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- 저자 : Baykal A. (검색결과 4 건)
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M. A. Almessiere,Y. Slimani,A.V. Trukhanov,A. Baykal,H. Gungunes,E.L. Trukhanova,S.V. Trukhanov,V.G. Kostishin 한국공업화학회 2020 Journal of Industrial and Engineering Chemistry Vol.90 No.-
The dysprosium ions (Dy3+)-substituted nanosized ferrites (NFs) of composition [Ni0.5Co0.5](DyxFe2-x)O4(x0.08) were prepared using the citrate gel process. To analyse the magnetic properties of the samples,the Mössbauer spectroscopy methods and vibrating sample magnetometry (VSM) were applied. Theroom temperature Mössbauer spectra werefitted to determine the hyperfine parameters of the proposedNFs. The preferential occupation of the octahedral B sites by the Dy3+ in the spinel ferrite sublattice wasconfirmed from the cations distribution. The hyperfine magneticfield of both sublattice decreasedwhereas the increase in the Dy3+ substitution was observed. The S-parameters of the prepared NFs in thehigh frequency range were measured by the co-axial method. In addition, the MW reflection losses wereevaluated by means of the frequency-dependent (in the range of 1–20 GHz) complex permittivity andpermeability spectra. All the NFs indicated that the absorption of the electromagnetic radiation wasranging between 2.9–5.5 GHz due to the natural ferromagnetic resonance. A correlation amongst the Dy3+ concentration, microstructure, magnetic and microwave (MW) characteristics of these NFs wasestablished. It’s been asserted that by controlling the Dy3+ contents carefully, the MW absorption andmagnetic attributes of the proposed spinel NFs can be tailored.
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B. Unal,M. Senel,A. Baykal,H. Sözeri 한국물리학회 2013 Current Applied Physics Vol.13 No.7
Functionalized multiwall carbon nanotubes (MWCNT-COOH) were decorated with crystalline cobalt ferrite nanoparticles (CoFe2O4 NPs) by co-precipitation reaction to form MWCNT-COOH/CoFe2O4 hybrid. The hybrid was characterized by X-ray diffraction analysis, transmission electron microscopy (TEM),Fourier transfom infrared spectroscopy and vibrating sample magnetometry. The results confirmed that MWCNTs and CoFe2O4 NPs coexisted in the hybrid. The TEM results showed a thick layer of CoFe2O4 was intimately connected to the surface of MWCNTs. The saturation magnetization value of the hybrid was 11.5 emu/g. There has been a high frequency fluctuation in conductivity, however, above all dc conductivity changes and resulting activation energy is calculated from the Arrhenius plots. It is found to vary with the temperature regions. This can be attributed to the existence of a conventional temperature independent tunneling conduction mechanism, which can be also explained that the metallic conduction is a dominant mechanism around room temperature. The ac conductivity of MWCNT-COOH/CoFe2O4hybrid might also be a consequence of the predictions of the universal dynamic response and the ‘n’power exponents could be determined with lower concentration of the addition in the hybrids.
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Hannachi E.,Slimani Y.,Almessiere M.A.,Alotaibi S.A.,Omelchenko L.V.,Petrenko E.V.,Kurbanov U.,Ben Azzouz F.,Solovjov A.L.,Baykal A. 한국물리학회 2023 Current Applied Physics Vol.48 No.-
We report the effect of the addition of BaTiO3 and WO3 nanoparticles on the pseudogap and excess conductivity of YBCO polycrystal. The excess conductivity analysis showed that the experimental data of pure and sample added with low amount of WO3 and BaTiO3 were perfectly described by the 2D Maki-Thompson (MT) and 3D Aslamazov-Larkin (AL) models. A sharp decrease in excess conductivity was obtained for samples added with high amount of nanoparticles where the analysis indicated the presence of the AL contribution and Lawrence- Doniach (LD) models. The pseudogap (PG) results showed that the value of Tpair (the temperature at which local pairs are transformed from strongly bound bosons into the fluctuating Cooper pairs) increased from around 117 K for the pure sample to around 187 K for sample co-added with low amount of nanoparticles. The pseudogap Δ*(TG) reduced from 230.9 K (for pure sample) to 223.4 K (for added sample).
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Rapid color degradation of organic dyes by Fe3O4@His@Ag recyclable magnetic nanocatalyst
Md. Amir,U. Kurtan,A. Baykal 한국공업화학회 2015 Journal of Industrial and Engineering Chemistry Vol.27 No.-
In this study, we reported the degradation of organic dyes (methyl orange, MO and methylene blue, MB)by Fe3O4@His@Ag MRC in which histidine was used as linker. The size of crystallite of MRC wascalculated as 19 nm. The M–H hysteresis loop of the product indicates that it exhibits superparamagneticproperty at room temperature. Catalytic studies showed that this product could catalyze the degradationof MO and MB in a reasonable time. Moreover, the product can be recycled five times by magneticseparation without major loss of its activity. Thus, Fe3O4@His@Ag MRC can be served as an effective andconvenient recyclable nanocatalyst for azo dye degradation and hence as an environmental protectionapplication too.
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