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Coloring mechanism of celadon glazes from Yaozhou kiln
Zhen Sang,Fen Wang,Xiaojuan Yuan,Shurui Shen,Jing Wang,Xiaohong Wei 한양대학교 청정에너지연구소 2022 Journal of Ceramic Processing Research Vol.23 No.6
The Five Dynasty sky-green, Song dynasty olive-green and Jin dynasty moon-white glazes are three typical glazes of theYaozhou celadon. In this work, the coloring mechanism of the three celadon glazes were compared and analyzed by usingcolorimeter, EDXRF, XRD, XPS and Raman spectrometer. The results indicate that the content of Fe2O3 is proportional tothe depth of the glaze colors. The Raman Ip value indicates that the firing temperature of the Song dynasty olive-green glazewas the highest, followed by the Five Dynasty, and then the Jin dynasty. The lower firing temperature and dense bubbles areimportant causes of the high opacification of the Jin moon-white glaze. The ratio of Fe2+ to Fe3+ in the glaze is directlyproportional to the b* value, which is the main reason for why the Yao celadon glaze colors are yellow-green in Song, butbluish in the Five Dynasty and Jin dynasty.
Peiqing La,Xin Guo,Hongding Wang,Ting Shi,Xiaojuan Zhen,Fuan Wei,Xuefeng Lu 대한금속·재료학회 2016 METALS AND MATERIALS International Vol.22 No.2
Bulk 1020 carbon steel was prepared by aluminothermic reaction casting. After casting, isothermal aging treatments at different temperatures are performed for different periods up to 8 h. Microstructure characterization was performed using many methods, including optical microscopy, X-ray diffraction, scanning electron microscopy and transmission electron microscopy. It was found that the steel consisted of a nanocrystalline- ferrite matrix and a microcrystalline pearlite phase with a laminar structure. The average grain sizes of the ferrite were 23, 24, 28, and 37 nm for the cast steel and for samples annealed at 600, 800, and 1000 °C, respectively. As the annealing temperature increased, the volume fraction of the pearlite initially increased and then decreased, while the laminar spacing of pearlite increased from 240 to 900 nm. When annealed at 1000 °C, a spherical black micron pearlite particle was formed. The tensile and yield strength dramatically decreased, and the elongation varied slightly with the annealing temperature. A ductile phase was achieved by extending the holding time.