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        Influence of Iron Doping on Structural, Optical and Magnetic Properties of TiO2 Nanoparticles

        R. Zahid,M. Manzoor,A. Rafi q,M. Ikram,M. Nafees,A. R. Butt,S. G. Hussain,S. Ali 대한금속·재료학회 2018 ELECTRONIC MATERIALS LETTERS Vol.14 No.5

        In this study, various concentrations of Fe doped TiO2nanoparticles have been successfully synthesized using the sol–gelmethod. A variety of characterization techniques as ultra-violet visible (UV–Vis) spectroscopy, X-ray diffractometer (XRD),vibrating sample magnetometry (VSM) and field emission scanning electron microscopy (FESEM) were employed to analyzethe prepared nanopowders. XRD measurement confirmed the substitution of Fe ion without disturbing the tetragonal crystalsystem of TiO2. The crystallite size was found to decrease and lattice strain increases upon doping estimated by WilliamsonHall plot. Furthermore, the average grain size calculated by FESEM found was between 10 and 30 nm for pure and dopedTiO2. UV–Vis spectroscopy showed an increase in absorption accompanied red shift and increase in band gap energies from3.36 to 3.62 eV with the addition of Fe. The FTIR spectroscopy was employed to confirm the presence of functional groupsin the fabricated nanopowders. Upon mixing the saturation magnetization (Ms) varying from (2.12 to 1.51)10−2 emu/g wasobserved.

      • Reinforced fibrous recycled aggregate concrete element subjected to uniaxial tensile loading

        Hameed, R.,Hasnain, K.,Riaz, M. Rizwan,Khan, Qasim S.,Siddiqi, Zahid A. Techno-Press 2020 Advances in concrete construction Vol.9 No.2

        In this study, effect of recycled aggregates and polypropylene fibers on the response of conventionally reinforced concrete element subjected to tensile loading in terms of tension stiffening and strain development was experimentally investigated. For this purpose, concrete prisms of 100 × 100 mm cross section and 500 mm length having one central deformed steel re-bar were cast using fibrous and non-fibrous Recycled Aggregate Concrete (RAC) with varying percentages of recycled aggregates (0%, 25%, 50%, 75% and 100%) and tested under uniaxial tensile load. For all fibrous RAC mixes, polypropylene fibers were used at constant dosage of 3.15 kg/㎥. Effect of recycled aggregates and fibers on the compressive strength of concrete was also explored in this study. Through studying tensile load versus global axial deformation of composite and strain development in concrete and steel, it was found that replacement of natural aggregates with recycled aggregates in concrete negatively affected the cracking load, tension stiffening and strain development, and this negative effect was observed to be increased with increasing contents of recycled aggregates in concrete. The results of this study showed that it was possible to minimize the negative effect of recycled aggregates in concrete by the addition of polypropylene fibers. Reinforced concrete element constructed using concrete containing 50% recycled aggregates and polypropylene fibers exhibited cracking behavior, tension stiffening and strain development response almost similar to that of concrete element constructed using natural aggregate concrete without fiber.

      • KCI등재

        Central line-associated bloodstream infections in the intensive care unit: importance of the care bundle

        Aynur Atilla,Zahide Doğanay,Hale Kefeli Çelik,Leman Tomak,Özgür Günal,S. Sırrı Kılıç 대한마취통증의학회 2016 Korean Journal of Anesthesiology Vol.69 No.6

        Background: The importance and efficacy of a care bundle for preventing central line-associated bloodstream infections (CLABSIs) and infectious complications related to placing a central venous catheter (CVC) in patients in the intensive care unit (ICU). Methods: A care bundle was implemented from July 2013 to June 2014 in a medical ICU and surgical ICU. Data were divided into three periods: the prior period (July 2012–June 2013), the intervention period (July 2013–June 2014; first and second periods), and the post-intervention period (July 2014–December 2014; third period). A care bundle consisting of optimal hand hygiene, skin antisepsis with chlorhexidine (2%) allowing the skin to dry, maximal barrier precautions for inserting a catheter (sterile gloves, gown, mask, and drapes), choice of optimal insertion site, prompt catheter removal, and daily evaluation of the need for the CVC was introduced. Results: The catheterization duration was longer and femoral access was more frequently observed in patients with CLABSIs. CLABSI rates decreased with use of the care bundle. The CLABSI rate in the medical ICU was 6.20/1,000 catheter days during the prior period, 3.88/1,000 catheter days during the intervention period, and 1.05/1,000 catheter days during the third period. The CLABSI rate in the surgical ICU was 8.27/1,000, 4.60/1,000, and 3.73/1,000 catheter days during these three periods, respectively. Conclusions: The choice of an optimal catheter insertion site, use of all barrier precautions, and removal of catheters when they are no longer needed are essential to decrease the CLABSI rate.

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        Dynamic speckle illumination wide-field reflection phase microscopy

        Choi, Youngwoon,Hosseini, Poorya,Choi, Wonshik,Dasari, Ramachandra R.,So, Peter T. C.,Yaqoob, Zahid The Optical Society 2014 Optics letters Vol.39 No.20

        <P>We demonstrate a quantitative reflection-phase microscope based on time-varying speckle-field illumination. Due to the short spatial coherence length of the speckle field, the proposed imaging system features superior lateral resolution, 520 nm, as well as high-depth selectivity, 1.03 관m. Off-axis interferometric detection enables wide-field and single-shot imaging appropriate for high-speed measurements. In addition, the measured phase sensitivity of this method, which is the smallest measurable axial motion, is more than 40 times higher than that available using a transmission system. We demonstrate the utility of our method by successfully distinguishing the motion of the top surface from that of the bottom in red blood cells. The proposed method will be useful for studying membrane dynamics in complex eukaryotic cells.</P>

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