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Jinshan Hu,Pengfei Zhang,Jifang Cui,Weijia An,Li Liu,Yinghua Liang,Qingbin Yang,Hongjun Yang,Wenquan Cui 한국공업화학회 2020 Journal of Industrial and Engineering Chemistry Vol.84 No.-
To achieve rapid separation of electron-hole pairs and improve photocatalytic degradation activity, theFe-g-C3N4 reduced graphene hydrogel (rGH/Fe-g-C3N4) with a 3D network structure was fabricated viathe hydrothermal method. Using visible light irradiation, H2O2 was added to form a photocatalysis-Fenton synergy system. The results showed that the synergistic degradation rate constant of 10% rGH/Feg-C3N4 was 52% higher than that of the multiphase Fenton reaction and 1.5 times higher than that of theFe-g-C3N4. In the seventh cycle, the catalytic efficiency was still as high as 86.9%. Based on the optimizedconditions from phenol degradation, the system was further applied to coking wastewater treatment,and the degradation efficiency of TOC and COD in 60 min reached 66.3% and 68.1%, respectively. Such highand stable degradation performance was ascribed to the synergy effect of photocatalysis and Fenton. Because of the photogenerated electrons not only can promote the Fe3+/Fe2+ cycle, accelerate thedecomposition of H2O2, but also can quickly transfer to graphene and directly decompose H2O2 to formOH. Thus, a large amount ofOH were generated through the two different channels, which greatlyimprove the degradation efficiency. Furthermore, rGH/Fe-g-C3N4 can be regenerated usingfilters withoutthe need for additional complicated processing. This work provides an effective strategy for the deeptreatment of industrial wastewater.
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원예연,백명현,최문권,전경진,김만경,Won Ye-Yeon,Baek Myong-Hyun,Cui WenQuan,Chun KeyoungJin,Kim Man Kyung 대한의용생체공학회 2004 의공학회지 Vol.25 No.6
골다공증이 있는 대퇴골두 해면골과 골다공증이 없는 대퇴골두 해면골의 특성을 평가하고자 미세단층촬영기 및 유한요소모델을 이용하여 해면골을 미세구조 특성과 기계적 특성을 비교 및 분석하였다. 골다공증이 있는 대퇴골두는 골밀도를 측정하여 T-score 값이 -2.5 이상인 시편 15개를 사용했으며, 골다공증이 없는 대퇴골두는 사망전 골다공증으로 인한 병력이 없었던 사체 4구에서 대퇴골두 5개를 획득하여 사용하였다. 대퇴골두 해면골의 미세구조 특성을 분석하기 위해서 미세단층촬영기를 이용하여 골다공증이 있는 대퇴골두와 골다공증이 없는 대퇴골두를 촬영하여 형태학적 지수(histomorphometry index)를 구했고, 미세단층촬영기에 의해서 획득된 미세영상(pixel size=21.31㎛)을 바탕으로 유한요소모델을 재건하여 기계적 특성을 구하였다. 형태학적지수는 골다공증이 없는 대퇴골두가 골다공증이 있는 대퇴골두에 비해서 골소주 두께, 골 체적, 골 체적비, 이방성 정도 그리고 골소주 개수가 증가했으며, 골소주 간격과 구조모델지수는 감소했다. 기계적특성 지수는 골다공증이 없는 대퇴골두 해면골 시편에서 반력, 표면응력 그리고 영률이 높게 분석되었다. 골다공증이 있는 대퇴골두 해면골 시편에서 미세구조 특성이 퇴화되며, 기계적 특성이 감소된다는 사실을 알수 있었다. This study investigates micro-structural and mechanical properties of trabecular bone in human femoral head with and without osteoporosis using Micro-CT and finite element-model. 15 cored trabecular bone specimens with 20min of diameter were obtained from femoral heads with osteoporosis (T-score > -2.5 ) resected for total hip arthroplasty, and 5 specimens were removed from femoral head of cadavers, which has no history of musculoskeletal diseases. A high-resolution micro-CT system was used to scan each specimen to obtain histomorphometry indices. Based on obtained micro-images(pixel size=21.31㎛), a FE-model was created to determine mechanical property indices. While non-osteoporosis group had increases trabecular thickness, bone volume, bone volume fraction, degree of anisotropy and trabecular number compared with those of non-osteoporotic group, the non-osteoporotic group showed decreases in trabecular separation and structure model index. Regarding the mechanical property indices, reaction force, apparent stress and young's modulus were 1ower in osteoporotic group than in non-osteoporotic group. Our data shows salient deteriorations in trabecular micro-structural and mechanical properties in human femoral head with osteoporosis.
