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Removal of chloride ions from acidic solution with antimony oxides
Xuewen Wang,Yanping Du,Haoxiang Yang,Shenghui Tian,Qi Ge,Sheng Huang,Mingyu Wang 한국공업화학회 2021 Journal of Industrial and Engineering Chemistry Vol.93 No.-
This studyaims to investigate the removal of Cl- from acidic solutionwith antimony oxides. The effects of theadsorbenttype,reaction time,reaction temperature,Sb/Clmole ratio andacidityonadsorptionperformanceand the regeneration of loaded adsorbent were systematically studied. The results shows that Sb2O3 xH2Ohas the highest adsorption rate (97.64%) among Sb2O3 xH2O, Sb2O5 xH2O, Sb2O4 xH2O and Sb2O3 in thesolution containing 1.25 mol/L H2SO4under the condition of Sb/Cl mole ratio 3:1 and stirring for 2 h at roomtemperature, and the concentration of Cl- in the acid solution can be reduced to 280 mg/L. Then the residualSb in the adsorbed solution can be decreased from 48.21 mg/L to 16.09 mg/L by C-SbA which is made bySb2O5 xH2O. The C-SbA which has been used can be reused after calcining at 400 ℃ for 2 h. The loadedadsorbent was completely regenerated by adding it into NaOH or Na2CO3 solution whose pH is equal ormore than 9.5 according to S/L ratio 1:6 g/mL and was stirred for 0.5 h at room temperature. The Cl- in theregenerated solution was crystallized and precipitated in the form of NaCl without evaporation andconcentration according to the common ion effect of Na+, and the purity of NaCl was more than 99%.
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