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Alloy 282 초내열합금 모재 및 용접부의 기계적 특성과 미세조직에 미치는 시효열처리 조건의 영향
방진혁,강용준,김남규,서성문,이상훈,송상우,강남현 대한금속·재료학회 2020 대한금속·재료학회지 Vol.58 No.8
The effect of aging heat treatment conditions on the mechanical properties and microstructure of the base and weld metal of Alloy 282 superalloy was investigated. The aging heat treatment conditions employed in this study were as follows: two-steps (1010 °C for 2 hours plus 788 °C for 8 hours) and one-step at 788 °C, 738 °C, and 688 °C for 4 hours. The base metal with the one-step aged condition exhibited lower hardness but longer creep life than that treated with the two-step aged condition. The base metal subjected to the two-step aging exhibited the highest hardness and the shortest creep life, mainly due to the precipitation of Mo-rich M6C-type carbides and coarse γ' (Ni3(Al,Ti)) phase. For the weld metal, regardless of aging heat treatment conditions, creep elongation and life decreased significantly compared to the base metal, due to the coarse effective grain size and inhomogeneous distribution of γ' precipitates.
테라헤르츠 시간 영역 분광법을 이용한 스피로파이란의 광 퇴화 특성 연구
방진혁,박명환,류한철,Bang, Jin-Hyuk,Park, Myoung-Hwan,Ryu, Han-Cheol 대한화학회 2016 대한화학회지 Vol.60 No.1
스피로파이란은 반복적인 광 변색현상 과정에서 광 퇴화 특성을 보이는 대표적인 물질이다. 스피로파이란은 뛰어난 안정성, 빠른 응답속도, 강한 색 변화, 빛에 의한 물질의 화학적, 물리적 특성 조절이 가능하다는 점으로 광 스위치, 광 메모리, 바이오 센서 등의 다양한 분야에 적용되고 있다. 하지만 스피로파이란은 광 퇴화되며 기능이 점차 떨어지기 때문에, 광퇴화에 따른 스피로파이란의 특성 변화에 대해 자외선-가시광선 분광법, 핵 자기 공명 분광법, 라만 분광법 등을 이용한 많은 연구가 이루어지고 있다. 본 연구에서는 스피로파이란의 광 퇴화 특성을 테라헤르츠 주파수 영역에서 테라헤르츠 시간 영역 분광법(Terahertz time-domain spectroscopy, THz-TDS)을 이용하여 측정 및 분석하였다. 반복적인 자외선 조사에 따른 스피로파이란의 광 퇴화 특성이 테라헤르츠 영역에서의 흡수량 증가로 나타남을 확인하였다. 이러한 스피로파이란의 광 퇴화 특성이 야기하는 테라헤르츠 영역 흡수량 변화 경향은 가시광선 영역 흡수량 변화 경향과 서로 반대됨을 확인할 수 있었다. The spiropyran is a typical material having photodegradation properties in the process of photochromism. The spiropyran has been utilized in various applications such as optical switch, optical memories, and biosensor because of its remarkable stability, fast responsive time, stronger color change, and photo-induced controllability. However, the spriropyran is photodegraded by the repetitive optical irradiation. The photodegradation of spiropyran have been investigated by using UV-Visible spectroscopy, nuclear magnetic resonance (NMR), and Raman spectroscopy. Herein, the properties of spiropyran were characterized by using terahertz time-domain spectroscopy (THz-TDS) in the terahertz frequency region. In terahertz region, the measured absorbance of spiropyran was increased due to the photodegradation induced by the repetitive UV irradiation. The absorbance tendency of spiropyran in the terahertz frequency region was compared with that in the visible region, and they were completely opposite to each other.
방진혁(Jin Hyeok Bang),권기환(Ki Hwan Kwon),박재준(Jae Jun Park),조남규(Nahm Gyoo Cho) 대한기계학회 2004 대한기계학회 춘추학술대회 Vol.2004 No.11
This paper presents a force/displacement sensing system to measure penetration depths and machining forces during pattering operation. This sensing system consists of a leaf spring mechanism and a capacitive sensor, which is mounted on a PZT driven in-feed motion stage with 1㎚ resolution. The sample is moved by a xy scanning motion stage with 5㎚ resolution. The constructed system was applied to nano indentation experiments, and the load-displacement curves of silicon(111) and aluminum were obtained. Then, the indentation samples were measured by AFM. Experimental results demonstrated that the developed system has the ability of preforming force/depth sensing indentations
방진혁(J. H. Bang),권기환(K. H. Kwon),박재준(J. J. Park),조남규(N. G. Cho) 한국정밀공학회 2004 한국정밀공학회 학술발표대회 논문집 Vol.2004 No.10월
This paper presents a high sensitive force sensing module to measure machining forces for a tip-based nanopatterning instrument. The force sensing module utilizing a leaf spring mechanism and a capacitive displacement sensor has been designed to provide a measuring range from 80μN to 8N. This force sensing module is mounted on a PZT driven in-feed motion stage with 1 ㎚ resolution. The sample can be moved by a X-Y scanning motion stage with 5 ㎚ resolution. In the patterning experiments, the machining forces were controlled and monitored by the force sensing module. Then, the patterned sample was measured by AFM. Experimental results demonstrated that the developed force sensing module can be used as an effective sensing device in the nanopatterning operation.