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Gas chromatography-Thermal Energy Analyzer에 의한 휘발성 니트로소아민과 담배 특유의 니트로소아민들의 동시 분석연구
이문수,지상운,박영수,Rhee, Mun-Su,Ji, Sang-Woon,Park, Yang-Su 한국연초학회 1993 한국연초학회지 Vol.15 No.2
This is to investigate the methodology for the simultaneous determination of Wk, mk and TSNA using gas chromatography(GC) in combination with chemiluminescence detector, thermal energy analyzer(TEA) . The simultaneous analysis has been estimated by evaluating tobacco. The TEA was linked to GC equipped with non -polar SPB -5 fused silica capillary column which was introduced into the ceramic pyrolysis tube by the point of 16cm from the end of TEA. Quantification was carried out by internal standardization with WDPA after calibration of retention times and response factors with authentic nitrosoamines. It was demonstrated that WDPA was most preferable as internal standard for the simultaneous analysis. The recoveries of the internal standard were in the range of 83∼96% . Nitrosoamines in this method were detected with determination limit of 0.1ng and was made by a straight line in calibration curve by TEA response. The suitability of nitrosoamines extraction in tobacco leaf was investigated. It was most suitable to extract nitrosoamines from tobacco leaves with 0.01 M NaOH within a period of 8 hours. Thimerosal as an antibacterial agent was added to NaOH solution to prevent artifactual formation. The fractionation and the purification of nitrosoamines form alkaline extracts were conveniently performed using Extrelut multilayer column and dichloromethane. Reproducible and reliable results were obtained for the determination of nitrosamines in a relatively short time compared to previous known method. TSNA contents in burley were about 4 times higher as those in the fluecured tobacco.
이문수,장기철,지상운,Rhee, Mun-Su,Jang, Gi-Cheol,Ji, Sang-Un 한국연초학회 1993 한국연초학회지 Vol.15 No.1
Nitric oxide of gas phase in cigarette smoke was conveniently determined by Chemiluminescence NO analyzer with 20 ports rotary type smoking machine Data are presented to support this observation. On the basis of this method the amount of NO in the smoke from nonblended and commercial cigarettes were estimated. Gas phase NO concentration in main stream smoke was correlated well with the nitrate levels in tobacco leaves, but there was no correlation with the tar yields. In consequence, it would be considered that the methodology in this study provided simple and rapid quantification for NO in cigarette smoke.
Environmental Tobacco Smoke의 이화학적 특성
이문수 한국연초학회 1995 한국연초학회지 Vol.17 No.1
On the basis of the literature, which is at present still scientific information improvable, the results of research done so far into the occurrence and analytical methodology of major markers of environmental tobacco smoke(ETS) have been summarized. Key areas addressed are: differences in physicochemical composition between mainstream smoke, sidestream smoke and ETS: techniques for field measurement of ETS: relationship between indoor air quality with ETS and its distribution view of US EPA and its problems: biological effects and concerning estimation of ETS exposure.
탄.소성구성식에 의한 점토지반의 거동해석 (I) -Lade의 모델, 입방체 삼축시험 및 토질매개변수 결정-
이문수,이광동,오재화 한국농공학회 1993 韓國農工學會誌 : 전원과 자원 Vol.35 No.4
The purpose of this study is to develop a multireservoir water balance model which may be used to evaluate rural water demands such as agricultural water, domestic water, industrial water and livestock water and to determine effective storage of reservoir. The model was verified to compare the observed reservoir release data with the simulated reservoir release data of the existing Munsan and Dongbu reservoirs located in the Gisan rural district for 3 years('87~'89). For model application, the effective storages of existing reservoirs(Munsan & Dongbu) were evaluated for 10-year frequency drought and that of newly planned reservoirs(Kumbok & Kudong) were determined for 10-year frequency drought. In addition, the behavior of effective storages for existing reservoirs were analyzed in the case of introducing new reservoirs in the existing system.
彈${\cdot}$粘塑性構成式을 使用한 粘性土地盤의 變形解析
이문수,Lee, Moon-Soo 한국농공학회 1992 韓國農工學會誌 : 전원과 자원 Vol.34 No.2
This study aims at predicting the behavior of saturated soft clayey foundation subjected to earth structure loads such as tidal dike, embankment etc. by using Biot's consolidation equation coupled with elasto-viscoplastic constitutive model. To validate the computer program developed b author, a case study was performed for the site of Kwang-yang steel works improved by sand drain, where since the beginning of the works, field measurements(settlement, lateral displacement and excess pore water pressure) had been accurately achieved. Comparisons between numerical results and observation values were carried out. The main results obtained are summarized as follows : 1. Settlement and lateral displacement between numerical and observation values show satisfactory accordance. 2. As for the exess pre water pressure, numerical results appear to be larger than observation values, which may be due to the existence of sand seams which were not found during soil investigation. 3. Useful data available for failure prediction of soft foundation can be secured by examining lateral displacement, settlement, exess pore water pressure and stress paths.