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- 저자 : Vesna Miškovi c-Stankovi c (검색결과 1 건)
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Katarina Nešovi c,Ana Jankovic,Aleksandra Peri c-Gruji c,Maja Vukašinovic-Sekulic,Tamara Radeti c,Ljiljana Živkovi c,박수진,이경엽,Vesna Miškovi c-Stankovi c 한국공업화학회 2019 Journal of Industrial and Engineering Chemistry Vol.77 No.-
Silver nanoparticles (AgNPs) were synthesized by in situ electrochemical reduction of Ag+ ions in poly(vinyl alcohol)/chitosan/graphene (PVA/CHI/Gr) hydrogel matrices with different concentrations ofchitosan. The physicochemical properties of nanocomposite hydrogels were investigated by UV–visspectroscopy (UV–vis), dynamic light scattering (DLS), transmission electron microscopy (TEM), X-rayphotoelectron spectroscopy (XPS),field-emission scanning electron microscopy (FE-SEM) and Fourier-transform infrared spectroscopy (FT-IR), thermal characteristics were determined by differentialscanning calorimetry (DSC) and mechanical properties were measured by tensile test. The swellingstudies were carried out in phosphate buffer to simulate natural physiological environment and datawerefitted by several kinetic models to determine the diffusion mechanism and diffusion coefficients ofthe swelling medium through the hydrogel matrices. It was shown that the presence of silvernanoparticles increased the uptake capability and equilibrium swelling degree of the compositehydrogels. The antibacterial activity was confirmed against Escherichia coli and Staphylococcus aureus,while the hydrogels without AgNPs exhibited antibacterial properties due to the presence of chitosan. With the addition of AgNPs, the samples showed stronger activity and fast reduction in the number ofcolonies, confirming the synergistic effect of chitosan and AgNPs on the antibacterial activity.
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