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황종일,Andrew T. Melville,지태구,김용규 대한금속·재료학회 2009 METALS AND MATERIALS International Vol.15 No.2
Experimental data on the activity of carbon in commercial plain carbon steel, AISI type 1010, common shimstock material, at 871 °C, 927 °C, 1000 °C, and 1038 °C, equilibrated with common endothermic carburizing atmospheres, were found to be generally in agreement at relatively high carbon concentrations with previously published data on pure iron equilibrated with CO-CO2 mixtures. However, noticeable differences were found at low carbon concentrations. The carbon contents of type 1010 steel were generally higher compared to those of previously published data regarding pure iron except at very high activities of carbon. The carbon contents of type 1010 steel foil specimens by weight gain were generally higher than or equal to those chemically analyzed; however, they corresponded with each other within 0.02 wt.% except at very low carbon potentials. Experimental data on the activity of carbon in commercial plain carbon steel, AISI type 1010, common shimstock material, at 871 °C, 927 °C, 1000 °C, and 1038 °C, equilibrated with common endothermic carburizing atmospheres, were found to be generally in agreement at relatively high carbon concentrations with previously published data on pure iron equilibrated with CO-CO2 mixtures. However, noticeable differences were found at low carbon concentrations. The carbon contents of type 1010 steel were generally higher compared to those of previously published data regarding pure iron except at very high activities of carbon. The carbon contents of type 1010 steel foil specimens by weight gain were generally higher than or equal to those chemically analyzed; however, they corresponded with each other within 0.02 wt.% except at very low carbon potentials.
황종일,지태구,김영규,황태영 대한금속·재료학회 2010 METALS AND MATERIALS International Vol.16 No.5
Carbon contents by the weight gain of AISI type 1010 steel foils equilibrated with CO-CO2 mixtures at 1000 °C were 0.03 wt.% to 0.07 wt.% higher than those by chemical analysis at carbon potentials of 0.2wt.%C to 0.7 wt.%C. The lower the carbon potential, the bigger the difference became. This difference of 0.05 wt.% to 0.08 wt.% was also measured when the same materials were equilibrated with CO-CO2 mixtures at 1038 °C at carbon potentials below 0.4 wt.%C. Oxygen analyses of these equilibrated steel foils confirmed that those differences of 0.03 wt.% to 0.07 wt.% and 0.05 wt.% to 0.08 wt.% were mainly due to the selective oxidation of manganese. When Armco steels and type 1010 steels were equilibrated simultaneously with endothermic-base carburizing atmospheres at 1038 °C, oxidation was negligible and the carbon contents of the both steels were identical at carbon potentials of 0.2 wt.%C to 1.4 wt.%C.
PLD 공정으로 제조된 LSM-YSZ 나노복합체층이 포함된 경사구조 박막 공기극을 적용한 SOFC의 성능 분석
명두환,홍종일,황재연,이종호,이해원,김병국,조성걸,손지원,Myung, Doo-Hwan,Hong, Jong-Ill,Hwang, Jae-Yeon,Lee, Jong-Ho,Lee, Hae-Weon,Kim, Byung-Kook,Cho, Sung-Gurl,Son, Ji-Won 한국세라믹학회 2011 한국세라믹학회지 Vol.48 No.6
The effect of the application of lanthanum strontrium manganite and yttria-stabilized zirconia (LSM-YSZ) nano-composite fabricated by pulsed laser deposition (PLD) as a cathode of solid oxide fuel cell (SOFC) is studied. A gradient-structure thin-film cathode composed of 1 micron-thick LSM-YSZ deposited at an ambient pressure ($P_{amb}$) of 200 mTorr; 2 micron-thick LSM-YSZ deposited at a $P_{amb}$ of 300 mTorr; and 2 micron-thick lanthanum strontium cobaltite (LSC) current collecting layer was fabricated on an anode-supported SOFC with an ~8 micron-thick YSZ electrolyte. In comparison with a 1 micron-thick nano-structure single-phase LSM cathode fabricated by PLD, it was obviously effective to increase triple phase boundaries (TPB) over the whole thickness of the cathode layer by employing the composite and increasing the physical thickness of the cathode. Both polarization and ohmic resistances of the cell were significantly reduced and the power output of the cell was improved by a factor of 1.6.