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Kiyoumars Labani Motlagh,Javad Seyfi,Hossein Ali Khonakdar,Saeed Mortazavi 한국고분자학회 2022 Macromolecular Research Vol.30 No.5
Vinyl ester (VE) based nanocomposite coatings, loaded with an optimum content of silica aerogels, were fabricated on aluminum. Different graphene contents (1, 2, and 3% w/w) were applied via one-step and two-step spraying methods. Surface properties exhibited pronounced changes for the two-step coatings but remained nearly unchanged for the one-step coatings. Graphene was localized in the bulk of one-step coatings whereas the two-step method led to the aggregation of graphene nanoplatelets on the coating surface. Depending on the graphene content, small stacks (2 μm) to large agglomerations (20 μm) were detected on the surface of two-step coatings. The water contact angle was essentially increased from 61° for the pure VE coating to 96° and 115° upon the incorporation of silica aerogel and induction of an individual graphene layer, respectively. Such enhanced hydrophobicity was the major reason for the improved corrosion protection properties as found by Tafel polarization plots. The maximum protection efficiency was obtained for the two-step coating loaded by 2% graphene (η=99.5%). In conclusion, vinyl ester resin was found to be a great candidate for applications where high-performance coatings with improved corrosion resistance are needed. Moreover, the use of graphene, as an individual layer on the coating surface, and the utilization of silica aerogel, as a corrosion protective additive, were demonstrated to be a promising approach in real-life corrosion protection applications.
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New PLA/PEI-functionalized Fe3O4 nanocomposite: Preparation and characterization
Meisam Shabanian,Mehdi Khoobi,Farideh Hemati,Hossein Ali Khonakdar,Seyed esmaeil Sadat ebrahimi,Udo Wagenknecht,Abbas Shafiee 한국공업화학회 2015 Journal of Industrial and Engineering Chemistry Vol.24 No.-
In this work, Fe3O4 nanoparticles were functionalized with hyperbranched polyethylenimine (PEI). The neat Fe3O4 nanoparticles (MNP) and functionalized Fe3O4 (MNP@PEI) were separately incorporated into a polylactic acid (PLA). Compared to the neat MNP, the functionalized nanoparticles (MNP@PEI) had better dispersion in the PLA matrix. The properties of the nanocomposites were strongly related to the dispersion and interaction between the nanoparticles and PLA matrix. The heat barrier effect and high nitrogen content of the MNP@PEI nanoparticles were found to be responsible for the improvement of the thermal and flame resistance properties.
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Mahdi Ghelichi,Nader Taheri Qazvini,Seyed Hassan Jafari,Hossein Ali Khonakdar 한국고분자학회 2013 Macromolecular Research Vol.21 No.4
The influence for the minor amount of sodium montmorillonite (Na+-MMT) nanoclay on the thermorheological complexity of a miscible blend of 20 wt% poly(ethylene oxide) (PEO) in poly(methyl methacrylate)(PMMA) is studied. The dispersion of Na+-MMT in the PEO/PMMA is assessed via X-ray diffraction. The empirical principle of time-temperature superposition is found to be partially restored in the case of blend nanocomposite,whereas it fails for the neat PEO/PMMA blend. The relaxation times of each component are determined from the oscillatory shear rheometry data in the form of a monomeric friction coefficient. The chain dynamics of components is coupled in the presence of hydrophilic nanoclay, which preferentially adsorbs PEO. The self-concentration model of Lodge and McLeish successfully describes the temperature dependence of the PMMA monomeric friction coefficient in both the neat and blend nanocomposite in regards to the temperature range studied.
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