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Zheng, Hao,Zhang, Qing,Kim, Seung-Joo,Jiang, Xueya,Dan, Meiyu,Gao, Hong,Li, Shengbiao,Wang, Shiquan,Feng, Chuanqi American Scientific Publishers 2013 Journal of Nanoscience and Nanotechnology Vol.13 No.4
<P>KMn8O16 nanorods were prepared through a facile hydrothermal method by using KMnO4 and MnSO4 as reactants. The KMn8O16 samples synthesized at different temperatures (100-160 degrees C) were characterized by X-ray diffraction (XRD), transmission electron microscopy (TEM), and its electrochemical properties were tested by galvanostatic charge/discharge system. The effect of reaction temperature on the morphology and electrochemical properties was investigated. As electrode materials for the lithium ion battery cycled between 1.5 and 4.2 V, the KMn8O16 nanorods synthesized at 160 degrees C show the highest reversible discharge capacity (160.1 mA h/g even after 50 cycles at current density of 50 mA/g) and the best cycling stability. These results indicate that the KMn8O16 nanorods could be a promising cathode material for lithium ion batteries.</P>
Wang Xin,Du Jun,Wei Zhengying,Zhang Shan,Zhao Guangxi,Ren Chuanqi,Bai Hao 대한기계학회 2019 JOURNAL OF MECHANICAL SCIENCE AND TECHNOLOGY Vol.33 No.2
In order to achieve good interlayer metallurgical bonding in the metal fused-coating additive manufacturing, the finite element thermal analysis model was established and the influences of different heating temperatures of fused coating nozzle and substrate on the interlayer remelting was analyzed. The maximum remelting depth under different temperature conditions was obtained. The multi-layer forming experiments were performed under different temperature conditions, and the results showed that increasing the heating temperature of nozzle or substrate will effectively increase the remelting depth, that the surface forming quality is better when the remelting depth is in the range of 0.1~0.2 mm, and that the deviation between the remelting depth and the calculated value is less than 15 %. So, the model can predict the remelting depth of the intermetallic microstructure.
Free arc liquid‑phase dispersion method for the preparation of carbon nanotube dispersion
Shaolong Li,Youdong Ci,Da Zhang,Chuanqi Zhang,Yan He 한국탄소학회 2021 Carbon Letters Vol.31 No.2
In this study, a new method of rapid preparation of carbon nanotube (CNT) solution with highly dispersed morphology by free arc excitation is proposed, which shortens the time of the preparation of CNT solution with low concentration. The principle is that the high-energy flow density heat generated by the free arc makes the vaporizable substance coated on the surface of CNTs vaporize rapidly, and then generates the bulk increasing motion, which makes the CNTs aggregates dispersed, and finally forms the CNTs gas-phase dispersion monomer with high dispersion or the cross-linking morphology of few CNTs. In this paper, the influence of gum Arabic (GA) and deionized water (DI water) contents in CNTs mixed electrode on the dispersion of CNTs in different environments (gas phase and liquid phase) is explored. In the limited case of this work, the dispersion effect is better when the mass ratio of CNTs, GA and DI water is 1:0.04:3.96 in the liquid-phase environment. The preparation method reported in this work is expected to be a rapid way to obtain low-concentration nanodispersion.
A novel preparation and formation mechanism of carbon nanotubes aerogel
Li Shaolong,He Yan,Jing Chengwei,Gong Xiubin,Cui Lianlei,Cheng Zhongyue,Zhang Chuanqi,Nan Fei 한국탄소학회 2018 Carbon Letters Vol.28 No.-
A novel, unique, and effective method for carbon nanotube (CNT) dispersion by the free arc stimulation is proposed. CNTs are introduced as an aerogel into the air space via the dispersion method and can be utilized as a solution by adding it to solvents. The volume of the original generated CNT aerogel with a high-volume expansion ratio displays a performance two orders of magnitudes better than that of raw CNTs, which is considered a powerful characterization of the dispersion effect. The CNT aerogel, which was observed by scanning electron microscopy also showed a satisfactory dispersion morphology. Its structure and properties were tested before and after dispersion by Raman spectroscopy and great consistency was observed, which proved that the CNTs were undamaged. This approach may greatly promote the large-scale application of CNTs.
Li Shaolong,Qingdao University of Science and Technology,Qingdao University of Science and Technology,Qingdao University of Science and Technology,Liu Xingyang,He Yan,Zhang Chuanqi,Wang Jinyu,Fu Jinfe 한국탄소학회 2020 Carbon Letters Vol.30 No.6
To investigate the efect of gas dispersing carbon nanotubes (CNTs) and hot pressing method on the transparency and the conductivity of thin flms, the free arc was used to disperse the CNTs in a high dispersion rate, and the dispersed CNTs were rapidly pressed into the surface of the PET flm by hot pressing to obtain electrical conductivity. The relationship between the light transmission and sheet resistance of the flm was studied by changing the deposition time and the presence or absence of electrostatic adsorption. It was found that the CNTs modifed flm still retains good electrical conductivity (sheet resist�ance up to 6×104 Ω, light transmittance 69%) through the cleaning of surfactants and ultrasonic waves, which proves that hot pressing is a simple physical method to achieve efective combination of CNTs and flms.