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Boo, Bong Hyun,Kang, Heun Kag,Kang, Sung Kwon,Lee, Sun Sook,Kim, Dongho,Lee, Myung Ho 충남대학교 기초과학연구소 1992 연구논문집 Vol.12 No.-
The title compounds were synthesized and characterized. The vibrational frequencies of (Me_3Si)_3SiX (X=H, Cl, OH, OD, Me, OMe, SiMe_3) were determined by means of IR and Raman spectroscopy. Based on our AM1 semiempirical calculation and the literature group frequencies of CH_3, Me_3Si, SiSi_3, SiX (X=H, Cl, OH, OD, CH_3, OCH_3) have been assigned. The intensities of the Raman lines of the stretching vibrations of (Me_3Si)_3Si-X (X=Cl, OH, OMe) and (Me_3Si)_3SiO-H are very low compared with those of the IR lines. This indicates that the bonds have a strong ionic nature.