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Wada Shintaro,Hagio Takeshi,Kunishi Hiroto,Park Jae-Hyeok,Phouthavong Vanpaseuth,Yamada Yuta,Terao Toshihiro,Li Xinling,Nijpanich Supinya,Ichino Ryoichi 한국세라믹학회 2023 한국세라믹학회지 Vol.60 No.6
Crystalline microporous membranes are promising tools for gas separation because their molecular dimension pores allow us to accurately sieve molecules by size. Recently, microporous hexagonal WO3 was reported as a new potential membrane material and its membrane was found to enable separation of water from water/acetic acid mixtures. Pore size of hexagonal WO3 seemed to be also suitable for separation of small gasses; however, its gas permeation properties have not been reported. Additionally, densification of membranes by decreasing intercrystalline gaps are extremely important in gas separation. One effective method to densify polycrystalline membranes is to repeat membrane synthesis, namely multi-stage synthesis. Here, we attempt to prepare dense hexagonal WO3 membranes on porous tubular supports by multi-stage synthesis and examined their densification and gas permeation properties. Densification was confirmed by permeation of SF6 (gas molecule larger than pores of hexagonal WO3), and its potential for separating small gasses was considered from single gas permeation of He and He/SF6 permselectivity. The results indicated that the multi-stage synthesis is effective to densify the membranes and He/SF6 permselectivity reached 42.8 for three-stage synthesis under modified conditions, implying hexagonal WO3 is a potential membrane material for small gas separation.
Development of Synthetic Magnetic Zeolite Adsorbents and Application to Ammonium Ion Removal
Yuki Kamimoto,Takeshi Hagio,정용준,Ryoichi Ichino,길경익 대한토목학회 2020 KSCE JOURNAL OF CIVIL ENGINEERING Vol.24 No.5
Synthetic magnetic zeolite with Fe3O4 was developed and its adsorption performance of ammonium ions was examined. The influence of pH levels, Fe3O4 content of the magnetic zeolite, magnetization curve of the magnetic zeolite and isotherm curve were examined in batch type experiments. Magnetic zeolite synthesized by a hydrothermal process was observed with less than 12.6 wt% of Fe3O4 content by scanning electron microscope (SEM) and X-ray diffraction (XRD) analysis. With the optimum pH level around 8, qe decreases linearly with the increase of Fe3O4 content. Additionally, the adsorption isotherm ofammonium ions is approximated by a Langmuir equation when the maximum adsorption was obtained at about 1.60 mmolg−1. Such processes as the substitution and thermal desorption methods were successfully introduced to regenerate the magnetic zeolite saturated by ammonium ions, which is shown to be easily separated by magnetic force. Thus, the magnetic zeolite is a potential adsorbent for the removal of ammonium ions with an easy separation method using a magnetic process.
Biofilms formation of polymeric materials and its new quantitative evaluation
Hideyuki Kanematsu,Dana M. Barry,Akiko Ogawa,Takeshi Kogo,Risa Kawai,Hidekazu Miura,Nobumitsu Hirai,Takehito Kato,Toshio Kamijo,Michiko Yoshitake,Takeshi Hagio,Ryoichi Ichino 한국표면공학회 2023 한국표면공학회 학술발표회 초록집 Vol.2023 No.11-1