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Effects of Bath Temperature on Electrodeposited Permanent Magnetic Co-Pt-W(P) Films
Hongliang Ge*,Qiong Wu,Guoying Wei,Xinyan Wang,Qiaoying Zhou 대한화학회 2007 Bulletin of the Korean Chemical Society Vol.28 No.12
The effects of bath temperature on electrochemical behavior, alloy composition, crystallographic structure, morphology and the magnetic properties of electrodeposited Co-Pt-W(P) films were investigated. Electro- chemical studies show that alloy electrodeposition has been shifted to more positive potentials and the critical time for nucleation decreased as electrolyte temperature increased. As the temperature increased from 40 oC to 80 oC, tungsten content in the deposit increased, while phosphorus content decreased. The films deposited at T = 40 oC exhibited soft magnetic properties. However, electrodeposited at T = 70 oC, the films exhibited hard magnetic properties. It is also demonstrated that higher temperature more than 70 oC could weaken hard magnetic properties. XRD results indicated that the deposits obtained at 50 oC-70 oC showed enhancement of [00.1] P.O. (preferred orientation) with the bath temperature, which resulted in the stronger perpendicular magnetic anisotropy.
Effects of Bath Temperature on Electrodeposited Permanent Magnetic Co-Pt-W(P) Films
Ge, Hongliang,Wu, Qiong,Wei, Guoying,Wang, Xinyan,Zhou, Qiaoying Korean Chemical Society 2007 Bulletin of the Korean Chemical Society Vol.28 No.12
The effects of bath temperature on electrochemical behavior, alloy composition, crystallographic structure, morphology and the magnetic properties of electrodeposited Co-Pt-W(P) films were investigated. Electrochemical studies show that alloy electrodeposition has been shifted to more positive potentials and the critical time for nucleation decreased as electrolyte temperature increased. As the temperature increased from 40 oC to 80 oC, tungsten content in the deposit increased, while phosphorus content decreased. The films deposited at T = 40 oC exhibited soft magnetic properties. However, electrodeposited at T = 70 oC, the films exhibited hard magnetic properties. It is also demonstrated that higher temperature more than 70 oC could weaken hard magnetic properties. XRD results indicated that the deposits obtained at 50 oC-70 oC showed enhancement of [00.1] P.O. (preferred orientation) with the bath temperature, which resulted in the stronger perpendicular magnetic anisotropy.
Yuanlong Zhang,Hongliang Ge,Mingxia Xu,Wenzhong Mei 대한신경외과학회 2023 Journal of Korean neurosurgical society Vol.66 No.2
Objective : The facial nerve trace on the ipsilateral side of the vestibular schwannoma was reconstructed by diffusion tensor imaging tractography to identify the adjacent relationship between the facial nerve and the tumor, and to improve the level of intraoperative facial nerve protection. Methods : The clinical data of 30 cases of unilateral vestibular schwannoma who underwent tumor resection via retrosigmoid approach were collected between January 2019 and December 2020. All cases underwent magnetic resonance imaging examination before operation. Diffusion tensor imaging and anatomical images were used to reconstruct the facial nerve track of the affected side, so as to predict the course of the nerve and its adjacent relationship with the tumor, to compare the actual trace of the facial nerve during operation, verify the degree of coincidence, and evaluate the nerve function (House-Brackmann grade) after surgery. Results : The facial nerve of 27 out of 30 cases could be displayed by diffusion tensor imaging tractography, and the tracking rate was 90% (27/30). The intraoperative locations of facial nerve shown in 25 cases were consistent with the preoperative reconstruction results. The coincidence rate was 92.6% (25/27). The facial nerves were located on the anterior middle part of the tumor in 14 cases, anterior upper part in eight cases, anterior lower part in seven cases, and superior polar in one case. Intraoperative facial nerve anatomy was preserved in 30 cases. Among the 30 patients, total resection was performed in 28 cases and subtotal resection in two cases. The facial nerve function was evaluated 2 weeks after operation, and the results showed grade I in 12 cases, grade II in 16 cases and grade III in two cases. Conclusion : Preoperative diffusion tensor imaging tractography can clearly show the trajectory and adjacent position of the facial nerve on the side of vestibular schwannoma, which is beneficial to accurately identify and effectively protect the facial nerve during the operation, and is worthy of clinical application and promotion.
Magnetic Microstructures and Corrosion Behaviors of Nd-Fe-B-Ti-C Alloy by Ga Doping
Qiong Wu,Pengyue Zhang,Hongliang Ge,Aru Yan,Dongyun Li 한국자기학회 2013 Journal of Magnetics Vol.18 No.3
The influences of Gallium doping on the magnetic microstructures and corrosion behaviors of Nd-Fe-B-Ti-C alloys are investigated. The cooling rate for obtaining fully amorphous structure is raised, and the glassforming ability is improved by the Ga addition. The High Resolution Transmission Electron Microscopy image shows that the α-Fe and Fe3B soft magnetic phases become granular surrounded by the Nd2Fe14B hard magnetic phase. The rms and (Δ?)rms value of Nd-Fe-B-Ti-C nanocomposite alloy thick ribbons in the typical topographic and magnetic force images detected by Magnetic Force Microscopy(MFM) decreases with 0.5 at% Ga addition. The corrosion resistances of Nd9Fe73B₁₂.6C ₁.₄Ti₄-xGax (x = 0, 0.5, 1) alloys are enhanced by the Ga addition. It can be attributed to the formation of more amorphous phases in the Ga doped samples.
