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Effect of FeNi30 Powder Catalyst by Water Atomizing on Synthesis High-grade Diamond
Cheng Dong-kai,Ma Hong-qiu,Cao Dan,Ding Fu-chang 한국분말야금학회 2006 한국분말야금학회 학술대회논문집 Vol.2006 No.1
This paper described the preparation method for composing high-grade synthetic diamond by water atomizing using FeNi30 powder catalyst. The objective of this article is about powder making process using super high water atomizing in the atmosphere of inert gas, and then corroded the powder with a corrosion inhibitor. Finally, FeNi30 catalyst powder with lower oxygen content and good sphericity is produced. The experiment of making diamonds by using cubic press and the performance of the diamonds are also discussed.
The Influence of Hi-flux Powders Characteristics on the Performance of Magnetic Powder Cores
Zhao Tong Chun,Ma Hong Qiu,Ding Fu Chang 한국분말야금학회 2006 한국분말야금학회 학술대회논문집 Vol.2006 No.1
The influence of Hi-flux powders characteristics on the performance of magnetic powder cores was studied. It was found that different cooling rate and nozzle configuration could change the shape and microstructure of powders. Smooth surface and spherical shape of powders were beneficial to improve DC bias performance and reduce core losses of magnetic powder core.
A study on the dynamic characteristics of the secondary loop in nuclear power plant
Zhang, J.,Yin, S.S.,Chen, L.,Ma, Y.C.,Wang, M.J.,Fu, H.,Wu, Y.W.,Tian, W.X.,Qiu, S.Z.,Su, G.H. Korean Nuclear Society 2021 Nuclear Engineering and Technology Vol.53 No.5
To obtain the dynamic characteristics of reactor secondary circuit under transient conditions, the system analysis program was developed in this study, where dynamic models of secondary circuit were established. The heat transfer process and the mechanical energy transfer process are modularized. Models of main equipment were built, including main turbine, condenser, steam pipe and feedwater system. The established models were verified by design value. The simulation of the secondary circuit system was conducted based on the verified models. The system response and characteristics were investigated based on the parameter transients under emergency shutdown and overload. Various operating conditions like turbine emergency shutdown and overspeed, condenser high water level, ejector failures were studied. The secondary circuit system ensures sufficient design margin to withstand the pressure and flow fluctuations. The adjustment of exhaust valve group could maintain the system pressure within a safe range, at the expense of steam quality. The condenser could rapidly take out most heat to avoid overpressure.
Study on molten salt oxidation process of simulated Co doped cation exchange resins
Yun Xue,Yue-Lin Wang,Yu Li,Wen-Da Xu,Fu-Qiu Ma,Yang-Hai Zheng,Qing-Guo Zhang,Zhi Zhang,Mi-lin Zhang,Yong-De Yan 한국공업화학회 2023 Journal of Industrial and Engineering Chemistry Vol.126 No.-
Cation exchange resins (CERs) are widely applied to purify waste liquids generated during the operationof nuclear reactors. The radioactive nuclides 60Co and 58Co are important corrosion activation products inreactor cooling water. In this study, the simulated Co doped CERs were oxidized with ternary carbonate. According to the thermogravimetric analysis (TG), the decomposition of Co doped CERs includes threeprocesses: 1. Elimination of the osmotic water; 2. Pyrolysis of sulfonic acid group; 3. Destruction of styrene–divinylbenzene copolymer. The X-Ray Diffraction (XRD) patterns indicate that sulfur mainly exists inthe form of sulfate in waste salt. The Co2+ undergoes the path of CoS2 ? Co3O4 with the increase of temperatureand the transition point is 650 C. Combined with Fourier Transform Infrared Spectrometer (FTIR)spectra and X-ray Photoelectron Spectroscopy (XPS) analysis, sulfonic acid groups begin to decomposeat 350 C. During the molten salt oxidation process, most of the sulfur in sulfonic acid groups is entrappedby carbonate as the form of sulfate, and a little of which remains as sulfone group, sulfoxide group andsulfur bridge in residue. When the resins are oxidized at 800 C, the retention rate of Co2+ is 97.3%, indicatingthat the molten salt oxidation can effectively remain Co2+ and convert it into a more stablesubstance.
Xin Liu,Zi-Yu Liu,Yang-Hai Zheng,Yong-De Yan,Wen-Da Xu,Yun Xue,Yue-Lin Wang,Fu-Qiu Ma,Kai Zhu,Yu-Sheng Yang 한국공업화학회 2023 Journal of Industrial and Engineering Chemistry Vol.120 No.-
The disposal of spent radioactive ion exchange resin generated during the operation of nuclear facilitieshas always been a conundrum. The molten salt oxidation (MSO) for the treatment of mixed resin (MR)shows obvious superiority. In this work, ternary carbonate (Li2CO3-Na2CO3-K2CO3) and MR was usedas the molten salt system and the oxidation target, respectively. The oxidation behavior of MR was analyzedby varying the temperature and oxygen equivalent during the MSO process. By studying the effectof different oxygen equivalents on the oxidation efficiency, the oxygen equivalent of 125% could make theoxidation efficiency of MR reach 99.99% at 800 C. The composition of C, N and S containing exhaust gasproduced through MSO process of MR with temperature were almost consistent with the simulationresults. The exhaust gas was successfully adsorbed by molten carbonate to produce nitrate and sulfurcompounds. The carbonate has good absorption to harmful gases such as SO2, CO, NO, etc. The contentof SO2 from the highest 0.32% to 0, and 71.23% of sulfur in MR was trapped by molten carbonate asthe form of sulfate. This work has important implications for reducing the potential harm of radioactivewaste resin to the environment.