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      • Nanoscale quantitative mechanical mapping of poly dimethylsiloxane in a time dependent fashion

        Zhang, Shuting,Ji, Yu,Ma, Chunhua Techno-Press 2021 Advances in nano research Vol.10 No.3

        Polydimethylsiloxane (PDMS) is one of the most widely adopted silicon-based organic polymeric elastomers. Elastomeric nanostructures are normally required to accomplish an explicit mechanical role and correspondingly their mechanical properties are crucial to affect device and material performance. Despite its wide application, the mechanical properties of PDMS are yet fully understood. In particular, the time dependent mechanical response of PDMS has not been fully elucidated. Here, utilizing state-of-the-art PeakForce Quantitative Nanomechanical Mapping (PFQNM) together with Force Volume (FV) and Fast Force Volume (FFV), the elastic moduli of PDMS samples were assessed in a time-dependent fashion. Specifically, the acquisition frequency was discretely changed four orders of magnitude from 0.1 Hz up to 2 kHz. Careful calibrations were done. Force data were fitted with a linearized DMT contact mechanics model considering surface adhesion force. Increased Young's modulus was discovered with increasing acquisition frequency. It was measured 878 ± 274 kPa at 0.1 Hz and increased to 4586 ± 758 kPa at 2 kHz. The robust local probing of mechanical measurement as well as unprecedented high-resolution topography imaging open new avenues for quantitative nanomechanical mapping of soft polymers, and can be extended to soft biological systems.

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        Modification of tool influence function for bonnet polishing tool based on analysis of interfacial contact state

        Ri Pan,Xiangxiang Zhu,Zhenzhong Wang,Dongju Chen,Shuting Ji,Jinwei Fan,Rui Wang 대한기계학회 2022 JOURNAL OF MECHANICAL SCIENCE AND TECHNOLOGY Vol.36 No.6

        The polishing mechanism of bonnet polishing (BP) and the tool influence function (TIF) of bonnet tool have been widely studied. However, most of current studies pay little attention to the influence of polishing slurry on the BP mechanism as well as TIF. This study proposes that the interfacial contact state between the polishing tool and the workpiece is in a mixed lubrication state, subsequently the BP mechanism is further explored. It is found that the workpiece material is removed by polishing pad and abrasives. The polishing slurry is not directly involved in workpiece removal, but shares the normal pressure of the polishing tool on workpiece, which affects material removal. Based on the above mechanism, the TIF removal prediction model is established and verified by experiments. The results show that the maximum error of the model prediction value is quiet small, which verifies the model. Moreover, compared with Preston model and the previous model, which ignored the influence of the fluid, the average prediction error of the model in this paper when D 0 = 20 mm is 6.38 %, while the previous model and Preston model are 11.21 % and 49.10 %, respectively. Which illustrates the model in this paper has higher accuracy.

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