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Yen H. Vo,Thanh V. Le,Hieu D. Nguyen,Tuong A. To,Hiep Q. Ha,Anh T. Nguyen,Anh N.Q. Phan,Nam T.S. Phan 한국공업화학회 2018 Journal of Industrial and Engineering Chemistry Vol.64 No.-
Zirconium-based metal-organic framework MOF-808 was synthesized, and sulfated with aqueous sulfuric acid. Sulfated MOF-808 was utilized as a recyclable heterogeneous catalyst for the synthesis of quinazolinones from β-ketoesters and benzamides, and for the synthesis of benzimidazoles from β-ketoesters and o-phenylenediamines in glycerol as a green solvent. The sulfated MOF-808 catalyst was more active than many heterogeneous and homogeneous catalysts. The combination of the sulfated MOF-808 and glycerol was also effective for the reaction of o-aminothiophenols with β-diketones or cyclic β-diketones to produce benzothiazoles. To our best knowledge, MOF-based catalysts were not previously utilized as heterogeneous catalyst in glycerol as green solvent.