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Synthesis, structure and tribological performance of tungsten disulphide nanocomposites
Si, Ping-Zhan,Choi, Chul-Jin,Lee, Jae-Wook,Geng, Dian-Yu,Zhang, Zhi-Dong Elsevier Sequoia 2007 Materials science & engineering Structural materia Vol.443 No.1-2
<P><B>Abstract</B></P><P>Tungsten disulphide nanocomposites were prepared in large scale by employing the direct reaction between tungsten nanoparticles and sulphur powders. The nanocomposites include a variety of shapes such as isolated WS<SUB>2</SUB> multi-layered sheets, WS<SUB>2</SUB>-coated WO<SUB>3</SUB> nanoparticles, and enclosed fullerene-like WS<SUB>2</SUB> structures. Pin-on-disc wear tests indicate that the addition of a small amount (5wt%) of these nanoparticles to paraffin decreases significantly the wear loss of the pin. Additives of these WS<SUB>2</SUB>/WO<SUB>3</SUB> nanoparticles possess much better tribological performance than micrometer-sized WS<SUB>2</SUB> powders additives do. The surface topography of wear scar of the pins after wear tests with different additives and different loads were studied by scanning electron microscopy. Small (severe) damage of the pin surface was observed for WS<SUB>2</SUB>/WO<SUB>3</SUB> nanoparticles (WS<SUB>2</SUB> micropowders) additives.</P>
Si, Ping-Zhan,Qian, Hui-Dong,Choi, Chul-Jin,Park, Jihoon,Ge, Hong-Liang North-Holland Pub. Co 2018 Journal of magnetism and magnetic materials Vol.451 No.-
<P><B>Abstract</B></P> <P>The temperature for phase transformation of ε → τ in Mn<SUB>54</SUB>Al<SUB>46</SUB>C<I> <SUB>x</SUB> </I> (hereafter denoted by MnAlC<I> <SUB>x</SUB> </I>, <I>x</I> = 0–5) alloys was systematically studied by using the traditional thermal analysis method and a more precise magnetic measurement method developed in this work. The effect of carbon content and cold-rolling on the magnetic properties of the MnAlC<I> <SUB>x</SUB> </I> alloys was studied. The onset temperature of massive growth of τ- from ε-phase increases with increasing carbon content in MnAlC<I> <SUB>x</SUB> </I>. The carbon content has little effect on the onset temperature of displacive growth of ε → τ but has substantial effect on the displacive growth rate at certain temperature. Pure τ-MnAlC<SUB> <I>x</I> </SUB> with varied <I>x</I> was obtained by annealing the ε-phase at optimum temperatures determined by our method. The Curie temperature of the MnAlC<SUB> <I>x</I> </SUB> decreases significantly first and then increases slightly with increasing carbon content. The coercivity and the remanent magnetization of the as-prepared τ-MnAlC<SUB> <I>x</I> </SUB> increase with increasing <I>x</I> first and become stable at <I>x </I>> 3 and <I>x</I> > 4, respectively. A cold-rolling method was introduced in this work to enhance the magnetic properties of τ-MnAlC<SUB> <I>x</I> </SUB>. The coercivity and remanent magnetization of the τ-MnAl after cold-rolling were enhanced up to 4.3 times and 3.3 times, respectively. The coercivity of the cold-rolled τ-MnAlC<SUB> <I>x</I> </SUB> decreases with increasing <I>x</I> and becomes stable when <I>x</I> > 2. The remanent magnetization and saturation magnetization of the cold-rolled τ-MnAlC<SUB> <I>x</I> </SUB> vary little with <I>x</I>.</P> <P><B>Highlights</B></P> <P> <UL> <LI> A method to measure the phase transformation temperature of MnAl-C is reported. </LI> <LI> A cold-rolling method is employed to enhance the magnetic properties of MnAl-C. </LI> <LI> The phase transformation temperature increases with increasing carbon content. </LI> </UL> </P> <P><B>Graphical abstract</B></P> <P>[DISPLAY OMISSION]</P>
Fu, Si-Rui,Zhang, Ying-Qiang,Li, Yong,Hu, Bao-Shan,He, Xu,Huang, Jian-Wen,Zhan, Mei-Xiao,Lu, Li-Gong,Li, Jia-Ping Asian Pacific Journal of Cancer Prevention 2014 Asian Pacific journal of cancer prevention Vol.15 No.7
Background: Sorafenib is a promising drug for advanced hepatocellular carcinoma (HCC); however, treatment may be discontinued for multiple reasons, such as progressive disease, adverse events, or the cost of treatment. The consequences of sorafenib discontinuation and continuation are uncertain. Materials and Methods: We retrospectively analyzed 88 HCC patients treated with sorafenib from July 2007 to January 2013. Overall survival (OS), post-disease progression overall survival (pOS), and time to disease progression (TTP) were compared for survival analysis. Cox proportional hazard regression was performed to assess the effect of important factors on OS in the overall patient population and on pOS in patients who continued sorafenib treatment. Results: Sorafenib was discontinued and continued in 24 and 64 patients, respectively. The median OS (355 vs 517 days respectively; p=0.015) and median post-PD OS (260 vs 317 days, respectively; p=0.020) were statistically different between the discontinuation and continuation groups. Neither the median time to first PD nor the time to second PD were significantly different between the 2 groups. In the discontinuation group, 3 of the 24 patients (12.5%) suffered disease outbreaks. In Cox proportional hazard regression analysis after correction for confounding factors, BCLC stage (p=0.002) and PD site (p=0.024) were significantly correlated with pOS in patients who continued sorafenib treatment. Conclusions: Sorafenib discontinuation may cause HCC flares or outbreaks. It is advisable to continue sorafenib treatment after first PD, particularly in patients with Barcelona Clinic Liver Cancer stage B disease or only intrahepatic PD.
The Effect of Mn/Al Substitution on the Structural Stability and Magnetic Properties of Mn₃AlC
Xin-You Wang,Ping-Zhan Si,Hui-Dong Qian,Yang Yang,Hong-Liang Ge,Jihoon Park,Xin-Qing Wang,Chul-Jin Choi 한국자기학회 2019 Journal of Magnetics Vol.24 No.1
The structural stability and magnetic properties of Mn3+xAl1-xC antiperovskite with varied Mn/Al substitution were studied systematically. Single phase Mn3+xAl1-xC alloys with antiperovskite structure were obtained in samples with x = −1/4, 0, 1/4, 1/2. An additional Mn23C₆ phase was precipitated from Mn3+xAl1-xC antiperovskite for x = 3/4 while Mn23C₆ phase was formed as major phase for x = 1. The mutual substitution of Mn and Al atoms has substantial effect on the Curie temperature and the saturation magnetization of the Mn3+xAl1-xC alloys. In comparison with the as-cast alloys, the as-annealed Mn3+xAl1-xC alloys exhibit reduced Mn/Al substitutions after high temperature homogenization, which enhances the ordering of Mn and Al atoms in the lattices. The Curie temperature of the homogenized Mn3+xAl1-xC increases with increasing Mn substitution to Al. The Mn₃AlC alloy shows the highest saturation magnetization among all samples with varied Mn/Al ratios. Most samples show zero coercivity and zero remanent magnetization. The maximum value of the magnetic entropy changes of Mn2.75Al1.25C at 285 K is 2.26 J/㎏ K in fields up to 3 T.