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- 저자 : Guoxiang Pan (검색결과 2 건)
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Yue Meng,Shengjie Xia,Guoxiang Pan,Jilong Xue,Junhui Jiang,Zheming Ni 한국화학공학회 2017 Korean Journal of Chemical Engineering Vol.34 No.8
Copper(II) Schiff-base Complexes (Salen-Cu(II)) intercalated zinc-chromium layered double hydroxides (ZnSBCuCr-LDHs) were successfully prepared via coprecipitation. Then, a novel photocatalytic material Zn-Cu-Cr composite oxides (ZnSBCuCr-MO) was prepared after calcination at 500 oC with ZnSBCuCr-LDHs as precursor. The structure and properties of the materials were thoroughly characterized by powder X-ray diffraction (XRD), inductively coupled plasma atomic emission spectrometry (ICP-AES), ultraviolet visible diffuse reflectance spectroscopy (UV-Vis DRS), scanning electron microscopy (SEM) and X-ray photoelectron spectroscopy (XPS). The photocatalytic activities of the materials were investigated by photodegradation of a cationic dye Rhodamin B (RhB), which was hard to adsorb by LDHs. The effects of the photocatalyst dosage, the initial pH and temperature of RhB solution on the photocatalytic efficiency were discussed. The results showed that ZnSBCuCr-MO displayed higher photocatalytic activity for RhB than calcined ZnCr-LDHs (ZnCr-MO) and calcined ZnCuCr-LDHs (ZnCuCr-MO). Meanwhile, ZnSBCuCr- MO exhibited better stability and reusability. In addition, the possible photocatalytic mechanism and degradation pathway for RhB were studied through density functional theory (DFT) calculation of the RhB molecule, UV-vis absorption variation and LC-MS analyses of the RhB solution.
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Peisong Tang,Yi Tong,Haifeng Chen,Feng Cao,Guoxiang Pan 한국물리학회 2013 Current Applied Physics Vol.13 No.2
Single phase perovskite LaFeO3 nanoparticles are directly synthesized by a one-step microwave-assisted route without additional high temperature calcination process. The prepared sample is characterized by X-ray diffraction (XRD), field emission scanning microscope (FE-SEM), BrunauereEmmetteTeller (BET) specific surface area measurement, diffuse reflectance spectroscopy (DRS) and Fourier transform infrared spectroscopy (FTIR). XRD and SEM show that the prepared LaFeO3 is single phase perovskite and spherelike shape. The DRS result shows that the prepared LaFeO3 has strong visible-light absorption and an optical absorption onset of 525 nm, corresponding to an optical band gap of 2.36 eV. The photocatalytic experiment demonstrates that LaFeO3 is highly visible-light photocatalytic active for the degradation of methylene blue. It is suggested that the narrow band gap and the strong visible-light absorption are responsible for the high visible-light photocatalytic activity of the prepared LaFeO3
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