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고로슬라그의 이용에 관한 연구 (II) (천연원료를 이용한 Slag-Ceramics)
지응업,이전,한기석,이재락,Chi, Ung-Up,Rhee, Jhun,Han, Ki-Suk,Lee, Jae-Rock 한국세라믹학회 1981 한국세라믹학회지 Vol.18 No.1
A glass-ceramics based on blast-furnace slag, with some additives to the theoretical composition in order to control properties of mother glass and the heat treatment conditions, has been investigated. The raw materials in this study were blast-furnace slag, serpentine, feldspar and quartz as mother glass ingredients. Titanium dioxide and chromite were used as the nucleating agents. Batch compositions of the prepared glasses and ceraming conditions were found by trial and error method. The optimum conditions were confirmed by analyzing several measured physical properties such as density change during heat treatment, microhardness of slag-ceramics prepared, viscosity change of glass at heat treatment temperatures, nucleation density change, dilatometric properties, differential thermal analysis, identification of the grown crystal and crystal sizes. The batch composition feasible to prepare slag-ceramics was 40% of blast-furnace slag, 25% of serpentine, 18% of feldspar and 17% of silica sand. Three percent titanium dioxide and 1% chromite of the mother glass were added as nucleating agents. The ceraming conditions under which the slag-ceramics having considerably good properties can be developed found as: "The glass was heated at 75$0^{\circ}C$ for 2 hours for nucleation, and the temperature was raised up to 1, 00$0^{\circ}C$ with a rate of 0.75$^{\circ}C$/min for crystal growth.owth.
지응업,이경재 한국세라믹학회 1976 한국세라믹학회지 Vol.13 No.3
The corelation between surface tensions and surface appearances of SK O5a opaque glazes for earthen wares were investigated. The surface tension values were theoretically calculated by using Dietzel's factors of constituent oxides of glaze. The surface appearances of glazes, especially the pinhole phenomena were strongly effected by the surface tension values showing the following general tendencies: (1) In the range of 305±3 dynes/cm of surface tensions, glazes showed almost no pjnholes. (2) In the range of surface tensions less than 300 dynes/cm, the large numbers of small pinholes or eggshell textures were observed. (3) In the range of surface tensions higher than 310 dynes/cm, large and deep pinholes were observed. (4) The contact angles of glazes on the wall tile body substrate are in the good proportional agreement with the surface tension values calculated by Dietzel's factors.
지응업,최상욱,김광호 한국세라믹학회 1975 한국세라믹학회지 Vol.12 No.4
In order to obtain the superior refractory setter having better spalling resistance, cordierite was synthesized from domestic raw materials. Raw mixtures were fired between 125$0^{\circ}C$ and 140$0^{\circ}C$, and qualitative determination of crytallization was investigated by x-ray diffraction analysis. The results obtained are as follows; 1) The optimum batch composition of synthesized cordierite is 80.5% of Hadong kaolin (pink), 14% of Kyulsung tromolite talc and 5.5% of magnesia clinker, and the firing temperature is 1375$^{\circ}C$. 2) The composition of the refractory setter which exhibits the best values for the thermal properties is 40% of synthesized cordierite, 30% of kaolin chamotte(contains more than 60% of mullite), and 30% of Japanese clay. 3) The optimum particle size distribution of ternary mixture consists of 50% of coarse articles (3.327-1.168mm), 25% of intermediate particles (1.168-0.208mm) and 25% of fine particles (0.208-0.000mm).
Tundish용 Zircon 내화물의 제조에 관한 연구
지응업,최상욱 한국세라믹학회 1977 한국세라믹학회지 Vol.14 No.2
Zircon sand of two different particle distribution with 2 percent of ground pyrophyllite were adoted to prepare the dense specimens of the stopper nozzle for the tundish. The molding pressure of $600kg/cm^2$ brought about the superior properties to those obtained t the pressure of $300kg/cm^2$, and as the firing temperatures were increased from $1, 350^{\circ}C$ to $1, 600^{\circ}C$, the better characteristics resulted. The addition of 2 percent $MgCr_2O_4$ to zircon pyrophyllite batch was more effective in corrosion-resistance to the blast furnace-slag.
지응업,최상흘,이응상,상기남,Chi, Ung-Up,Choi, Sang-Eul,Lee, Ung-Sang,Sang, Ki-Nam 대한화학회 1964 대한화학회지 Vol.8 No.4
現在 國內에서 使用되고 있는 主要 窯業原料들에 對한 基礎的 data가 不足하므로 이에 國內 主要 窯業工場의 使用量을 基準으로 하여 約 40 種의 鑛物을 試料로 設定하고 그 基礎的 硏究를 하였다. 設定된 試料에 對하여 化學分析, D.T.A.試險, X-ray 廻折試險 및 粒度分析試驗을 行하고 그 結果 및 解析의 一部를 第 1報로서 發表한다. 모든 試料鑛物은 그 試驗結果를 結晶構造的 見地에서 鑛物學的으로 다루어 解析되었는데 特히 本 硏究의 結果 河東白土는 halloysite 라는 設$^{29}$과 一致하였으며 또한 國內 蠟石은 그 主成分 鑛物이 pyrophyllite 質, kaolin 質 및 muscovite 質의 3 者로 分類되어야 한다는 것이 밝혀졌다. 또한 本 第 1報에서 다루지 못한 詩料들, 疑問으로 남은 點들, 電子顯微鏡寫眞 및 光學的 試驗結果는 次報에서 다루기로 한다. Various ceramic raw minerals occuring in Korea were investigated laying emphasis on mineralogical identifications of them. Data of chemical analysis, differential thermal analysis, powder patterns of x-ray diffraction and particle size distribution were obtained for the present study. Hadong kaolin was confirmed as halloysite, and it was found that main constituent of some commercial pyrophyllite is mineralogically not pyrophyllite; Seongsan and Ockmaesan pyrophyllite consist of mainly kaolin group mineral, Tongnae pyrophyllite consists of muscovite, however Milyang and Jindo pyrophyllite is mineralogically pyrophyllite.