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크롬염화물 첨가에 따른 지르코니아 색상 및 물리적 성질 변화에 관한 연구
오계정,서윤정,윤귀덕,임현필,박상원,이경구,임태관,이도재,Oh, Gye-Jeong,Seo, Yoon-Jeong,Yun, Kwi-Dug,Lim, Hyun-Pil,Park, Sang-Won,Lee, Kyung-Ku,Lim, Tae-Kwan,Lee, Doh-Jae 대한치과보철학회 2011 대한치과보철학회지 Vol.49 No.2
연구 목적: 본 연구의 목적은 색소체인 크롬염화물을 지르코니아에 첨가함으로써 지르코니아의 색상 및 물리적 성질, 그리고 미세구조가 어떻게 변화하는지 알아보고자 한다. 연구 재료 및 방법: 크롬염화물의 함량이 지르코니아 분말에 각각 0.06, 0.12, 0.25 wt%가 되도록 측량하고 알코올에 녹여 액상상태의 크롬염화물을 준비하였다. 지르코니아 분말과 각각의 액상상태의 크롬염화물을 혼합하고 혼합된 분말을 이용하여 디스크형태의 지르코니아 시편을 제작하였다. 제작된 시편은 $1450^{\circ}C$에서 완전소결 후 색상 및 물리적 성질, 그리고 미세구조를 관찰하였다. 색상은 분광측색장치를 이용하여 국제조명위원회 (CIE) ISO 기준인 D65 광원, SCE 방식으로 측정하여 $L^*$, $C^*$, $a^*$, $b^*$ 값으로 분석하였다. 밀도는 아르키메데스 법으로 측정하였고, 주사전자현미경과 X선 회절 분석기를 이용하여 시편의 미세구조 및 결정상을 관찰하였다. 파괴인성은 압흔 형성법(Vickers indentation법)을 이용하여 시편에 압흔 형성 후, 광학현미경으로 압흔의 크기를 측정하고 이를 이용하여 파괴인성을 구하였다. 결과는 일원배치분산분석 (one-way ANOVA)으로 통계처리 하였고, Tukey test로 사후 검정하였다. 결과: 1. 크롬염화물을 첨가하여 지르코니아의 색상을 조절할 수 있음을 확인하였으며, 크롬염화물 첨가 함량이 증가함에 따라 지르코니아 색상은 백색계통의 갈색에서 짙은 색의 갈색으로 변하였다. 2. 크롬염화물의 첨가는 시편의 밀도를 점점 감소시켰으며, 크롬염화물이 첨가되지 않은 시편과 비교 시, 크롬염화물의 첨가량이 증가할수록 통계학적으로 유의한 차이를 보였다 (P<.05). 3. 크롬염화물이 첨가된 시편은 첨가되지 않는 시편에 비해 결정립 크기가 증가하였다. 4. X-선 회절 분석결과, 크롬염화물의 첨가 여부와 첨가 함량에 상관없이 지르코니아 결정상의 차이점은 관찰되지 않았다. 5. 지르코니아에 크롬염화물을 첨가 시 크롬염화물의 첨가 함량에 따라 파괴인성값은 감소하였고, 특히 0.25 wt%의 크롬염화물을 첨가 시 가장 낮은 파괴인성 값을 보였다 (P<.05). 결론: 이상의 결과로 크롬염화물을 액체상태로 첨가하여 지르코니아의 색상을 조절할 수 있음을 확인하였으며, 제작한 유색 지르코니아의 색상은 자연치아 색상과 다소 차이가 있지만, 본 소재는 임상에서 사용되는 완전도재관 코어 (Core) 재료로써 사용할 수 있을 것으로 생각한다. Purpose: The purpose of this study was to examine the effects of chromium chloride addition on coloration, mechanical property and microstructure of 3Y-TZP. Materials and methods: Chromium chloride was weighed as 0.06, 0.12, and 0.25 wt% and each measured amount was dissolved in alcohol. $ZrO_2$ powder was mixed with each of the individual slurry to prepare chromium doped zirconia specimen. The color, physical properties and microstructure were observed after the zirconia specimen were sintered at $1450^{\circ}C$. In order to evaluate the color, spectrophotometer was used to analyze the value of $L^*$, $C^*$, $a^*$ and $b^*$, after placing the specimen on a white plate, and measured according to the International Commission on Illumination (CIE) standard, Illuminant D65 and SCE system. The density was measured in the Archimedes method, while microstructures were evaluated by using the scanning electron microscopy (SEM) and XRD. Fracture toughness was calculated Vickers indentation method and indentation size was measured by using the optical microscope. The data were analyzed with 1-way ANOVA test (${\alpha}$ = 0.05). The Tukey multiple comparison test was used for post hocanalysis. Results: 1. Chromium chloride rendered zirconia a brownish color. While chromium chloride content was increased, the color of zirconia was changed from brownish to brownish-red. 2. Chromium chloride content was increased; density of the specimen was decreased. 3. More chromium chloride in the ratio showed increase size of grains. 4. But the addition of chromium chloride did not affect the crystal phase of zirconia, and all specimens showed tetragonal phase. 5. The chromium chloride in zirconia did not showed statistically significant difference in fracture toughness, but addition of 0.25 wt% showed a statistically significant difference (P<.05). Conclusion: Based on the above results, this study suggests that chromium chlorides can make colored zirconia while adding in a liquid form. The new colored zirconia showed a slight difference in color to that of the natural tooth, nevertheless this material can be used as an all ceramic core material.
