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무가압 분말 충전 성형법에 의한 알루미늄 성형체의 산화반응 소결체 제조에 대한 연구
박정현,홍기의,염강섭,유재영 한국세라믹학회 1997 한국세라믹학회지 Vol.34 No.1
평균입경이 22.1$\mu$m인 알루미늄 분말을 사용하여 무가압 분말 충전 성형법으로 52%의 상대밀도를 갖는 성형체를 제조하였다. 산화반응의 활성화 에너지는 TG의 무게 변화로부터 구하였으며, 16~64kJ/mol 범위의 값을 나타내었다. 활성화에너지의 변화와 미세구조의 관찰로부터 산화반응이 산화막의 파괴와 용출에 의존함을 확인하였다. 알루미늄 성형체를 1000~140$0^{\circ}C$에서 4~60시간동안 산화반응시켰을 때, 알루미늄의 산화반응이 시간보다 온도에 의존하였다. 140$0^{\circ}C$에서 60시간동안 산화반응시킨 시편의 산화율은 92%를 나타내었으며, 이 시편을 다시 1$600^{\circ}C$에서 15시간 소결시켰을 때, 소결체는 62%의 상대밀도를 나타내었다. Using aluminum powder with average particle size of 22.1 $\mu$m, aluminum compact made by Pressureless Powder Packing Method showed 52% green density. The activation energy of aluminum oxidation was cal-culated from the weight change of TG, and it was varied in the range of 16~64 kJ/mol. It was found from the variation of the activation energy and the observation of the microstructure that oxidation was de-pendent on the destruction of oxide film and the melt-out of aluminum. Aluminum compact was reaction-bonded at 1000~140$0^{\circ}C$ for 4~60hrs, and oxidation was dependent on temperature rather than time. Reac-tion-bonded aluminum oxide at 140$0^{\circ}C$ for 60hrs showed 92% oxidation percent. It was sintered at 1$600^{\circ}C$ for 15hrs and the sintered body showed 62% relative density.
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박정현,이현권,정경원,염강섭 한국세라믹학회 1992 한국세라믹학회지 Vol.29 No.6
Fabrication possibility of low-shrinkage alumina without oxidation and wetting agent was presented on the basis of observation about oxidation behavior, microstructure and physical characteristics of such reaction agents free Al2O3-Al system. The composition less than Al 10w/o where Al can act as a sintering agent for Al2O3 was excluded. Under the condition of present experiments oxidation of Al2O3-Al system was dependent not on holding time but mainly on oxidation temperature. In thes case of Al powder not comminuted effectively during powder mixing of Al2O3-Al, columnar structure which would act as a hindrance to the densification during sintering developed more during oxidation with higher Al contents, and which made the fabrication of low-shrinkage Al2O3 ceramics impossible. If Al powder was comminuted effectively due to co-mixed Al2O3 characteristics, densification was improved because of no columnar structure and made the fabrication of sintered body with -2.7% dimensional change and 81% relative density possible. As a result, it is possible to fabricate dense low-shrinkage Al2O3 ceramics without oxidation and wetting agent under conditions such as smaller particle size of Al, Al contents below 50v/o, higher green density of Al2O3-Al compact and the use of Al2O3 powder used for high-density ceramics.
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무가압 분말 충전 성형법에 의해 제조된 Si 성형체의 반응 소결과 가스압 소결에 관한 연구
박정현,강민수,백승수,염강섭 한국세라믹학회 1996 한국세라믹학회지 Vol.33 No.12
평균 입경 8${\mu}{\textrm}{m}$ Si 분말을 사용하여 무가압 분말 충전 성형볍에 의해 Si 성형체를 제조하였다. 이 Si 성형체를 1350,140$0^{\circ}C$의 온도에서 3~35시간동안 N2/H2 분위기에서 반응 소결한 후 미세구조를 관찰하였다. 반응 소결체는 90% 이상의 질화율과 88%의 상대밀도를 보였다. 반응 소결체의 가스압 소결을 위해 소결조제로서 MgO를 Mgnitrate 수용액 형태로 Si 성형체에 5wt% 첨가한 후140$0^{\circ}C$에서 15시간동안 반응 소결하였다. 이후 반응 소결체를 1800, 1900, 200$0^{\circ}C$에서 각각 150, 300분 동안 가스압 소결을 행하여 95%의 상대밀도와 598 MPa의 꺾임강도, 6 MPa.m1/2의 파괴인성을 나타내는 질화규소 소결체를 제조하였다. Using Si powder with average particle size of 8${\mu}{\textrm}{m}$ Si compacts were formed by pressureless powder packing method. The compacts were reaction bonded at 1350, 140$0^{\circ}C$ for 3~35 hrs under N2/H2 atmosphere and its microstructures were examined. Reaction bonded silicon nitrides showed nitridation of 90% and relative density of 88% After the impregnation of 5wt% MgO as sintering additive using aqueous solution of Mg nitrate the Si compacts were reaction bonded at 140$0^{\circ}C$ for 15hrs. The reaction bonded bodies were gas pressure sintered at 180$0^{\circ}C$ 190$0^{\circ}C$ 200$0^{\circ}C$ for 150, 300min. They showed relative density of 95% bending strength of 600MPa and fracture toughness of 6 MPa.m1/2.
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$BaTiO_3$ 세라믹스와 Oxide Setter의 반응성에 관한 연구
박정현,최현정,조경식,염강섭,조철구 한국세라믹학회 1994 한국세라믹학회지 Vol.31 No.6
BaTiO3 ceramics were sintered on Al2O3, MgAl2O4, MgO and Mg-, Ca-, Y-stabilized zirconia setters. Then the influence of setters on the microstructure of BaTiO3 ceramics and the stability of setters were investigated by SEM, EDAX and XRD analyses. The microstructure of BaTiO3 ceramics sintered on Al2O3, MgAl2O4, MgO and Mg-PSZ showed large grain growth, but little grain growth on Ce-TZP(Tetragonal Zirconia Policrystal). Mg-PSZ(Partially Stabilized Zirconia), Ca-PSZ, Ce-TZP setters showed extensive phase transformation. Y-TZP and fused Y-SZ (Stabilized Zirconia) setters were stable. The liquid sintering aids of BaTiO3 ceramics accelerate mass transport. The reaction of SrTiO3 in BaTiO3 with ZrO2 resulted in the formation of SrZrO3.
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분말 충전 성형법을 이용한 SiC-Al Alloy 복합체의 제조
박정현,송준광,백승수,염강섭,강민수 한국세라믹학회 1997 한국세라믹학회지 Vol.34 No.4
To fabricate the ceramic/metal(SiC/ Al alloy) composite, SiC preform was prepared by Pressureless Powder Packing Forming Method and 6061 Al alloy was infiltrated into the preform. Uniform compact having an average pore size of 10 ${\mu}{\textrm}{m}$ and narrow pore size distribution was prepared. Phenolic resin solution(40 wt%) was penetrated into the SiC compact, and then the compact was preheated at the temperature of 120$0^{\circ}C$. The pore size distribution and the microstructure of the preform were not changed by preheating. An uniform microstructure without any crack in the preform was obtained in SiC-Al alloy composite. The infiltration of 6061. Al alloy into the preform began at the temperature of 130$0^{\circ}C$ and the amount of infiltration increased in proportion to the infiltration temperature and the soaking time. The increasement rate of the infiltration amount decreased after 3 h. As a result of the infiltration at 140$0^{\circ}C$ for 4 h, Al alloy was well distributed in the interparticle channels and the relative density of the composite was above 98%. The strength and the fracture toughness of the composite were 303 MPa and 21.65 MPam1/2, respectively.
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