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Karami, Bahador,Khodabakhshi, Saeed,Safikhani, Niloofar,Arami, Afsaneh Korean Chemical Society 2012 Bulletin of the Korean Chemical Society Vol.33 No.1
A facile and simple procedure for the synthesis of novel and known calix[4]resorcinarene derivatives were developed via a reaction of arylaldehydes with resorcinol in the presence of catalytic amounts of tungstate sulfuric acid (TSA) under solvent-free conditions. This eco-friendly method has many appealing attributes, such as excellent yields, short reactions times, use of safe and recoverable catalyst, and simple work-up procedures. TSA was characterized by powdered X-ray diffraction (XRD), X-ray fluorescence (XRF) and FTIR spectroscopy.
Bahador Karami,Saeed Khodabakhshi,Niloofar Safikhani,Afsaneh Arami 대한화학회 2012 Bulletin of the Korean Chemical Society Vol.33 No.1
A facile and simple procedure for the synthesis of novel and known calix[4]resorcinarene derivatives were developed via a reaction of arylaldehydes with resorcinol in the presence of catalytic amounts of tungstate sulfuric acid (TSA) under solvent-free conditions. This eco-friendly method has many appealing attributes,such as excellent yields, short reactions times, use of safe and recoverable catalyst, and simple work-up procedures. TSA was characterized by powdered X-ray diffraction (XRD), X-ray fluorescence (XRF) and FTIR spectroscopy.
Failure analysis of a heat-resistant stainless steel ring in a gas turbine burner
Aliakbar Fallah Sheykhlari,Saeed Khani Moghanaki,Meisam Khodabakhshi 대한기계학회 2020 JOURNAL OF MECHANICAL SCIENCE AND TECHNOLOGY Vol.34 No.4
Hot gas path components in gas turbines are damaged by several mechanisms due to aggressive environments. In this research, the cracking of an insert ring, which is composed of Nb-stabilized heat-resistant stainless steel, after 8000 operation hours, is investigated. The microstructure of the ring is examined by optical and scanning electron microscopes equipped with energy-dispersive X-ray spectroscopy. The generated stress and strain within the ring during a complete operation cycle (startup to shutdown) of gas turbine are simulated by finite element simulation software. The microstructural investigations indicate the formation of some precipitates that mainly contain nitrogen atoms. The development of tensile loads within the ring during shutdown and brittle N-contained precipitates leads to cracking. The indicators of both types of hot corrosion are also observed.
Bahador Karami,Sedigheh Akrami,Saeed Khodabakhshi 대한화학회 2013 Bulletin of the Korean Chemical Society Vol.34 No.12
Novel tri- and tetra-substituted pyrimido[4,5-d]pyridazines-2(1H,3H,7H)-ones have been synthesized via the regiospecific condensation reaction of hydrazine derivatives with 5-acetyl-4-aryloyl-6-methyl-3,4-dihydropyrimidinones in the presence of SiO2-Y(NO3)3 as a green and recyclable catalyst under solvent-free conditions. All products were obtained in high yields and short reaction time. Employing this method is in accord with green chemistry principles.
Karami, Bahador,Akrami, Sedigheh,Khodabakhshi, Saeed Korean Chemical Society 2013 Bulletin of the Korean Chemical Society Vol.34 No.12
Novel tri- and tetra-substituted pyrimido[4,5-d]pyridazines-2(1H,3H,7H)-ones have been synthesized via the regiospecific condensation reaction of hydrazine derivatives with 5-acetyl-4-aryloyl-6-methyl-3,4-dihydropyrimidinones in the presence of $SiO_2-Y(NO_3)_3$ as a green and recyclable catalyst under solvent-free conditions. All products were obtained in high yields and short reaction time. Employing this method is in accord with green chemistry principles.