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Jute/PP 복합 재료의 제조와 이에 따른 기계적 물성 향상 및 계면 성분 분석
이진우(Jin W. Yi),황병선(Byung S. Hwang),이정훈(Jung H. Lee),나창운(Chang W. Nah) 대한기계학회 2006 대한기계학회 춘추학술대회 Vol.2006 No.6
Thermoplastic PP (Polypropylene) composites reinforced with natural fiber, jute, were prepared through the environment-friendly process. In order to effectively improve interfacial adhesion strength between polypropylene (PP) and jute fiber, we particularly incorporated maleic anhydride grafted PP (MAPP) into the matrix through the environment-friendly process without an additional method of process and had better mechanical performances by providing the alignment into the natural fiber than those of the conventional fabrication technology such as an extrusion or injection molding. We also proposed hot pressing method which applied relatively low shear to the composites and confirmed the chemical bonds among the functional groups of MAPP and jute using FT-IR approach. The concentration of MAPP for maximum tensile strength and modulus was optimized at 3 wt%. Flexural properties had no noticeable tendency to increase with MAPP contents compared to tensile strength, which could probably be explained by the degree in wetting of PP/MAPP matrix.
Production of zoogloea gum by Zoogloea ramigera with glucose analogs
Lee, Jin W.,Yeomans, Walter G.,Allen, Alfred L.,Gross, Richard A.,Kaplan, David L. 東亞大學校附設遺傳工學硏究所 1998 遺傳工學硏究 Vol.- No.5
Zoolgans with altered sugar composition were synthesized by Zoogloea ramigera by varying the glucose concentration and initial medium pH. The relative mol% of the sugar components, glucose and galactose, in the exopolymer made with 2% (w/v) glucose as the carbon source was 66 and 34%, respectively. By varying the glucose concentration and initial medium pH, the mol% ratios of glucose to galactose in zooglan ranged from 70:30 to 58:42. Also, glucose analogs, 3-O-methyl-D-glucose, 2-amino-2-deoxy-D-glucose, and 2-acetamido-2-deoxy-D-glucose, were used as a co-substrate with glucose to produce to produce modified zooglans. The mol% ratios of glucose to galactose in exopolymers produced by co-feeding glucose analogs ranged from 70:30 to 9:91.
Compositional consistancy of a heteropolysaccharide-7 produced by Beijerinckia indica
Lee, Jin W.,Yeomans, Walter G.,Allen, Alfred L.,Gross, Richard A.,Kaplan, David L. 東亞大學校附設遺傳工學硏究所 1998 遺傳工學硏究 Vol.- No.5
The component sugars of heteropolysaccharide-7(PS-7) produced by Beijerinckia indica were rhamnose and glucose (1.0:4.8,mol:mol) by gas chromatographic analysis. Galacturonic acid, previously reported as a repeat unit of PS-7, was not found in purified PS-7. The yield of PS-7 varied with physiological conditions, such as concentration of carbon source and initial pH of medium, but the molar ratio of rhamnose to glucose stayed within 1.0 to 4.6-5.1. B indica utilized glucose and some glucose analogs as carbon sources and produced exopolymers, although there was no direct incorporation of these sugars into PS-7. The molar ratio of rhamnose to glucose in each polymer synthesized from glucose-related sugars showed no significant variation(1.0 to 4.5-4.7).