Guoying Wei,Yongdong Jin,Hongliang Ge,Jiuli Luo 대한화학회 2005 Bulletin of the Korean Chemical Society Vol.26 No.4
The Belousov-Zhabotinskii system measured by a Pt electrode is investigated under external electrode current constraint. A dynamical analysis of the electrode reaction phase has been made by means of a linearized stability criterion valid for three-variable system. It turns out that limit cycle oscillatory regime and dynamical behaviors of the electrode reaction phase have been degenerated under periodical electrode current.
Study on Anomalous Codeposition Phenomenon of CoNi Magnetic Films
Yundan Yu,Guoying Wei,Hongliang Ge,Li Jiang,Lixia Sun 한국자기학회 2017 Journal of Magnetics Vol.22 No.2
CoNi alloy films prepared from electrolytes with various concentrations of cobalt ions were studied in the paper. Influences of different cobalt ions concentrations on electrochemistry processes, components, microstructures, surface morphologies and magnetic properties of CoNi films were investigated. It was found that CoNi film plating was a kind of anomalous codeposition process. The percentage of cobalt content in CoNi films was higher than that of in the electrolyte. Moreover, with the rise of cobalt ions concentrations, the percentage of cobalt content in the samples increased gradually. CoNi films possessed crystal structures with four stronger diffraction peaks. However, CoNi films prepared from bath with higher cobalt ions possessed hcp structures which contributed to dendrite structures resulting in the increase of coercivity.
Wei, Guoying,Jin, Yongdong,Ge, Hongliang,Luo, Jiuli Korean Chemical Society 2005 Bulletin of the Korean Chemical Society Vol.26 No.4
The Belousov-Zhabotinskii system measured by a Pt electrode is investigated under external electrode current constraint. A dynamical analysis of the electrode reaction phase has been made by means of a linearized stability criterion valid for three-variable system. It turns out that limit cycle oscillatory regime and dynamical behaviors of the electrode reaction phase have been degenerated under periodical electrode current.
Lingfeng Wang,Guoli Lei,Chong Yan,Hongliang Ge 한국자기학회 2019 Journal of Magnetics Vol.24 No.4
With the development of switching power supplies, miniaturization and high efficiency become hot research issues, and decreasing high-frequency losses is an effective method to achieve it. In this article, the effect of different calcination temperature on the power losses of MnZn ferrites at high frequency (500 kHz) over a broad temperature range is reported. The MnZn ferrites samples were prepared by ceramic process and the effect of calcination temperature was analyzed. The raw materials were calcined at 775 ℃, 800 ℃, 825 ℃, 850 ℃, 875℃, 900 ℃, 925 ℃ and 950 ℃, and the regular fluctuations of particle size (as-calcined), density (as-sintered) and magnetic properties are presented in this work. It is shown that the samples calcined at 850 ℃ exhibit optimal microstructure and magnetic properties. The newly developed MnZn ferrites are characterized by sintered density of 4.61 g/cm³, initial permeability of 1223 (10 kHz/0.1 mT/25 ℃), saturation magnetic flux density of 488 mT (10 kHz/1200 A/m/25 ℃) and power losses of 68 mW/cm³ (500 kHz/50 mT/100 ℃).
Sihao Hua,Pengyue Zhang,Hangfu Yang,Suyin Zhang,Hongliang Ge 한국자기학회 2013 Journal of Magnetics Vol.18 No.1
This paper studies the effects of the Mn-site substitution by nickel on the magnetic properties and the magnetocaloric properties of La0.7Ca0.3Mn1-xNixO₃ (x = 0, 0.05 and 0.1). The orthorhombic crystal structures of the samples are confirmed by the room temperature X-ray diffraction. The dependence of the Curie temperature (TC) and the magnetic entropy change (ΔSM) on the Ni doping content was investigated. The samples with x = 0 had the first order phase transition, while the samples with x = 0.05 and 0.1 had the second order phase transition. As the concentration of Ni increased, the maximum entropy change (|ΔSM|max) decreased gradually, from 2.78 Jㆍ㎏?¹ㆍK?¹ (x = 0) to 1.02 Jㆍ㎏?¹ㆍK?¹ (x = 0.1), in a magnetic field change of 15 kOe. The measured value of TC was 185 K, 150 K and 145 K for x = 0, 0.05 and 0.1, respectively. The phase transition temperatures became wider as x increased. It indicates that the Mn-site substitution by Ni may be used to tailor the Curie temperature in La0.7Ca0.3Mn1-xNixO₃.