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서윤정,오계정,이효일,신유진,김홍주,박상원,Seo, Yoon-Jeong,Oh, Gye-Jeong,Lee, Hyo-Il,Shin, Yoo-Jin,Kim, Hong-Joo,Park, Sang-Won 대한치과보철학회 2013 대한치과보철학회지 Vol.51 No.4
연구 목적: 본 연구는 납형의 크기 및 형태 변화가 티타늄의 주조성에 어떠한 영향을 미치는지 확인하고자 하였다. 연구 재료 및 방법: 납형의 크기에 따라 Small Pattern군과 Large Pattern군으로 나누었고, 각각 Flat, Semicircular, Horse-shoe 및 V-shape형으로 납형의 형태에 따라 4개의 하위군으로 나누어 총 8개의 군으로 분류하였다. 모든 납형의 주입선은 Runner-bar형으로 하였다. 티타늄 주조 전용 매몰재인 실리카계 매몰재(Rematitan Plus$^{(R)}$, Dentarum, Germany)를 이용하여 매몰하였고, 아크용융 방식의 원심 주조기(Ti Cast Super R$^{(R)}$, Selec, Japan)를 사용하여 주조하였다. 주조성 평가는 완전한 형태로 주조 된 격자의 개수를 척도로 재현 정도를 확인하였다. 통계처리는 SPSS ver. 19.0 for WIN (SPSS. Inc. Chicago, IL, USA)를 사용하였다. 납형의 크기 및 형태에 따른 티타늄의 주조성을 이원변량 분산분석(Two-way ANOVA)을 이용하여 분석하였다. 결과:납형의 평균 재현율은 Small Pattern군은 95.14%, Large Pattern군은 94.30%로 Small Pattern군의 주조성이 유의하게 높았다(P<.05). 납형의 형태 변화에 따른 주조성은 Small Pattern군에서 Semicircular군 133.20개(96.52%), Horse-shoe군 132.40개(95.94%), Flat군 132.00개(95.65%), V-shape군 127.60개(92.46%) 순으로 감소하였다. Large Pattern군은 Flat군 198.60개(95.94%), V-shape군 197.80개(95.56%), Semicircular군 196.40개(94.88%), Horse-shoe군 188.00개(90.82%)순으로 감소하였다. Small Pattern군과 Large Pattern군 모두에서 납형의 형태변화에 따른 주조성은 유의할 만한 차이를 보이지 않았다(P>.05). 결론:주조체의 크기가 작을수록 주조성이 높아짐을 알 수 있었고 형태에 따른 주조성에서는 큰 영향을 받지 않는 것을 알 수 있었다. Purpose: The purpose of this study was to investigate the effect of geometrically different wax pattern shapes and sizes on the castability of Grade2 Cp-Ti (commercially pure titanium). Materials and methods: Total of 40 mesh wax pattern ($61mm{\times}24mm$, 207 grids), ($61mm{\times}17mm$, 138 grids) was cast in this experiment. Depending on the geometrical shape of the wax pattern, 8 groups was organized; Flat, Semicircular, Horse-shoe and V-shape, each consisting 5 samples. Runner-bar sprue was used in all patterns. The number of completely cast grid in wax pattern served as a measure for the castability of comercially pure titanium. Results: The mean value of square count in each group was as followed; 133.20 squares in group SS (96.52%), 132.40 squares in group SH (95.94%), 132.00 squares in group SF (95.65%), 127.60 squares in SV (91.43%), 198.60 squares in group LF (95.94%), 197.80 squares in group LV (95.56%), 196.40 squares in group LS (94.88%), and 188.00 squares in group LH (90.82%). Conclusion: Within the limitations of this study the results indicate that there were no sttistically significant difference in castability of titanium regarding wax pattern shape (P>.05). However, Small size wax patterns were showing the noticeable castability more than Large size pattern.
