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Weak u-S-flat Modules and Dimensions
Refat Abdelmawla Khaled Assaad,Xiaolei Zhang 경북대학교 자연과학대학 수학과 2023 Kyungpook mathematical journal Vol.63 No.3
In this paper, we generalize the notions uniformly S-flat, briefly u-S-flat, modules and dimensions. We introduce and study the notions of weak u-S-flat modules. An R-module M is said to be weak u-S-flat if TorR 1 (R/I, M) is u-S-torsion for any ideal I of R. This new class of modules will be used to characterize u-S-von Neumann regular rings. Hence, we introduce the weak u-S-flat dimensions of modules and rings. The rela tions between the introduced dimensions and other (classical) homological dimensions are discussed.
Disguised Full-Duplex Transmission-Aided Covert Communications
Refat Khan,Jihwan Moon(문지환) 대한전자공학회 2023 대한전자공학회 학술대회 Vol.2023 No.6
In this paper, we study a covert communications system where a source node communicates with a disguised full-duplex (FD) destination node. Supposedly receive-only, the destination node covertly delivers critical messages to another hidden receiver while evading the surveillance of a warden node as much as possible. We derive and minimize the detection error probability (DEP) of the covert message detector at the CF relay. The numerical results present the covert rate performance for different DEP requirements.
Dynamic characterization of 3D printed lightweight structures
Refat, Mohamed,Zappino, Enrico,Sanchez-Majano, Alberto Racionero,Pagani, Alfonso Techno-Press 2022 Advances in aircraft and spacecraft science Vol.9 No.4
This paper presents the free vibration analysis of 3D printed sandwich beams by using high-order theories based on the Carrera Unified Formulation (CUF). In particular, the component-wise (CW) approach is adopted to achieve a high fidelity model of the printed part. The present model has been used to build an accurate database for collecting first natural frequency of the beams, then predicting Young's modulus based on an inverse problem formulation. The database is built from a set of randomly generated material properties of various values of modulus of elasticity. The inverse problem then allows finding the elastic modulus of the input parameters starting from the information on the required set of the output achieved experimentally. The natural frequencies evaluated during the experimental test acquired using a Digital Image Correlation method have been compared with the results obtained by the means of CUF-CW model. The results obtained from the free-vibration analysis of the FDM beams, performed by higher-order one-dimensional models contained in CUF, are compared with ABAQUS results both first five natural frequency and degree of freedoms. The results have shown that the proposed 1D approach can provide 3D accuracy, in terms of free vibration analysis of FDM printed sandwich beams with a significant reduction in the computational costs.
Dynamic characterization of 3D printed lightweight structures
Refat, Mohamed,Zappino, Enrico,Sanchez-Majano, Alberto Racionero,Pagani, Alfonso Techno-Press 2022 Advances in aircraft and spacecraft science Vol.9 No.4
This paper presents the free vibration analysis of 3D printed sandwich beams by using high-order theories based on the Carrera Unified Formulation (CUF). In particular, the component-wise (CW) approach is adopted to achieve a high fidelity model of the printed part. The present model has been used to build an accurate database for collecting first natural frequency of the beams, then predicting Young's modulus based on an inverse problem formulation. The database is built from a set of randomly generated material properties of various values of modulus of elasticity. The inverse problem then allows finding the elastic modulus of the input parameters starting from the information on the required set of the output achieved experimentally. The natural frequencies evaluated during the experimental test acquired using a Digital Image Correlation method have been compared with the results obtained by the means of CUF-CW model. The results obtained from the free-vibration analysis of the FDM beams, performed by higher-order one-dimensional models contained in CUF, are compared with ABAQUS results both first five natural frequency and degree of freedoms. The results have shown that the proposed 1D approach can provide 3D accuracy, in terms of free vibration analysis of FDM printed sandwich beams with a significant reduction in the computational costs.
Refat, M. S.,Sadeek, S. A. Korean Chemical Society 2006 대한화학회지 Vol.50 No.2
[X=ortho (L1), meta(L2) 및 para(L3)]리간드를 갖는 주석(II) 화합물들을 합성하고, 그 특성을 원소분석, 적외선 분광광도법, 자외선/가시광선 분광광도법 및 열분석법을 이용하여 확인하였다. 자외선 분광광도법을 통하여, 주어진 ONNO 주게 리간드들의 이민(imine) 및 카보닐기의 배위 모드가 C2v 대칭성을 갖는 것으로 나타났다. 또한 열분석 결과, Sn(L3) 화합물이 가장 높은 활성화 에너지를 가지는 반면, Sn(L2) 화합물이 가장 낮은 활성화 에너지를 가짐을 알 수 있었다. Complexes of Sn(II) with L1 = acac-o-phdnH2 [N,N'-o-phenylene bis(acetylacetoneimine)], L2 = acac-m-phdnH2 [N,N'-m-phenylene bis(acetylacetoneimine)] and L3 = acac-p-phdnH2 [N,N'-p-phenylene bis(acetylacetoneimine)] have been prepared and characterized by elemental analyses, vibrational, electronic spectra and thermal studies (TGA and DTA). Vibrational spectra indicated the coordination mode of imine and carbonyl oxygen for ligands giving (ONNO) that belong to C2V point group symmetry. The [Sn(L3)] complex has a maximum activation energy and [Sn(L2)] complex has a minimum activation energy.
