUC, 0.93; sensitivity 94%, specificity 80%) was more likely to demonstrate significant EF improvement (OR: 0.38; 95% CI: 0.17–0.85; p = 0.019). Conclusion: Extracellular volume fraction obtained by CMR may provide incremental value for the prediction of functional recovery both at the segmental and global levels in CTO patients, and may facilitate the identification of patients who can benefit from revascularization.
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Mouse Fyn induces pseudopodium formation in Chinese hamster ovary cells
Lei An,Shengnan Liu,Wei Zhang,Yamei Zhang,Yingxue Huang,Xinde Hu,Shu-lin Chen,Shanting Zhao 대한수의학회 2014 Journal of Veterinary Science Vol.15 No.1
Molecular mechanisms underlying the effects of Fyn on cellmorphology, pseudopodium movement, and cell migrationwere investigated. The Fyn gene was subcloned into pEGFP-N1to produce pEGFP-N1-Fyn. Chinese hamster ovary (CHO)cells were transfected with pEGFP-N1-Fyn. The expression ofFyn mRNA and proteins was monitored by reversetranscription-PCR and Western blotting. Additionally,transfected cells were stained with 4´,6-diamidino-2-phenylindole and a series of time-lapse images was taken. Sequences of the recombinant plasmids pMD18-T-Fyn andpEGFP-N1-Fyn were confirmed by sequence identificationusing National Center for Biotechnology Information in USA,and Fyn expression was detected by RT-PCR and Westernblotting. The morphology of CHO cells transfected with therecombinant vector was significantly altered. Fyn expressioninduced filopodia and lamellipodia formation. Based on theseresults, we concluded that overexpression of mouse Fyn inducesthe formation of filopodia and lamellipodia in CHO cells, andpromotes cell movement.
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Current progress on gold recovery from refractory ore and waste electrical and electronic equipment
Ji Xuran,Shen Zhijie,Xu Wenping,Yao Shimiao,Zhang Hairong,Xiong Lian,Li Hailong,Guo Haijun,Chen Xuefang,Chen Xinde 한국화학공학회 2023 Korean Journal of Chemical Engineering Vol.40 No.9
The physical and chemical properties of gold promote its application, such as in the high-tech, electronic products, and aerospace industries. The easily leachable ore is gradually depleted. Thus, it becomes necessary to extract gold from other resources such as refractory ore and electrical and electronic equipment. The normal method of leaching for gold is cyanide leaching, but it is very dangerous for both environment and operator. Non-cyanide leaching methods, including thiourea leaching, halide leaching, and sulfate leaching have been developed to substitute cyanide leaching. A variety of methods to enrich gold from leaching solutions are described in this paper, including solvent extraction, electrowinning, activated carbon adsorption, and ion exchange resins. Among those methods, ion exchange resins can adsorb gold with high adsorption efficiency and regenerate easily as well. This paper focuses on the research progress of the recovery of gold from non-cyanide leachates by ion exchange resins, summarizes the existing resin types and elution processes, points out the limitations in the application of current ion exchange resins, and discusses possible solutions.
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Piperazine-activated diethanolamine formulation for post-combustion CO2 capture
Bisweswar Das,Haijun Guo,Lian Xiong,Bishnupada Mandal,Arindam Modak,Kamal Kishore Pant,Xinde Chen 한국공업화학회 2023 Journal of Industrial and Engineering Chemistry Vol.118 No.-
Although activated alkanolamine based solvents had great potential for energy-efficient post-combustionCO2 capture, yet these suffers from disadvantageous due to high capital cost of the process. In thisresearch we developed and discussed the overall reaction scheme between CO2 and activated solvents. We investigated the kinetics of CO2 into piperazine (PZ) activated aqueous diethanolamine (DEA) bywetted-wall column contactor at (298–323) K, (5–15) kPa and fixed 3.0 kmol∙m3. Physicochemical propertiesof such systems were determined while detailed uncertainty analysis were conducted. In thermodynamicspoint of view, liquid–liquid interaction were explored and evaluated by related parameters. The kinetics rate parameters for such activated solvents were interpreted based on kinetic study affordingto the pseudo-first-order reaction method. At various temperature, kov of (PZ + DEA + H2O) were considerablylarger than reported (AMP + PZ + H2O) systems. The results of kinetics study demonstrated thatrate of CO2 in solvents were enhanced substantially as compared to DEA due to the addition of low quantity(0–0.45 kmol∙m3) PZ into solvents. Besides, physicochemical properties were measured in terms ofdifferent models with absolute average deviation (AAD) < 5 %. Ultimately, (PZ + DEA + H2O) may be consideredas vital solvents in amine scrubbing due to lower energy requirement for CO2 capture comparedto (PZ + MEA + H2O).
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