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Bien Dong Che,Le-Thu T. Nguyen,Bao Quoc Nguyen,Ha Tran Nguyen,Thang Van Le,Nieu Huu Nguyen 한국고분자학회 2014 Macromolecular Research Vol.22 No.11
Radar absorbing materials (RAMs) for practical applications are expected not only to have strong microwaveabsorption and a wide absorption bandwidth, but also to be lightweight, to have a fine thickness and acceptablestructural performance, as well as being cost-effective. Although the dispersion of carbon-nanofillers in polymermatrices is a key factor determining the microwave absorbing properties of the composites, there have few studieson these effects. To our knowledge, to date, the realization of pristine multi-walled carbon nanotube (MWCNT)/polymercomposites as RAMs in industrial production has been restricted, due to high CNT contents or large composite thicknesses. Thus, in this work, two MWCNT dispersion processing methods, a solution process with surfactant-aid anda ball-milling dispersion, were investigated to fabricate pristine MWCNT/epoxy nanocomposites. The effects of thedifferent dispersion processes, CNT loading, and composite thickness on CNT dispersion in the matrix, were observedby TEM, and the electrical conductivity and X-band absorbing performance of the composites were assessed. Theuse of an ionic surfactant to aid the dispersion of CNTs in solution resulted in the best RAMs, with a good compromiseamong effective X-band absorption, small composite thickness, and very low CNT content. The ball-millingmethod also resulted in materials with a low CNT content and microwave absorbing performance acceptable forindustrial applications. Moreover, it offers a very simple and efficient route suitable for low-cost, mass productionof RAMs. The results showed that by facile approaches of dispersing pristine commercial MWCNTs in an epoxyresin matrix, composites of only 2-3 mm thickness and as little as 0.25-0.5 wt% CNT loading could be obtained,with a relatively wide X-band operating bandwidth and maximum absorptions exceeding 18-25 dB.
Hoan Minh Tran,Tam Huu Nguyen,Viet Quoc Nguyen,Phuc Huynh Tran,Linh Duy Thai,Thuy Thu Truong,Le-Thu T. Nguyen,Ha Tran Nguyen 한국고분자학회 2019 Macromolecular Research Vol.27 No.1
The photoswitching poly(pyrene-1-ylmethyl-methacrylate-random-methyl methacrylate-random-methacrylate spirooxazine) was synthesized via atom transfer radical polymerization and characterized by proton nuclear magnetic resonance (1H NMR), gel permeation chromatography (GPC), Fourier transform infrared (FTIR) spectroscopy, UV-visible spectroscopy, and differential scanning calorimetry (DSC). The obtained copolymer exhibited the capability of erasable and rewritable photoimaging, making it a potential candidate for optical data storage materials. Moreover, the copolymer also showed the sensing ability for cyanide anions effect in aqueous solutions.
Anh Thi Le,Manh Ha Hoang,Minh Hoa Nguyen,T. Anh Thu Do,Minh Tan Man 한국진공학회(ASCT) 2020 Applied Science and Convergence Technology Vol.29 No.5
We present an analytical method to model the influence of gold nanoparticle (Au NP) concentration on the energy transfer between Cy3 orange beads (OBs) and Au NPs. The OBs and Au NPs act as donor (D) and acceptor (A), respectively. In the D–A system, the energy transfer efficiency strongly depends on the spectral overlap and separation R between donor and acceptor. Theoretical calculations for a range of R values between 10 and 100 Å produce three parameters that each characterize one of three different resonant energy transfer mechanisms: fluorescence resonant energy transfer, surface resonant energy transfer and Coulomb energy transfer. The values of these parameters provide estimates of the degree of quenching or enhancement of the fluorescence of D–A complexes as a function of concentration. A comparison between experimental and theoretical data confirms the validity of the model.
Nhung Thanh Thi Truong,Tam Huu Nguyen,Bao Kim Doan,Le-Thu T. Nguyen,Tam Hoang Luu,Chau Duc Tran,Thiet Quoc Nguyen,Ha Tran Nguyen 한국고분자학회 2021 Macromolecular Research Vol.29 No.11
In this research, three organic photocatalysts, 4-(4H-dithieno[3,2-b:2',3'- d]pyrrol-4-yl)-N,N-diphenylaniline, 4-(pyren-1-yl)-4H-dithieno[3,2-b:2',3'-d]pyrrole and 4-(6b,10-dihydroperylen-3-yl)-4H-dithieno[3,2-b:2',3'-d]pyrrole have been successfully synthesized through C-N coupling reactions. The chemical structures and the optical properties of the obtained organic photocatalysts have been characterized via 1H NMR,13C NMR, elemental analysis, and UV-Vis spectroscopy. Next, these dithieno[3,2-b:2′,3′-d]pyrrole-based photocatalysts have been used for the polymerization of methyl methacrylate, 2-(dimethylamino)ethyl methacrylate and tert-butyl methacrylate monomers under 365 nm UV irradiation, resulting in (meth)acrylate polymers with controlled molecular weights and low polydispersity indexes.
Hoan Minh Tran,Lan Ngoc Tan Phan,Thang Van Le,Thuy Thuy Truong,Tam Huu Nguyen,Khuong Tung Truong,Le-Thu T. Nguyen,Mai Thanh Phong,Ha Tran Nguyen 한국고분자학회 2019 폴리머 Vol.43 No.4
A novel organic photocatalyst, 4-(10H-phenothiazin-10-yl)-N,N-diphenylaniline (PDPA) has been successfully synthesized from triphenylamine and phenothiazine moiety via Buchwald-Hartwig C-N coupling. The chemical structure of catalyst was characterized via proton nuclear magnetic resonance (1H NMR) and the optical properties were investigated via UV-vis spectroscopy. The PDPA has been applied as an organic photocatalyst for metal free atom transfer radical polymerization (O-ATRP). The well-controlled molecular weights of polymethacrylates have been obtained with high yield of 95% and narrow polydispersity index (Đ).