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Muhammad Altaf Nazir,Tayyaba Najam,Muhammad Sohail Bashir,Muhammad Sufyan Javed,Muhammad Aswad Bashir,Muhammad Imran,Umair Azhar,Syed Shoaib Ahmad Shah,Aziz ur Rehman 한국화학공학회 2022 Korean Journal of Chemical Engineering Vol.39 No.1
The use of highly efficient, environment-friendly and economically inexpensive materials for the adsorption removal of contaminants from water has always been considered as emerging task. In this study, we synthesized hybrid tri-metallic nickel cobalt layered double hydroxide (NiCoAl-LDH) porous material for the adsorption removal of Eosin yellow (EY) and Malachite green (MG) from water. The characterization results disclosed that tri-metallic LDH has been synthesized with extraordinary purity, identical morphology and high surface area (134.21 m2·g−1). The NiCoAl-LDH performs the best for adsorption of EY (qe=37.30mg·g−1 at pH=2) and MG (qe=39.61 mg·g−1 at pH=10). The Langmuir and Freundlich isotherm models were applied to explain the adsorption process of dyes on the surface of LDH. The Langmuir model (R2=0.991 and 0.999 for Eosin Y and Malachite G, respectively) was very appropriate to explain the process of adsorption on NiCoAl-LDH as homogeneous (monolayer). The maximum adsorption capacity of EY and MG calculated with Langmuir model was 78.74 and 110.13 mg·g−1 at 30 °C, respectively. Also with 240 minutes contact time 94.8% EY and 89.9% MG was adsorbed by as synthesized NiCoAl-LDH nanosheets. The NiCoAl-LDH nanosheets showed excellent performance of reusability of up to five regeneration cycles. The results showed that the adsorption capacity of NiCoAl-LDH nanosheets after five regeneration cycles, to adsorb EY, decreased only from 40.80 to 36.93 mg·g−1 and that of MG from 79.21 to 75.42 mg·g−1, which is acceptable. The overall results Suggest that the fabricated NiCoAl-LDH is favorable for the purification of dye contaminated water.
Muhammad Kashif Iqbal Khan,Abid Aslam Maan,Rana Muhammad Aadil,Akmal Nazir,Masood Sadiq Butt,Muhammad Imtiaz Rashid,Muhammad Inam Afzal 한국식품과학회 2020 Food Science and Biotechnology Vol.29 No.4
Onion and ginger are rich sources of bioactive compounds which are lost during conventional drying process. The present study was designed to optimize the novel Microwave Assisted Drying and Extraction technique (MADE) for simultaneous drying and extraction/recovery of bioactive compounds from model food products. The time required for drying of samples was 11 (onion) and 16 (ginger) minutes with recovery yield of 87% (onion) and 85% (ginger). The drying time was reduced to 100 times compared to hot air drying and moisture ratio of dried samples was best described by Midilli model. The diffusivities of onion and ginger slices were 1.27 e-11 and 1.43 e-11 m2/s, respectively. Moreover, microwave-based extraction was compared with conventional one. The results of antioxidant activity and total phenolic contents of condensates obtained through MADE were higher compared to conventional method. In short, MADE exhibited better yield of extraction and drying properties compared to conventional methods.
Muhammad Kamran,Nazir Javed,Ihsan Ullah,Shahid Nazir,Shakra Jamil,Muhammad Zafar Iqbal,Huma Abbas,Sajid Aleem Khan,Muhammad Ehetisham ul Haq 한국식물병리학회 2019 Plant Pathology Journal Vol.35 No.1
A great variable response was observed when PP-3 and PP-J encumbered with 116 populations of root knot nematode (RKN) at two different temperatures (25 ± 2°C and 30 ± 2°C) and concentrations (104 and 105 spores/ml). The PCR reaction amplified intergenic region between cytochrome oxidase subunit II gene (COII) and large subunit of rRNA gene (lrRNA) of the mitochondrial genome of different RKN species. The primer C2F3 and 1108 identified M. incognita with the highest frequency (52.6%) followed by M. javanica (36.8%) and M. arenaria (10.5%). The sizes of PCR products were 1.7 kb for M. incognita and M. javanica populations while populations of M. arenaria produced 1.1 kb fragment. The digestion with Hinf I yielded three different fragment length patterns on 1.5 % agarose gel. From current research it is concluded that intra-Meloidogyne genetic variability exist in RKN populations which have better encumbrance with P. penetrans.