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Synthesis of Cd1-xZnxS/K4Nb6O17 Composite and its Photocatalytic Activity for Hydrogen Production
Yinghua Liang,Meiyi Shao,Li Liu,Jinshan Hu,Wenquan Cui 대한화학회 2014 Bulletin of the Korean Chemical Society Vol.35 No.4
Cd1-xZnxS-sensitized K4Nb6O17 composite photocatalysts (designated Cd1-xZnxS/K4Nb6O17) were prepared via a simple deposition-precipitation method. The samples were characterized by X-ray diffraction (XRD), scanning electron microscopy (SEM), transmission electron microscopy (TEM), energy dispersive X-ray spectrometry (EDS), N2 sorption, ultraviolet–visible light diffuse reflectance spectroscopy (UV–Vis DRS), photoluminescence measurements (PL), and X-ray photoelectron spectroscopy (XPS). The Cd0.8Zn0.2S particles were scattered on the surface of K4Nb6O17, and had a relatively uniform size distribution around 50 nm. The absorption edge of K4Nb6O17 was shifted to the visible light region and the recombination of photo-generated electrons and holes suppressed after Cd0.8Zn0.2S loading. The Cd0.8Zn0.2S(25 wt %)/K4Nb6O17 composite possessed the highest photocatalytic activity for hydrogen production under visible light irradiation, evolving 8.278 mmol/g in 3 h. Recyclability tests were performed, and the composite photocatalysts were found to be fairly stable. The mechanism of charge separation between the photogenerated electrons and holes at the Cd0.8Zn0.2S/K4Nb6O17 composite was discussed.
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Liang, Yinghua,Shao, Meiyi,Liu, Li,Hu, Jinshan,Cui, Wenquan Korean Chemical Society 2014 Bulletin of the Korean Chemical Society Vol.35 No.4
$Cd_{1-x}Zn_xS$-sensitized $K_4Nb_6O_{17}$ composite photocatalysts (designated $Cd_{1-x}Zn_xS/K_4Nb_6O_{17}$) were prepared via a simple deposition-precipitation method. The samples were characterized by X-ray diffraction (XRD), scanning electron microscopy (SEM), transmission electron microscopy (TEM), energy dispersive X-ray spectrometry (EDS), $N_2$ sorption, ultraviolet-visible light diffuse reflectance spectroscopy (UV-Vis DRS), photoluminescence measurements (PL), and X-ray photoelectron spectroscopy (XPS). The $Cd_{0.8}Zn_{0.2}S$ particles were scattered on the surface of $K_4Nb_6O_{17}$, and had a relatively uniform size distribution around 50 nm. The absorption edge of $K_4Nb_6O_{17}$ was shifted to the visible light region and the recombination of photo-generated electrons and holes suppressed after $Cd_{0.8}Zn_{0.2}S$ loading. The $Cd_{0.8}Zn_{0.2}S$(25 wt %)/$K_4Nb_6O_{17}$ composite possessed the highest photocatalytic activity for hydrogen production under visible light irradiation, evolving 8.278 mmol/g in 3 h. Recyclability tests were performed, and the composite photocatalysts were found to be fairly stable. The mechanism of charge separation between the photogenerated electrons and holes at the $Cd_{0.8}Zn_{0.2}S/K_4Nb_6O_{17}$ composite was discussed.
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