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Johannes Steinmetz,이현정,Soyoung Kwon,이동수,Christophe Goze-Bac,Edy Abou-Hamad,김화용,박영우 한국물리학회 2007 Current Applied Physics Vol.7 No.1
critical carbon dioxide to ll the nanotubes with toluene and then add the ZieglerNatta catalyst. In order to assure controlled polymer-ization inside the nanotube, the catalyst outside is removed before the reaction. The resulting polyacetylene lled nanotubes arecharacterized by1H NMR and scanning electron microscope.
Polymerization of conducting polymers inside carbon nanotubes
Steinmetz, Johannes,Kwon, Soyoung,Lee, Hyun-Jung,Abou-Hamad, Edy,Almairac, Robert,Goze-Bac, Christophe,Kim, Hwayong,Park, Yung-Woo Elsevier 2006 Chemical physics letters Vol.431 No.1
<P><B>Graphical abstract</B></P><P>Supercritical carbon dioxide impregnation is used to prepare carbon nanotubes filled with pyrrole and <I>N</I>-vinyl carbazole. After the impregnation, the monomers were polymerized inside the nanotubes. The samples are characterized by HRTEM and <SUP>1</SUP>H NMR.</P><ce:figure id='figure.0010'></ce:figure> <P><B>Abstract</B></P><P>Supercritical carbon dioxide is an universal tool to impregnate carbon nanotubes with a wide range of organic molecules. In this Letter, we present our results of carbon nanotubes filled with the photo-conducting polymer poly(<I>N</I>-vinyl carbazole) and the conducting polymer polypyrrole which were prepared by polymerizing the monomers inside the nanotubes. The endohedral nanotubes were characterized by HRTEM and <SUP>1</SUP>H NMR which confirmed that the encapsulated material was indeed the conducting polymer.</P>