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      • KCI등재

        Measurement and Theoretical Calculation Confirm the Improvement of T7651 Aging State Influenced Precipitation Characteristics on Fatigue Crack Propagation Resistance in an Al–Zn–Mg–Cu Alloy

        Kai Wen,Baiqing Xiong,Yongan Zhang,Zhihui Li,Xiwu Li,Lizhen Yan,Hongwei Yan,Hongwei Liu 대한금속·재료학회 2021 METALS AND MATERIALS International Vol.27 No.5

        Precipitation characteristics influencing fatigue crack propagation contained matrix precipitate, grain boundary precipitateand precipitate free zone for Al–Zn–Mg–Cu alloys. Over-aging treatment could effectively regulate precipitation and then tobe able to change fatigue crack propagation behavior compared with the peak aging state. In the current work, typical T651and T7651 aging tempers of the alloy were extracted via hardness, electrical conductivity and mechanical properties underone-step and two-step aging treatments. Fatigue crack propagation (FCP) rate under them was tested and correspondingprecipitation characteristics and fracture morphology were observed. The results indicated that fatigue crack propagationresistance for the T7651 temper possessed an obvious improvement on the side of that for the T651 temper, which was alsosupported by fracture appearance, including tearing ridge, tearing dimple and fatigue striation. The precipitation observationshowed that the T651 alloy contained GPI zone, GPII zone and ηʹ phase while the T7651 alloy possessed ηʹ phase and η phase.Compared with the T651 temper, matrix precipitate for the T7651 temper distinctly owed an expanding of size distributionand an enlargement of average size while cuttable phase still remained the dominance for both tempers. Grain boundaryprecipitate and precipitate free zone manifested no obvious difference between the two aging tempers. Cut and bypass mechanismsof dislocation–precipitate interactions were used for explanation and it revealed the reinforced cuttable phase was infavor of enhancing fatigue crack propagation resistance. A theoretical model which directly correlated FCP rate with matrixprecipitate characteristics was employed to calculate FCP rate by substituting quantitative precipitate characteristics and thecalculation results were vaguely consistent with the experimental measurement, which proved its reliability and feasibility.

      • KCI등재

        Effect of Various Retrogression Regimes on Aging Behavior and Precipitates Characterization of a High Zn-Containing Al–Zn–Mg–Cu Alloy

        Kai Wen,Baiqing Xiong,Yongan Zhang,Zhihui Li,Xiwu Li,Shuhui Huang,Lizhen Yan,Hongwei Yan,Hongwei Liu 대한금속·재료학회 2018 METALS AND MATERIALS International Vol.24 No.3

        In the present work, the infl uence of various retrogression treatments on hardness, electrical conductivity and mechanicalproperties of a high Zn-containing Al–Zn–Mg–Cu alloy is investigated and several retrogression regimes subjected to a samestrength level are proposed. The precipitates are qualitatively investigated by means of transmission electron microscopy(TEM) and high-resolution transmission electron microscopy techniques. Based on the matrix precipitate observations, thedistributions of precipitate size and nearest inter-precipitate distance are extracted from bright-fi eld TEM images projectedalong ⟨110⟩ Al orientation with the aid of an imaging analysis and an arithmetic method. The results show that GP zonesand η′ precipitates are the major precipitates and the precipitate size and its distribution range continuously enlarge with theretrogression regime expands to an extent of high temperature. The nearest inter-precipitate distance ranges obtained arequite the same and the average distance of nearest inter-precipitates show a slight increase. The infl uence of precipitates onmechanical properties is discussed through the interaction relationship between precipitates and dislocations.

      • KCI등재

        Microstructure Evolution of High-Alloyed Al–Zn–Mg–Cu–Zr Alloy Containing Trace Amount of Sc During Homogenization

        Yu Wang,Zhihui Li,Baiqing Xiong,Kai Wen,Shuhui Huang,Xiwu Li,Yongan Zhang 대한금속·재료학회 2019 METALS AND MATERIALS International Vol.25 No.3

        Microstructure evolution of a new high-alloyed Al–Zn–Mg–Cu–Zr–Sc aluminium alloy during two-stage homogenizationprocess was investigated by use of scanning electron microscope, transition electron microscope and high resolution transitionelectron microscope. The results indicate that the morphology and chemical composition of Al 3 (Sc, Zr) particles formedin the fi rst stage were greatly aff ected by heating temperature. With the increase of heating temperature, the morphologyof Al 3 (Sc, Zr) particles transform from cuboidal with evident faceting to spheroidal due to improved Zr diff usivity. MoreZr atoms enrich in the interface of precipitate/matrix forming a thin layer. Moreover, the mean diameter of precipitatesincreases a little bit with the increase of heating temperature, showing very restricted coarsening rate and high thermal stabilityof Al 3 (Sc, Zr) particles. After an appropriate second stage heat treatment (474 °C × 48 h), the intermetallic formed inthe solidifi cation process could dissolve suffi ciently and Al 3 (Sc, Zr) particles still keep very good coherency with Al matrixwithout abnormal growth.

      • KCI등재

        Effect of In-situ TiC particles on the microstructure and mechanical properties ofAl8.5Fe1.4V1.7Si aluminum alloy

        Baohong Zhu,Yong’an Zhang,Baiqing Xiong,Hongwei Liu,Likai Shi,Songxiao Hui 한양대학교 세라믹연구소 2006 Journal of Ceramic Processing Research Vol.7 No.2

        Heat-resistant Al-Fe-V-Si aluminum alloys enhanced by in-situ TiC particles have been prepared by spray forming process with suitable process parameters. Research results show that the microstructure of the as-deposited alloy is fine and homogeneous. In-situ TiC particles prevent the unstable phases from coming into being. On the other hand, the TiC particles increase the volume fraction of heat-resistant phases. So the mechanical properties of the reinforced alloy by in-situ TiC particles are better than that of Al-Fe-V-Si alloy without the TiC particles. The hot extrusion temperature is also an important parameter to be considered. It is proved better to extrude the alloy at lower temperature. The tensile strength of the alloy without TiC particles is about 435 MPa at room temperature and is about 204 MPa at 350oC. However, when the alloy is enhanced by in-situ TiC particles, the strength of alloy is about 482 MPa at room temperature and is about 224 MPa at 350oC.

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