Kamran, Muhammad,Javed, Nazir,Ullah, Ihsan,Nazir, Shahid,Jamil, Shakra,Iqbal, Muhammad Zafar,Abbas, Huma,Khan, Sajid Aleem,Haq, Muhammad Ehetisham ul The Korean Society of Plant Pathology 2019 Plant Pathology Journal Vol.35 No.1
A great variable response was observed when PP-3 and PP-J encumbered with 116 populations of root knot nematode (RKN) at two different temperatures ($25{\pm}2^{\circ}C$ and $30{\pm}2^{\circ}C$) and concentrations ($10^4$ and $10^5$ spores/ml). The PCR reaction amplified intergenic region between cytochrome oxidase subunit II gene (COII) and large subunit of rRNA gene (lrRNA) of the mitochondrial genome of different RKN species. The primer C2F3 and 1108 identified M. incognita with the highest frequency (52.6%) followed by M. javanica (36.8%) and M. arenaria (10.5%). The sizes of PCR products were 1.7 kb for M. incognita and M. javanica populations while populations of M. arenaria produced 1.1 kb fragment. The digestion with Hinf I yielded three different fragment length patterns on 1.5 % agarose gel. From current research it is concluded that intra-Meloidogyne genetic variability exist in RKN populations which have better encumbrance with P. penetrans.
Microwave-assisted urea-modified sorghum biomass for Cr (III) elimination from aqueous solutions
Muhammad Salman,Makshoof Athar,Umar Farooq,Huma Nazir,Anam Noor,Saba Nazir 한국화학공학회 2013 Korean Journal of Chemical Engineering Vol.30 No.6
The present study concentrated on the use of an agro-waste biodegradable sorghum biomass in its simple and modified forms for the binding of Cr (III) ions. A relatively new method of modification was adopted using urea under microwave irradiation. FTIR analysis showed the presence of oxygen and nitrogen bearing functional groups in unmodified (UMS) and modified (MS) sorghum biomass. The appearance of new bands and shifts in the peaks confirmed the modification. The influence of different process parameters such as the adsorbent dose, solution pH, contact time, agitation speed and initial metal ion concentration was studied thoroughly to evaluate optimum conditions for adsorption. Maximum adsorption for Cr (III) ions occurred at pH 5.0-6.0 using UMS and MS. Langmuir, Freundlich,Temkin, and Dubinin-Radushkevich isotherm models in a non-linear fashion were used to explain the phenomenon. Maximum adsorption capacity was 7.03 and 16.36 mg of Cr (III) per gram of UMS and MS, respectively. Adsorption mechanism was explored by pseudo-first- and pseudo-second-order kinetic models, and it was found that the process followed pseudo-second-order kinetics. Thermodynamic study indicated the process favorability. The study concluded that urea modification under microwave irradiation produces a non-toxic and more effective adsorbent for Cr (III) remediation by inducing new nitrogen bearing functional groups to sorghum biomass.
Real-Time Brain Activation Detection by FPGA Implemented Kalman Filter
Muhammad Shahid Nazir,Muhammad Aqil,Ambreen Mustafa,Ameer Hamza Khan,Fatima Shams 제어로봇시스템학회 2015 제어로봇시스템학회 국제학술대회 논문집 Vol.2015 No.10
This paper presents an embedded system for real-time multi-channel brain activity detection by implementing the Kalman filter (KF) core on a field-programmable gate array (FPGA). The KF with a model driven approach is implemented on an FPGA, for the first time as per our knowledge. The model driven based brain activation model and its parameters" estimation methodology by KF is depicted from Aqil et al., 2012 (Detection of event-related hemodynamic response to neuroactivation by dynamic modeling of brain activity). The multiple instantiations of the KF core along with the coding of necessary compatibilities amongst the KF cores and with a single communication core, allow the parallel processing of multiple measurement channels. Through a serial universal asynchronous receiver/transmitter core, the fNIRS data is communicated to the system where it is being concurrently processed in 32-bit single precision IEEE754 format. The proposed fNIRS-KF embedded system is verified by an fNIRS dataset in real-time.
