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Zr-V-Mn-Ni계 라브스상 합금의 미세 구조와 전기 화학적 특성
정치규,한동수,정원섭,김인곤,김원백,Jeong, Chigyu,Han, Dongsoo,Chung, Wonsub,Kim, Ingon,Kim, Wonbaek 한국수소및신에너지학회 1997 한국수소 및 신에너지학회논문집 Vol.8 No.3
아크 용해법으로 제작한 $ZrV_{0.1}Mn_{0.7}Ni_{1.2}$ 합금(bulk 합금) 잉고트는 $ZrV_{0.2}Mn_{0.98}Ni_{1.04}$의 조성식을 가지는 fcc 구조의 C15형 Laves상이 주류를 이루는 matrix와 $ZrV_{0.01}Mn_{0.13}Ni_{1.2}$의 조성으로 $Z_9Ni_{11}$의 금속간 화합물 구조를 가지는 2nd phase가 균일하게 분포된 2개의 상으로 구성되어 있었다. $ZrV_{0.1}Mn_{0.7}Ni_{1.2}$ 합금의 방전 특성에 이 두 가지 상들이 미치는 영향을 알아보기 위해서 matrix와 2'nd phase합금을 분리 제작하였고, 이들 전극에 대한 전기 화학적인 충방천 특성들을 조사하였다. 그 결과 방전용량은 2nd phase가 가장 낮은 $160mAh/g$, 그 다음으로 matrix가 200mAh/g으로 bulk의 250mAh/g보다 낮았다. Matrix조성의 합금은 bulk합금과 거의 유사한 활성화, 고율 방전율, 자기방전 특성을 가졌고, 또한 활성화 후에 충방전에 따른 용량감소의 경향이 현저히 관찰되었다. 그러나 2nd phase 조성의 합금은 이들과는 확연한 차이를 보였다. 즉 활성화되기 어렵지만 활성화된 후에 용량감소의 경향은 거의 없었고 또한 자기방전 특성도 우수하였다. $ZrV_{0.1}Mn_{0.7}Ni_{1.2}$ alloy ingot (bulk alloy) made by the arc melting was found to be consisting of mostly of $ZrV_{0.2}Mn_{0.98}Ni_{1.04}$ matrix alloy and $ZrV_{0.01}Mn_{0.13}Ni_{1.2}$ 2nd phase alloy. The former alloy had the form of the C15 type Laves alloy structure and the latter one had the intermetallic compound structure of $Zr_9Ni_{11}$. In order to investigate the effect of these two phases on the electrochemical charge-discharge characteristics of bulk $ZrV_[0.1}Mn_0.7}Ni_{1.2}$ alloy, the matrix and the 2nd phase alloys were fabricated separately by arc melting method and their electrochemical characteristics were studied and compared with the bulk alloy. It was found that the discharge capacity was the lowest of 160 mAh/g in the 2nd phase alloy. The matrix alloy exhibited 200 mAh/g. Both were lower than that of the bulk alloy of 250 mAh/g. The matrix and the bulk alloys showed a similar properties in the activation stage, the high rate dischargeability and the self discharge characteristics. Also a signigicant capacity decrease was observed after activation in both alloys. Whereas the 2nd phase alloy showed the very different characteristics. This alloy was found to be difficult to activate. However the capacity was remained constant after the activation. Also the self discharge rate was seen to be better than those of the matrix and the bulk alloys.
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복사에너지를 이용한 TIM소재의 방열 특성 향상을 위한 연구
황명원,김도형,정우창,정원섭,Hwang, Myungwon,Kim, Dohyung,Jung, Uoo-Chang,Chung, Wonsub 한국표면공학회 2019 한국표면공학회지 Vol.52 No.2
The aim of this study is to quantitatively demonstrate the possibility of heat transfer by thermal radiation by comparing heat transfer by conventional heat transfer and radiation by radiation. 1) The heat transfer was measured by using filler of TIM material with low thermal conductivity (CuS). As a result, heat transfer was easier than ceramic with high thermal conductivity ($Al_2O_3$ and $Si_3N_4$). 2) The reason for this is thought to be that the infrared wave due to radiation of the air diaphragm has moved easily. 3) From the above results, the heat dissipation of the TIM material indicates the possibility of heat transfer by thermal radiation.
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Ag925의 전기화학적 특성에 미치는 네오디뮴 함량의 영향
신병현(Byung-Hyun Shin),정승진(Seungjin Jung),정원섭(Wonsub Chung) 한국표면공학회 2021 한국표면공학회지 Vol.54 No.2
Ag925, silver with added copper, is popular alloy due to its low price. However, it has a difficult to use because of the low corrosion resistance. In various alloys, neodymium (Nd) works as an element to improve corrosion resistance by reacting with interstitial elements in the alloy. When 1.5 wt. % Neodymium was added to Ag925, the potential on the activated polarization in a potentiodynamic polarization test was increased from -0.15 V to –0.05 V. Ag925 with added neodymium showed the passivation after activation polarization. But When the potential increased around 50 ㎷, the current density is increased to 3 x 10-3. Ag925 with the 1.5 wt. % Nd had the low corrosion rate.
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서미희(Mihui Seo),김동현(Donghyun Kim),이정훈(Junghoon Lee),정원섭(Wonsub Chung) 한국표면공학회 2013 한국표면공학회지 Vol.46 No.5
The aim of the present study was to improve the radiative heat dissipation of aluminum alloy, Al 1050. Resin/CuO coating and Cu/CuO composite plating were applied on aluminum alloy to improve the radiative heat dissipation. Resin/CuO coating was made using thermosetting silicon resin and Cu/CuO composite plating was made in pyrophosphate copper plating bath. Radiant heat flux(W/㎡) was measured by self-produced radiant heat measurement device to compare each specimen. The cross section of specimen and chemical bonding of surface were analyzed by FE-SEM, XPS and FT-IR. As a result, radiant heat of Resin/CuO coating was higher than Cu/CuO composite plating due to the adhesion with aluminum plate and the difference in chemical bonding. But, Both of them were higher than aluminum alloy. In order to confirm the result of experiment, aluminum plate, Resin/CuO coating and Cu/CuO composite plating sample were applied LED and measured the LED temperature. As a result, LED temperature of samples were matched previous results and confirmed coated samples were lower about 10 degrees than the aluminum alloy.
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