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한국 유치악 성인의 상악 중절치 위치 및 견치간 거리에 관한 연구
양동헌,이지윤,반재삼,오계정,박상원,Yang, Dong-Hun,Lee, Jee-Yun,Ban, Jae-Sam,Oh, Gye-Jeong,Park, Sang-Won 대한치과보철학회 2013 대한치과보철학회지 Vol.51 No.3
연구 목적: 이 연구는 정상배열을 가지고 있는 한국 유치악 성인에서 얼굴형과 성별에 따라 절치유두를 기준으로 한 상악전치의 위치와 견치폭경 계측치를 제시한다. 연구 대상 및 방법: 전남대학교 치의학 전문대학원에 다니는 학생 중 crowding 및 spacing이 없으며, Angles Class I의 정상 교합관계를 가지고 있는 42명을 대상으로 조사하였다. 선정된 학생들의 두부 측면 방사선 사진을 찍고, posterior facial height (PFH)과 anterior facial height (AFH)을 측정하여 PFH / AFH%를 구하여 cephalic type을 나누었다. 그 후 42명의 상악 모형을 준비하여 버니어캘리퍼스로 상악 중절치 절단연에서 절치 유두 중앙까지의 수평거리(A)와 상악 견치간 거리(B)를 계측, 평균값을 구하였으며, SPSS version 15를 사용하여 통계분석 및 유의성을 검토하였다. 결과: Dolichocephalic type을지닌10명에서A의 평균값은 $8.43{\pm}0.61$, B의 평균값은 $36.73{\pm}2.17$으로 나타났다. Mesocephalic type과 brachycephalic type의경우각각A의평균값은 $8.51{\pm}1.27$, $8.76{\pm}1.03$, B의 평균값은 $35.91{\pm}1.86$, $37.34 {\pm}2.23$로 나타났다. 성별에 따른 계측 결과 남성에서A의 평균값은 $8.86{\pm}1.04$, B의 평균값은 $37.60{\pm}0.24$으로 나타났으며, 여성에서A의 평균값은 $8.41{\pm}0.93$, B의 평균값은 $36.18{\pm}2.01$로 나타났다. A값의 경우 남성이 여성보다 큰 값을 보였으나 그 차이는 통계적으로 유의하지 않았다(P>.05). B값의 경우 남성이 여성보다 큰 값을 보였으며, 통계적으로 유의성을 나타내었다 (P<.05). 결론:한국에서 정상 치열 및 교합을 가진 평균 연령 30세, 42명의 학생을 대상으로 조사하였을 때, 절치유두에서 상악 중절치 절단연까지의 수평 거리는 cephalic type이나 성별에 따른 차이가 없었고, 견치 교두정간 거리는 cephalic type에 따른 차이가 없었지만, 성별에 따라 유의한 차이를 보였으며 남성이 여성보다 큰 값을 나타냈다. Purpose: The aim of this study was to propose the position of maxillary anterior teeth and intercanine width measurements based on the incisive papilla in accordance with the cephalic type and gender of dentate Korean adult with normal teeth alignment. Materials and methods: 42 students with Class I normal occlusion, without crowding or spacing, were selected from the Chonnam National University School of Dentistry. The lateral skull radiographs of the subjects were taken and were classified as different cephalic types, based on their PFH / AFH ratios. 42 casts of their maxilla were prepared and both the distance between the upper central incisors and the middle of the incisor papilla was measured with a vernier caliper (A) and the distance between the maxillary canine cusp tips (B) were measured. Statistical analysis was performed using SPSS version 15 and their significance was investigated. Results: For dolichocephalic group, the mean values for A and B were 8.43 (SD: 0.61) and 36.73 (SD: 2.17), respectively. The mean value for A was 8.51 (SD: 1.27) for the mesocephalic group and 8.76 (SD 1.03) for the brachycephalic group. The mean value for B was 35.91 (SD: 1.86) for the mesocephalic group and 37.34 (SD: 2.23) for the brachycephalic group. For the male group, the mean A value was 8.86 (SD: 1.04) and the mean B value was 37.60 (SD: 0.24). For the female group, the mean A value was 8.41 (SD: 0.93) and the mean B value was 36.18 (SD: 2.01). The difference between male and female group in A values were not statistically significant (P>.05). The B values of the male subjects were greater than those of the female subjects and was statistically significant (P<.05). Conclusion: 42 students with normal dentition and occlusion in korea, the distance from the incisive papilla and the incisal edge of maxillary central incisors had no difference in cephalic type or gender. However, the distance between the cusp tip of both canines had significant difference in gender where the male showed higher values than the female, while having no difference in cephalic types.