Nazir, Ghazanfar,Rehman, Malik Abdul,Khan, Muhammad Farooq,Dastgeer, Ghulam,Aftab, Sikandar,Afzal, Amir Muhammad,Seo, Yongho,Eom, Jonghwa American Chemical Society 2018 ACS APPLIED MATERIALS & INTERFACES Vol.10 No.38
<P>As one of the newly discovered transition-metal dichalcogenides (TMDs), rhenium disulfide (ReS<SUB>2</SUB>) has been investigated mostly because of its unique characteristics such as the direct band gap nature even in bulk form, which is not prominent in other TMDs (e.g., MoS<SUB>2</SUB>, WSe<SUB>2</SUB>, etc.). However, this material possesses a low mobility and an on/off ratio, which restrict its usage in high-speed and fast switching applications. Low mobilities or on/off ratios can also be caused by substrate scattering as well as environmental effects. In this study, we used few-layer ReS<SUB>2</SUB> (FL-ReS<SUB>2</SUB>) as a channel material to investigate the substrate-dependent mobility, current on/off ratio, Schottky barrier height (SBH), and trap density of states of different dielectric substrates. The hexagonal boron nitride (h-BN)/FL-ReS<SUB>2</SUB>/h-BN structure was observed to exhibit a high mobility of 45 cm<SUP>2</SUP> V<SUP>-1</SUP> s<SUP>-1</SUP>, current on/off ratio of about 10<SUP>7</SUP>, the lowest SBH of about 12 mV at a zero back-gate voltage (<I>V</I><SUB>bg</SUB>), and a low trap density of states of about 5 × 10<SUP>13</SUP> cm<SUP>-3</SUP>. These quantities are reasonably superior compared to the FL-ReS<SUB>2</SUB> devices on SiO<SUB>2</SUB> substrates. We also observed a nearly 5-fold improvement in the photoresponsivity and external quantum efficiency values for the FL-ReS<SUB>2</SUB> devices on h-BN substrates. We believe that the photonic characteristics of TMDs can be improved by using h-BN as the substrate and capping layer.</P> [FIG OMISSION]</BR>
Muhammad Shoaib Bhutta,Tang Xuebang,Shakeel Akram,Chen Yidong,Xiancheng Ren,Muhammad Fasehullah,Ghulam Rasool,Muhammad Tariq Nazir 한국공업화학회 2022 Journal of Industrial and Engineering Chemistry Vol.114 No.-
Graphene and its oxides are the most extensively studied, fascinating 2-dimensional Sp2 carbon hybridizedmaterials. Due to its superior and excellent thermal conductivity, it is considered to be a practicalsolution for the thermal dissipation of electric machines electronic components. Furthermore, grapheneoxide invariably reduces electrical insulation capability, which is inappropriate for electrical machinesrequiring low electrical and high thermal conductivity. Therefore, we have created 2D-3D hybrid grapheneoxide (GO)-diamond (DM) micro-composite polyimide (PI) films for high temperature and electricallyinsulated environments of electric machines such as motors and generators. With a modest fillingcharge of 10 wt% GO with 10% diamond (DM), the maximum thermal conductivity of 1.83 Wm-1K1 isachieved for polyimide micro composite and is almost 11 times higher than that of pristine PI films. The 10% PI/GO/DM micro composite films also show lower electrical conductivity than other samples. Hybrid fillers with high thermal and low electrical conductivities are responsible for synergistic improvementsin experimental results.
Muhammad Nazir Tahir,정다함,김환희,Jae-Hyuk Yu,조은애,정선호 대한화학회 2014 Bulletin of the Korean Chemical Society Vol.35 No.1
Glass discs functionalized with alkynyl (GDA) terminated monolayers were prepared and incubated in AgNO 3 solution (GDA-Ag). The modified functional glass surfaces were characterized by X-ray photoelectron microscopy (XPS). The potential of GDA and GDA-Ag as antimicrobial surfaces was investigated. Anti- microbial efficacies of GDA against Escherichia coli, Pseudomonas aeruginosa, Staphylococcus aureus, Bacillus cereus, and Candida albicans was relatively low ranging from 4.67 to 17.00%. However, the GDA- Ag was very effective and its antimicrobial efficacy ranged from 99.90 to 99.99% against the same set of microbial strains except for C. albicans where it was 95.50%. The durability of the Ag bonded to the terminal alkynyl groups was studied by placing the GDA-Ag in PBS buffer solution (pH 7.4) for two weeks. Initially, the silver release was relatively fast, with 40.05 ppb of silver released in first 24 h followed by a very slow and constant release. To study the potential of GDA-Ag for medical applications, in vitro cytotoxicity of GDA-Ag against Human Embryonic Kidney 293 (HEK293) cell lines was studied using WST-assay. The cytotoxicity of the GDA-Ag was very low (5%) and was almost comparable to the control (blank glass disc) indicating that GDA-Ag has a promising potential for medical applications.