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Binh Hai Nguyen,Binh Thanh Nguyen,Hanh Van Vu,Chuc Van Nguyen,Dzung Tuan Nguyen,Loc Thai Nguyen,Thu Thi Vu,Lam Dai Tran 한국물리학회 2016 Current Applied Physics Vol.16 No.2
In this work, a lactose biosensor was developed by co-immobilizing b-galactosidase (b-Gal) and glucose oxidase (GOx) on microelectrodes pre-modified with Pt/graphene/P(1,5-DAN) for estimation of lactose in dairy products to prevent lactose intolerance. The Pt microelectrode was modified with graphene and 1,5-polydiaminonaphthalene film. Graphene was synthesized by chemical vapor deposition on copper tape and manually transferred to the electrode surface. Polymeric P(1,5-DAN) was grafted on top of the graphene film by electropolymerization. Modified surface of the electrode was characterized by Raman spectra analysis, FE-SEM, AFM and cyclic voltammetry. The results indicated that deposition graphene film on electrode surface induced considerable enhancement in current signal, over 20 times as high as the uncoated electrode surface. The developed sensor was successfully used to determine lactose in model samples with sensitivity, correlation coefficient (R2) and limit of detection (LOD) estimated to be 1.33 mA/(mgml1), 0.995 and 1.3 mg/ml, respectively. The combined graphene and conductive P(1,5-DAN) could serve as a novel sensing platform on electrochemical sensors with superior sensitivity.
Highly efficient adsorption of arsenite from aqueous by zirconia modified activated carbon
Pham Ngoc Chuc,Nguyen Quang Bac,Dao Thi Phuong Thao,Nguyen Trung Kien,Nguyen Thi Ha Chi,Nguyen Van Noi,Vo Thang Nguyen,Nguyen Thi Hong Bich,Dao Ngoc Nhiem,Dinh Quang Khieu 대한환경공학회 2024 Environmental Engineering Research Vol.29 No.2
Carbon-Nanotube Growth over Iron Nanoparticles Formed on CaCO3 Support by Using Hydrogen Reduction
Nguyen Duc Dung,Nguyen Van Chuc,Ngo Thi Thanh Tam,Nguyen Hong Quang,Phan Hong Khoi,Phan Ngoc Minh 한국물리학회 2008 THE JOURNAL OF THE KOREAN PHYSICAL SOCIETY Vol.52 No.5
Carbon nanotubes (CNTs) were grown by chemical vapor deposition on a mixture of iron salt and CaCO3. Salt mixtures of Fe(NO₃)₃9H₂O/CaCO₃ and FeCl₃6H₂O/CaCO₃ with various Fe weight contents were used as catalysts for growing the CNTs. A scanning electron microscope study revealed that the CNTs were densely grown on the Fe(NO₃)₃9H₂O/CaCO₃ catalyst containing 5 wt.% Fe. The effect of growth temperature on the segregation of Fe nanoparticles formed by hydrogen reduction is discussed. The result shows that 800 ℃ is the optimal temperature for the formation of Fe nanoparticles over which CNTs grow with the highest yield of 78.61 %. A raman spectroscope and a scanning transmission electron microscope were utilized to characterize the multiwall structure of the CNTs. The 92.16 % purity of the CNTs was determined by using thermal gravimetric analysis. Carbon nanotubes (CNTs) were grown by chemical vapor deposition on a mixture of iron salt and CaCO3. Salt mixtures of Fe(NO₃)₃9H₂O/CaCO₃ and FeCl₃6H₂O/CaCO₃ with various Fe weight contents were used as catalysts for growing the CNTs. A scanning electron microscope study revealed that the CNTs were densely grown on the Fe(NO₃)₃9H₂O/CaCO₃ catalyst containing 5 wt.% Fe. The effect of growth temperature on the segregation of Fe nanoparticles formed by hydrogen reduction is discussed. The result shows that 800 ℃ is the optimal temperature for the formation of Fe nanoparticles over which CNTs grow with the highest yield of 78.61 %. A raman spectroscope and a scanning transmission electron microscope were utilized to characterize the multiwall structure of the CNTs. The 92.16 % purity of the CNTs was determined by using thermal gravimetric analysis.
Synthesis of Carbon Nanotubes on Steel Foils
Nguyen Van Chuc,Nguyen Duc Dung,Phan Ngoc Hong,Le Dinh Quang,Phan Hong Khoi,Phan Ngoc Minh 한국물리학회 2008 THE JOURNAL OF THE KOREAN PHYSICAL SOCIETY Vol.52 No.5
Carbon nanotubes (CNTs) were synthesized by using a thermal chemical vapor deposition (CVD) at 800 ℃ in a mixture of C₂H₂, H₂ and N₂ gases with steel foils as both catalysts and substrates. More than 2 grams of CNTs were grown on approximately 7 grams of steel foil with a 0.5 cm² surface area after 30 minutes of growth. The effects of CVD parameters, such as the growth temperature and the deposition time, on the size and the morphology of the CNTs were studied using scanning electron microscopy (SEM). We found that the optimized temperature and growth time for having high quality CNTs were 800 ℃ and 30 minutes, respectively. The purity of the CNTs was evaluated by using thermogravimetric analysis (TGA) and the result showed that the carbon content was approximately 93 wt.%. The graphite crystallinity of the CNTs was analyzed by using Raman spectroscopy. The steel foil was found to maintain its catalytic behavior after several growths. The technique holds great promise for use in mass production (approximately 120 grams CNTs per day) with signicantly reduced cost. Carbon nanotubes (CNTs) were synthesized by using a thermal chemical vapor deposition (CVD) at 800 ℃ in a mixture of C₂H₂, H₂ and N₂ gases with steel foils as both catalysts and substrates. More than 2 grams of CNTs were grown on approximately 7 grams of steel foil with a 0.5 cm² surface area after 30 minutes of growth. The effects of CVD parameters, such as the growth temperature and the deposition time, on the size and the morphology of the CNTs were studied using scanning electron microscopy (SEM). We found that the optimized temperature and growth time for having high quality CNTs were 800 ℃ and 30 minutes, respectively. The purity of the CNTs was evaluated by using thermogravimetric analysis (TGA) and the result showed that the carbon content was approximately 93 wt.%. The graphite crystallinity of the CNTs was analyzed by using Raman spectroscopy. The steel foil was found to maintain its catalytic behavior after several growths. The technique holds great promise for use in mass production (approximately 120 grams CNTs per day) with signicantly reduced cost.
New Technique for the Synthesis of Carbon Nanotubes
Phan Ngoc Minh,Phan Hong Khoi,Nguyen Van Chuc,Phan Ngoc Hong,Ngo Thi Thanh Tam 한국물리학회 2008 THE JOURNAL OF THE KOREAN PHYSICAL SOCIETY Vol.53 No.5
Carbon nanotubes (CNTs) are considered as a promising material for various applications. However, due to their limited availability and high purchasing costs, at the present time, only a few of these applications have been realized. The realization of CNT-based devices and CNT-based materials depends on success in material synthesis and on the possibility of controlling the nanotube's chirality, diameter and purity. This paper describes new simple techniques for (i) synthesis of vertically-aligned carbon nanotubes (VA-CNTs), (ii) mass and low-cost production of multiwall carbon nanotubes (MWCNTs) and (iii) growth of individual CNTs on tungsten tips.