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- 저자 : Feichao Zhu (검색결과 3 건)
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Fabrication of recyclable UiO-66-NH2/PVDF hybrid fibrous membrane for Cr(VI) removal in wastewater
Fan Yu,Liusha Cen,Caihong Lei,Feichao Zhu,Lan Zhou,Hailin Zhu,Bin Yu 한국공업화학회 2023 Journal of Industrial and Engineering Chemistry Vol.123 No.-
Efficient and recyclable water treatment technology plays a vital role in practical application of Cr(Ⅵ)removal. Zr-based metal–organic framework (UiO-66-NH2) is widely used in wastewater treatmentdue to its water stability. Powdery UiO-66-NH2 has disadvantages of easy aggregation, reclamation difficultyand secondary pollution. In this work, UiO-66-NH2 was successfully loaded on electrospunpolyvinylidene fluoride (PVDF) fibers by in-situ growth to achieve efficient adsorption and photoreductionof Cr(Ⅵ). Grooved surface of PVDF fibers and truncated octahedron shape of UiO-66-NH2 ensuredthe loading uniformity and firmness. The loading rate and size of UiO-66-NH2 crystals increased withthe amount of trifluoroacetic acid (TFA) in the preparation process. Meantime, the introduction of TFAin synthesis was conducive to the separation efficiency of photogenerated carries. When the additionamount of TFA was 5 ml, UiO-PVDF-3 with loading rate of 44.8% exhibited best Cr(VI) adsorption andphotocatalysis performance. For the pure adsorption process, the adsorption capacity of UiO-PVDF-3 at90 min was 3.76 mg/cm2, and the corresponding removal rate was 95.8%. When visible light was applied,the Cr(VI) removal rate for UiO-PVDF-3 reached to about 95.0% at 45 min. Furthermore, regenerationexperiments showed UiO-PVDF-3 had excellent adsorption and photocatalysis reusability. Based on thismethod, synthesized UiO-66-NH2/PVDF hybrid membrane as a bifunctional material for adsorption andphotocatalysis realizes the reuse of UiO-66-NH2 crystals conveniently and avoids secondary pollutionduring Cr(VI) wastewater treatment.
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Effect of PCL and Compatibilizer on the Tensile and Barrier Properties of PLA/PCL Films
Hui Sun,Aiju Xiao,Bin Yu,Gajanan Bhat,Feichao Zhu 한국고분자학회 2017 폴리머 Vol.41 No.2
In this work, the blend films of poly(lactic acid) (PLA) and poly(ε-caprolactone) (PCL) were prepared by the solvent casting method. The influence of PCL content and compatibilizer on the structure, tensile and barrier properties was studied. The results indicated that PCL showed good dispersion in PLA matrix as tributyl citrate (TBC) was added as a compatibilizer. PCL showed a promotion effect on the crystallinity of PLA/PCL films. The compatibility of PLA and PCL was improved by TBC. The tensile modulus and the elongation at break of PLA/PCL films increased to various extents due to the input of PCL and TBC compared to pure PLA film. The improvement of oxygen and water vapor barrier properties of the blend films were provided and depended on the content of PCL and the appearance of TBC. The transparency of the blend films decreased with the increase of the PCL content.
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멜트블론 부직포 제조를 위한 PLA/PCL 블렌드의 미세구조,열적특성, 및 유변학적 성질
Hui Sun,Bin Yu,Jan Han,Jinjin Kong,Lingrui Meng,Feichao Zhu 한국고분자학회 2014 폴리머 Vol.38 No.4
Poly(lactic acid)(PLA)and poly(εcaprolactone) (PCL) blends with various components for melt-blown non-wovens were prepared by a twin-screw extruder. Tributyl citrate (TBC) was added in order to improve the miscibility between PLA and PCL. The results showed that small circular particles of PCL were dispersed in PLA matrix aniformly. The addition of PCL had the heterogeneous nucleation effect on the crystallization of PLA and decreased thermal stability of PLA. The flow of pure PLA and blends approached to Newtonian liquid at a low shear rate and expressed more obvi-ous viscoelasticity at a high shear rate.
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