Lee, Jin W.,Allen, Alfred L.,Deng, Flank,Yeomans, Walter G.,Kaplan, David L.,Gross, Richard A. 東亞大學校附設遺傳工學硏究所 1998 遺傳工學硏究 Vol.- No.5
Three different exopolymers were purified from cultures of Agrobacterium sp. strain ATCC 31749 grown in a mineral salts medium containing 2% glucose at 30℃ for 5 days under aerobic culture conditions. These exopolymers were curdlan (extracellular, homo-B-(1-3)-gulcan.water insoluble at neutral pH), a water-soluble noncurdlan-type exopolymer A (WSNCE-A), and a water-soluble noncurdlan-type exopolymer B (WSNCE-B). Curdlan. WSNCE-A. and WSNCE-B composed by weight 61,27,and 12%,respectively, of the exopolymer produced from goucose. Compositions of all polymers were confirmed by gas chromatography (GC) and gas chromatography -mass spectrometry(GC-MS). The WSNCE-A is composed of glucose and galactose with lower contents of rhamnose. The WSNCE-B consists of glucose and mannose. To biosynthesize modified biopolymers, glucose-related sugars including 3-0-methyl-D-glucose, 2-amino-2-deoxy-D-glucose, and 2-acetamido-2-deoxy-D-glucose(N-acetylgucosamine)were fed separately as the sole carbon source. Using 3-O-methyl-D-glucose, 8-12 mol% of the curdlan repeats were 3-O-methyl-D-glucose based on GC and H-nuclear magnetic resonance spectrometry. N-Acetylgucosamine was incorporated into WSNCE-A at 10 mol% based on the GC-MS but was not found in curdlan or WSNCE-B. Trois exopolymeres differents ont ete purifies a partir de cultures d'Agrobacterium sp. souche ATCC 31749, dont la croissance s'est effectuee a 30℃ durant 5 jours sur un milieu contenant des sels mineraux et 2% de glucose dans des conditions aerobies. Ces trois exopolymeres se sontreveles etre:un type coagule(curdlan) extracellulaire. insoluble dans 1'eau a pH neutre et constitue d'homo-B-(1-3)-glucane, et deux types solubles, non coagules, soit 1'exopolymere A (WSNCE-A) et 1'exopolyere B(WSNCE-B). Les poids respectifs du type coagule esdes deux types noncoagules A et B ont represente 61,27 et 12% de 1'exopolymere produit a partir du glucose. La composition de chacun des polymeres a ete identifiee par chromatographie en phase gazeuse(GC) et par chromatographie en phage gazeuse-spectrometrie de masse (GC-MS). Le WSNCE-A s'est revele constitue de glucose et de galactose avec faible teneur en rhamnose, et lw WSNCE-B, de glucose et de mannose. Dans le but de biosynthetiser des biopolymeres modifies, des sucres apparentes au glucose ont ete incorpores separement aux milieux de culture comme seule source de carbone:le 3-O-methyl-D-glucose, le 2-amino-2-desoxy-D-glucose, et le 2-acetamido-2-desoxy-D-glucose(N-acetylgulcosamine). Utilisant le 3-O-methyl-D-glucose, 8-12 mol% des repetitions du type coagule ont ete du 3-O-methyl-D-glucose, d'apres la GC et la spectrometrie de resonnance magnetique nucleaire-'H. La N-acetylglucosamine a ete incorporee dans le WSNCE-A a 10 mol% d'apres les GC-MS, mails il n'a pas ete trouve chez les exopolymeres coagules ou le WSNCE-B.
Lee, Jin W.,Yeomans, Walter G.,Allen, Alfred L.,Gross, Richard A.,Kaplan, David L. 東亞大學校附設遺傳工學硏究所 1998 遺傳工學硏究 Vol.- No.5
The cell growth, production of exopolymers, and the molar ratio of glucose to mannose in the water-soluble non curdlan type exopolymer-B (WSNCE-B), which is one of three exopolymers purified from the culture of Agrobacterium sp. varied with carbon source, culture medium, and initial medium pH. The molar percentage of rhamnose, a ninor component in WSNCE-B, varied up to 13%, dependent on physiological condition. No rhamnose was found in the WSNCE-B purified from the culture with initial medium pH>6.8. The relative amount of mannose in WSNCE-B increased regularly with the amount of yeast extract added to the mineral salts medium. The relative amounts of glucose, mannose, and rhamnose in the WSNCE-B can be controlled by varying culture conditions.