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Synthesis of Nano Titanium Dioxide and Its Application in Photocatalysis
Truong Van Chuong,Le Quang Tien Dung,Dinh Quang Khieu 한국물리학회 2008 THE JOURNAL OF THE KOREAN PHYSICAL SOCIETY Vol.52 No.5
This paper presents a simple way to synthesize titaniumdioxide nanotubes by using a microwave- assisted reaction of TiO2 particles and NaOH solution. The main advantage of the introduction of microwave into the reaction system is the extremely rapid kinetics for synthesis. This method is simple and easy to reproduce. Structural and microstructural characterizations of titania nanotubes were accomplished using X-ray diffraction (XRD), scanning-electron microscopy (SEM) and transmission-electron microscopy (TEM) techniques. The specific surface area was calculated using the Brunauer-Emmett-Teller model and was found to be 52 m2/g. A high photocatalysis of our TiO2 nanotubes was obtained. This paper presents a simple way to synthesize titaniumdioxide nanotubes by using a microwave- assisted reaction of TiO2 particles and NaOH solution. The main advantage of the introduction of microwave into the reaction system is the extremely rapid kinetics for synthesis. This method is simple and easy to reproduce. Structural and microstructural characterizations of titania nanotubes were accomplished using X-ray diffraction (XRD), scanning-electron microscopy (SEM) and transmission-electron microscopy (TEM) techniques. The specific surface area was calculated using the Brunauer-Emmett-Teller model and was found to be 52 m2/g. A high photocatalysis of our TiO2 nanotubes was obtained.
Relaxor characteristics of PSLZT-BMT-based ferroelectric material ceramics
Nguyen Van Thinh,Le Dai Vuong,Do Viet On,Truong Van Chuong,Le Vu Truong Son,Trinh Ngoc Dat,Le Van Thanh Son,Vo Thanh Tung 한양대학교 청정에너지연구소 2023 Journal of Ceramic Processing Research Vol.24 No.3
(1-x)[(Pb0.94Sr0.05La0.01)(Zr0.54Ti0.46)0.9975O3]-x[Bi(Mn1/2Ti1/2)O3] (PSLZT-BMT) ferroelectric material ceramics with x in therange of 0-0.05 mol were successfully synthesized following the conventional solid-phase route. The materials were thoroughlyinvestigated to study their structural phase, microstructure, ferro-piezoelectric characteristics, and dielectric behavior. Theexperimental results show that the density of the samples decreased from 7.75 to 7.58 g/cm3, and the relative density decreasedin the range of 98.48%-96.28%. However, with increasing contents of BMT, the dielectric and ferroelectric properties ofPSLZT-BMT ceramics tend to decrease, specifically the maximum dielectric constant (εmax) of PSLZT-BMT decreased in therange of 23579-9991 and the residual polarization (Pr) decreases in the range of 22.54-7.87 μC/cm2 when the doping contentincreased in the range of 0.0-0.05 mol. The diffusivity values (γ) of the PSLZT-BMT material are 1.74, 1.78, 1.82, 1.84, 1.79,and 1.77 when the doping content x varies as 0.0, 0.01, 0.02, 0.03, 0.04, and 0.05 mol, respectively, which is characteristic ofrelaxor ferroelectric materials. Besides, the Tm, TB, TC-W, and C values depend on BMT concentration, and the trend decreases.