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김연미,김현승,이광민,이도재,오계정,임현필,서윤정,박상원,Kim, Yeon-Mi,Kim, Hyun-Seung,Lee, Kwang-Min,Lee, Doh-Jae,Oh, Gye-Jeong,Lim, Hyun-Pil,Seo, Yoon-Jung,Park, Sang-Won 대한치과보철학회 2007 대한치과보철학회지 Vol.45 No.5
Statement of problem: The adhesion between titanium and ceramic is less optimal than conventional metal-ceramic bonding, due to reaction layer form on cast titanium surface during porcelain firing. Purpose: This study characterized the effect of titanium-ceramic adhesion after gold and TiN coating on cast and wrought titanium substrates. Material and method: Six groups of ASTM grade II commercially pure titanium and cast titanium specimens$(13mm{\times}13mm{\times}1mm)$ were prepared(n=8). The conventional Au-Pd-In alloy served as the control. All specimens were sandblasted with $110{\mu}m\;Al_2O_3$ particles and ultrasonically cleaned for 5min in deionized water and dried in air before porcelain firing. An ultra-low-fusing dental porcelain (Vita Titankeramik) was fused on titanium surfaces. Porcelain was debonded by a biaxial flexure test at a cross head speed of 0.25mm/min. The excellent titanium-ceramic adherence was exhibited by the presence of a dentin porcelain layer on the specimen surface after the biaxial flexure test. Area fraction of adherent porcelain (AFAP) was determined by SEM/EDS. Numerical results were statistically analyzed by one-way ANOVA and Student-Newman-Keuls test at ${\alpha}=0.05$. Results: The AFAP value of cast titanium was greatest in the group 2 with TiN coating, followed by group 1 with Au coating and the group 3 with $Al_2O_3$ sandblasting. Significant statistical difference was found between the group 1, 2 and the group 3 (p<.05). The AFAP value of wrought titanium was greatest in the group 5 with TiN coating, followed by the group 4 with Au coating and the group 6 with $Al_2O_3$ sandblasting. Conclusion: No significant difference was observed among the three groups (p>.05). The AFAP values of the cast titanium and the wrought titanium were similar. However the group treated with $Al_2O_3$ sandblasting showed significantly lower value (p<.05).
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최택휴,박상원,방몽숙,양홍서,박하옥,임현필,오계정,김현승,이광민,이경구,Choi, Taek-Huw,Park, Sang-Won,Vang, Mong-Sook,Yang, Hong-So,Park, Ha-Ok,Lim, Hyun-Pil,Oh, Gye-Jeong,Kim, Hyun-Seung,Lee, Kwang-Min,Lee, Kyung-Ku 대한치과보철학회 2007 대한치과보철학회지 Vol.45 No.2
Statement of problem: Titanium is well known as a proper metal for the dental restorations, because it has an excellent biocompatibility, resistance to corrosion, and mechanical property. However, adhesion between titanium and dental porcelains is related to the diffusion of oxygen to the reaction layers formed on cast-titanium surfaces during porcelain firing and those oxidized layers make the adhesion difficult to be formed. Many studies using mechanical, chemical and physical methods to enhance the titanium-ceramic adhesion have been actively performed. Purpose: This study meant to comparatively analyse the adhesion characteristics depending on different titanium surface coatings after coating the casts and wrought titanium surfaces with Au and TiN. Material and method: In this study, the titanium specimens (CP-Ti, Grade 2, Kobe still Co. Japan) were categorized into cast and wrought titanium. The wrought titanium was cast by using the MgO-based investment(Selevest CB, Selec). The cast and wrought titanium were treated with Au coating($ParaOne^{(R)}$., Gold Ion Sputter, Model PS-1200) and TiN coating(ATEC system, Korea) and the ultra low fusing dental porcelain was fused and fired onto the samples. Biaxial flection test was done on the fired samples and the porcelain was separated. The adhesion characteristics of porcelain and titanium after firing and the specimen surfaces before and after the porcelain fracture test were observed with SEM. The atomic percent of Si on all sample surfaces was comparatively analysed by EDS. In addition, the constituents of specimen surface layers after the porcelain fracture and the formed compound were evaluated by X-ray diffraction diagnosis. Result: The results of this study were obtained as follows : 1. The surface characteristics of cast and wrought titanium after surface treatment(Au, TiN, $Al_2O_3$ sandblasting) were similar and each cast and wrought titanium showed similar bonding characteristics. 2. Before and after the biaxial flection test, the highest atomic weight change of Si component was found in $Al_2O_3$ sandblasted wrought titanium(28.6at.% $\rightarrow$ 8.3at.%). On the other hand, the least change was seen in Au-Pd-In alloy(24.5at.% $\rightarrow$ 9.1at.%). 3. Much amount of Si components was uniformly distributed in Au and TiN coated titanium, but less amount of Si's was unevenly dispersed on Al2O3 sandblasting surfaces. 4. In X-ray diffraction diagnosis after porcelain debonding, we could see $Au_2Ti$ compound and TiN coating layers on Au and TiN coated surfaces and $TiO_2$, typical oxide of titanium, on all titanium surfaces. 5. Debonding of porcelain on cast and wrought titanium surface after the biaxial flection is considered as a result of adhesion deterioration between coating layers and titanium surfaces. We found that there are both adhesive failure and cohesive failure at the same time. Conclusion: These results showed that the titanium-ceramic adhesion could be improved by coating cast and wrought titanium surfaces with Au and TiN when making porcelain fused to metal crowns. In order to use porcelain fused to titanium clinically, it is considered that coating technique to enhance the bonding strength between coating kKlayers and titanium surfaces should be developed first.