Refat, Moamen S.,Megahed, Adel S.,El-Deen, Ibrahim M.,Grabchev, Ivo,El-Ghol, Samir Korean Chemical Society 2011 대한화학회지 Vol.55 No.1
본 연구에서는 Benzanthrone 치환체인 3-N-2-hydroxy ethylamine benzanthrone (HEAB)와 3-N-2-amino ethylamine benzanthrone (AEAB)의 Cu(II), Co(II) 및 Ni(II) 염화물 착물에 대한 분광학 (IR, UV-vis 및 $^1H$-NMR), 원소분석, 몰전도도, 열무게분석 (TGA/DTG) 및 생물학적 특성에 대해 고찰하였다. 이 연구의 결과에서 HEAB리간드가 히드록소 및 아미노기를 통하여 각 금속에 배위되어 [Cu(HEAB)$(Cl)_2$].$2H_2O$, [Co(HEAB)$(Cl)_2(H_2O)_2$].$8H_2O$ 및 [Ni(HEAB)$(Cl)_2(H_2O)_2$].$7H_2O$ 착물을 형성함을 알았다. 한편, AEAB는 [Cu(HEAB)$(Cl)_2$].$2H_2O$, [Co(HEAB)$(Cl)_2(H_2O)_2$].$8H_2O$ 및 [Ni(HEAB)$(Cl)_2(H_2O)_2$].$7H_2O$의 분자식을 갖는 팔면체 배위구조를 갖는다. $25^{\circ}C$ DMF에서 모든 착물의 몰전기전도도는 반응안한 리간드보다 약간 컸는데, 이는 염화 이온이 배위권 내부에 존재함을 의미한다. Benzanthrone계 리간드와 이들 착물을 이용하여 서로 다른 종류의 박테리아에 대한 생물활성을 조사하였다. Spectroscopic (infrared, electronic and $1^H$-NMR), elemental analyses CHN, molar conductivity, thermogravimetric analyses (TGA/DTG) and biological studies, of both benzanthrone derivatives 3-N-2-hydroxy ethylamine benzanthrone (HEAB) and 3-N-2-amino ethylamine benzanthrone (AEAB) with Cu(II), Co(II) and Ni(II) chlorides were discussed herein. Based on the above studies, HEAB ligand was suggested to be coordinated to each metal ions via hydroxo and amino groups to form [Cu(HEAB)$(Cl)_2$].$2H_2O$, [Co(HEAB)$(Cl)_2(H_2O)_2$].$8H_2O$ and [Ni(HEAB)$(Cl)_2(H_2O)_2$].$7H_2O$ coordinated complex. On the other hand, AEAB has an octahedral coordinated feature with formulas [Cu(AEAB)$(Cl)_2(H_2O)_2$].$2H_2O$, [Co(AEAB)$(Cl)_2(H_2O)_2$].$4H_2O$ and [Ni(AEAB)$(Cl)_2(H_2O)_2$]. $6H_2O$. The molar conductance values at $25{\circ}C$ for all complexes in DMF are slightly higher than free ligands; this supported the presence of chloride ions inside the coordination sphere. Both benzanthrone ligands and their complexes have been screened against different kinds of bacteria.
Refat, Moamen S.,Mohamed, Gehad G.,Fathi, Ahmed Korean Chemical Society 2010 Bulletin of the Korean Chemical Society Vol.31 No.6
Spectrophotometric micro determination of allopurinol (ALP) via charge-transfer formation is described. This includes the utility of some $\pi$-acceptors such as 2,3-dichloro-5,6-dicyano-p-benzoquinone (DDQ) and 3,6-dichloro-2,5-dihydroxy-p-benzoquinone (p-CLA) for estimation of ALP drug (act as $\grave{e}$-donor). These reactions are applied for determination of ALP in its pharmaceutical preparations coming from different companies. Elucidation of the chemical structure of the solid CT complexes formed via reaction between drugs under study and $\pi$-acceptors, using elemental analyses (C, H, N), I. R., $^1H$ NMR and mass spectrometry.