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Manna Ashis K.,Joshi Shalik R.,Satpati B.,Dash P.,Chattaraj Ananya,Srivastava S.K.,Kanjilal A.,Kanjilal D.,Varma Shikha 한국물리학회 2022 Current Applied Physics Vol.43 No.-
The present study explores the role of Ti ion implantation in structural phase transition in TiO2 thin films. Raman and TEM results reveal that after implantation Rutile phase in films increases at the expense of Anatase nanostructures. Though the as-deposited films display the presence of bigger anatase nanoparticles, after implantation, predominantly phonon confined smaller (~ 8 nm in size) anatase nanostructures are observed. GIXRD and Raman results further reflect presence of a critical fluence, 1 × 1013 ions/cm2, where the initial transformation from anatase to Rutile phase is observed. The role of Oxygen vacancies, in this transformation, has been explored here by XPS. Modifications in UV–Vis and Bandgap results show rich behavior which also reflects phase transformation at the critical fluence. Results further indicate that the phase transition gets first initiated deeper in the film and later on the surface. Interestingly, aggregation of larger Anatase nano-particles appears to be responsible for the structural transformation as observed here.
Subhankar Manna,Raj Kumar,Santosh K. Satpati,Saswati B. Roy,Jyeshtharaj B. Joshi 한국원자력학회 2017 Nuclear Engineering and Technology Vol.49 No.3
Uranium metal used for fabrication of fuel for research reactors in India is generally produced by magnesio-thermic reduction of UF4. Performance of magnesio-thermic reaction and recovery and quality of uranium largely depends on properties of UF4. As ammonium diuranate (ADU) is first product in powder form in the process flow-sheet, properties of UF4 depend on properties of ADU. ADU is generally produced from uranyl nitrate solution (UNS) for natural uranium metal production and from uranyl fluoride solution (UFS) for low enriched uranium metal production. In present paper, ADU has been produced via both the routes. Variation of uranium recovery and crystal structure and composition of ADU with progress in precipitation reaction has been studied with special attention on first appearance of the precipitate Further, ADU produced by two routes have been calcined to UO3, then reduced to UO2 and hydroflorinated to UF4. Effect of two different process routes of ADU precipitation on the characteristics of ADU, UO3, UO2 and UF4 were studied here.
Large Spin Diffusion Length in an Amorphous Organic Semiconductor
Shim, J. H.,Raman, K. V.,Park, Y. J.,Santos, T. S.,Miao, G. X.,Satpati, B.,Moodera, J. S. American Physical Society 2008 Physical Review Letters Vol.100 No.22
<P>We directly measured a spin diffusion length (lambdas) of 13.3 nm in amorphous organic semiconductor (OS) rubrene (C42H28) by spin polarized tunneling. In comparison, no spin-conserved transport has been reported in amorphous Si or Ge. Absence of dangling bond defects can explain the spin transport behavior in amorphous OS. Furthermore, when rubrene barriers were grown on a seed layer, the elastic tunneling characteristics were greatly enhanced. Based on our findings, lambdas in single-crystalline rubrene can be expected to reach even millimeters, showing the potential for organic spintronics development.</P>