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타이타늄 표면 코팅 처리에 따른 타이타늄도재관의 파절강도 비교
김지혜,박상원,방몽숙,양홍서,박하옥,임현필,오계정,김현승,이광민,이경구,Kim, Ji-Hye,Park, Sang-Won,Vang, Mong-Sook,Yang, Hong-So,Park, Ha-Ok,Lim, Hyun-Pil,Oh, Gye-Jeong,Kim, Hyun-Seung,Lee, Kwang-Min,Lee, Kyung-Ku 대한치과보철학회 2007 대한치과보철학회지 Vol.45 No.2
Statement of problem: Titanium and its alloy, with their excellent bio-compatibility and above average resistance to corrosion, have been widely used in the field of dentistry. However, the excessive oxidization of titanium which occurs during the process of firing on porcelain makes the bonding of titanium and porcelain more difficult than that of the conventional metal-porcelain bonding. To solve this problem related to titanium-porcelain bonding, several methods which modify the surfaces, coat the surfaces of titanium with various pure metals and ceramics, to enable the porcelain adhesive by limiting the diffusion of oxygen and forming the adhesive oxides surfaces, have been investigated. Purpose: The purpose of this study was to know whether the titanium-porcelain bonding strength could be enhanced by treating the titanium surface with gold and TiN followed by fabrication of clinically applicable porcelain-fused-to-titanium crown Material and method: The porcelain-fused-to-titanium crown was fabricated after sandblasting the surface of the casting titanium coping with $Al_2O_3$ and treating the surface with gold and TiN coating followed by condensation and firing of ultra-low fusing porcelain. To compare with porcelain-fused-to-titanium crowns, porcelain-fused-to-gold crowns were fabricated and used as control groups. The bonding strengths of porcelain-fused-to-gold crowns and porcelain-fused-totitanium crowns were set for comparison when the porcelain was fractured on purpose to get the experimental value of fracture strength. Then, the surface were examined by SEM and each fracturing pattern were compared with each other Result:Those results are as follows. 1. The highest value of fracture strength of porcelain-fused-to-titanium crowns was in the order of group with gold coating, group with TiN coating, group with $Al_2O_3$ sandblasting. No statistically significant difference was found among the three (P>.05). 2. The porcelain-fused-to-gold crowns showed the highest value in bonding strength. The bonding strength of crowns porcelain-fused-to-titanium crowns of rest groups showed bonding strength reaching only 85%-94% of that of PFG, though simple comparision seemed unacceptable due to the difference in materials used. 3. The fracturing patterns between metal and porcelain showed mixed type of failure behavior including cohesive failure and adhesive failure as a similar patterns by examination with the naked eye and SEM. But porcelain-fused-to-gold crowns showed high incidence of adhesive failure and porcelain-fused-to-titanium crowns showed high incidence of cohesive failure. Conclusion: Above results proved that when fabricating porcelain-fused-to-titanium crowns, treating casting titanium surface with gold or TiN was able to enhance the bonding strength between titanium and porcelain. Mean value of masticatory force was found to showed clinically acceptable values in porcelain bonding strength in all three groups. However, more experimental studies and evaluations should be done in order to get better porcelain bonding strength and various surface coating methods that can be applied on titanium surface with ease.
RISS
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