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Paleogene lacustrine dolomitization, Xingou region, southern Qianjiang Depression, China
Junjun Shen,Bo Chen,Fangfang Chen,Chao Cheng,Yangfan Li,Ying Tian 한국지질과학협의회 2016 Geosciences Journal Vol.20 No.2
The lacustrine dolomicrites of Unit II of the lower Xingouzui Formation deposited in the southern part of the Qianjiang Depression provide a good “tight carbonate” hydrocarbon reservoir. The dolomicrites are typically interbedded with and sourced from organic-rich argillite, which together form a source-reservoir assemblage characterized by thin single-layer thicknesses, far lateral extent and continuous lateral distribution. Systematic sedimentological and geochemical studies indicate that the depositional environment and organic matter evolution of the dark argillites (with TOC of 0.5–2%) are favorable for formation of the dolomicrites. The dolomicrite was mainly formed in a shallow-water evaporative environment; crystals are anhedral under SEM, in non-surface contact, and include a number of honeycomb intergranular micropores associated with replacement. The dolomicrite shows orange-orangered light by cathodoluminescence, indicative of association with minor terrigenous debris; X-ray diffraction results indicate that the dolomicrite is characterized by high calcium content (CaCO3 molar contents of 52.28–52.28%), low degree of orders of 0.2–0.4), and high content of Fe. The dolomicrite has δ18O values of 2.47–2.47‰ PDB, more positive than micrite, and δ13C values as moderately negative as 9.4–4.21‰ PDB, similar to micrite. Both values indicate the dolomicrite formed in a low-temperature genetic zone. Together, these characteristics indicate that the dolomicrite in the study area was formed in a high-salinity, confined lake basin, characterized by low temperature, shallow burial, and rapid nucleation and crystallization. The dolomicrite experienced a contemporaneous period with formation of dark mudstone, shale and calcite, and a penecontemporaneous period with formation of dolomicrite via seepage-reflux and a diagenetic period when ferrodolomite was formed via burial.
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Coprecipitation Synthesis of Fe-doped ZnO Powders with Enhanced Microwave Absorption Properties
Ruiwen Shu,Xin Wang,Yingying Yang,Xiayu Tang,Xian Zhou,Yangfan Cheng 성균관대학교(자연과학캠퍼스) 성균나노과학기술원 2016 NANO Vol.11 No.12
In this work, the Fe-doped ZnO powders have been synthesized by a facile chemical coprecipitation method. The structure, morphology and magnetic properties of the as-prepared powders were characterized by X-ray diffraction (XRD), scanning electron microscopy (SEM), transmission electron microscopy (TEM), energy dispersive X-ray spectrum (EDS), X-ray photoelectron spectroscopy (XPS) and vibrating sample magnetometer (VSM). The results showed that the Fe ions were well incorporated into the crystal lattice of ZnO and had a valence state of +3. The magnetization curves indicated the Fe-doped ZnO presented the ferromagnetic behavior at room temperature. Moreover, the electromagnetic (EM) parameters and microwave absorption properties of Fe-doped ZnO/paraffin wax in the frequency range of 2–18 GHz were explored. The minimum reflection loss reached -38.4 dB at 6.6 GHz, and the reflection loss less than -10.0 dB was 4.0 GHz (from 11.0 GHz to 15.0 GHz) with a thickness of only 2.5 mm. Significantly, the enhanced microwave absorption of the as-prepared powders could be achieved by doping with Fe3+ ions or varying the thickness of the absorbers. The mechanism of microwave absorption were attributed to the good impedance matching, the dielectric loss resulted from the crystal lattice defects and the magnetic loss originated from the natural resonance. It is believed that the Fe-doped ZnO powders could be used as potential microwave absorbers.
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