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한약재중의 잔류농약 분석 - GC에 의한 18종 잔류농약의 분석 -
황인숙,최병현,배청호,김명희,조해전,Hwang, In-Sook,Choi, Byung-Hyun,Bae, Chong-Ho,Kim, Myung-Hee,Cho, Hae-Jeon 한국생약학회 2001 생약학회지 Vol.32 No.3
This study was carried out to determine the 11 organochlorine, 7 organophosphorus residual pesticides in 251 crude drugs. These residual pesticides in herbal drugs were extracted with acetonitrile and the extracts were cleaned up via LC-florisil solid phase extraction column. The prepared samples were assayed for pesticide residues using GC-ECD, NPD with capillary column and identified by GC-MSD. Recoveries were $63.9{\sim}111.5%$ in the organochlorine pesticides and $69.8{\sim}92.4%$ in the organophosphorus pesticides, and detection limits were $0.001{\sim}0.65\;ppm$ in the organochlorine pesticides and $0.0009{\sim}0.0074\;ppm$ in the organophosphorus pesticides. Pesticide residues were detected in 9 cases.
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박건용,김애경,박경애,정보경,배청호,김명희 한국식품위생안전성학회 2003 한국식품위생안전성학회지 Vol.18 No.1
튀김닭 전문점의 튀김조건 및 소비자에 대한 기호도 조사와 튀김닭에 사용하는 식용유지의 산패와 관하여 연구한 결과는 다음과 같다. 1. 튀김닭 전문점에서의 닭의 튀김조건을 조사한 결과 사용유지는 주로 콩기름이었으며 튀김온도는 170-180℃, 튀김시간은 10-15분, 튀김유 교체는 30번 정도 튀긴 후에 이루어지는 것으로 조사되었다. 2. 튀김닭에 대한 소비자 기호도 조사를 실시한 결과를 보면 응답자 중 76.2%가 ‘튀김유가 유해할 것이다’라고 생각하고 있었으며 신선도를 유지하기 위해서는 튀김유를 매일 교체해야 한다(50.8%)고 생각하고 있으나 업체에서는 3-4일 정도는 사용할 것이다(37.3%) 라는 추측을 갖고 있는 것으로 조사되었다. 3. 튀김닭 전문점의 튀김조건에 맞춰 닭을 튀겨 튀김횟수에 따른 변화를 측정한 결과 AV 및 POV는 같은 기름으로 30번 정도를 튀겼을 때 그 값이 약간씩은 증가했으나 튀김식품의 기준치에는 미치지 못하는 값으로 튀김유의 산패진행이 많지 않음을 알 수 있었다. 4. 닭을 1일 3회씩 10일간을 튀겨 튀김일수에 따른 산패의 변화를 알아본 결과 어느 정도의 산패가 진행되고 있었으나 그 진행의 수준은 낮은 편이었다. 5. 생닭의 경우 보관기간에 따라 AV가 높게 증가하여 닭의 신선도가 튀김유의 산패에 많은 영향을 주고 있었으며 튀김시 생닭의 선택에 주의를 기울여야 할 것이다. This study was performed to investigate the condition of frying at fried chicken shop, taste and thinking refer to fried chicken in the consumer. The acidification of frying oil was determined as acid value, peroxide value and fatty acid composition. The results were as follows: 1) Soybean oil was used for frying at a fried chicken shop at 170-180℃ for 10-15 min and replaced by every thirty cycles. 2) 76.2% of the consumer among answeres for the question thought that the oil of frying could be harmful to health. 3) The AV and POV were increased while chickens were fried after thirty cycles successively, but the values were lower than a standard level of fried-food. 4) The acidification of fried oil was in progress when chickens were fried for ten days by three times a day, but the value was low. 5) The AV of raw chicken was significantly increased as time goes, suggesting that a fresh chicken should be chosen.
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HPLC-MS/MS를 이용한 어린이 기호식품중의 감미료 분석
김일영,두옥주,이성득,박영혜,김미선,배청호,채영주 한국식품위생안전성학회 2010 한국식품위생안전성학회지 Vol.25 No.2
A HPLC-MS/MS method was developed for simultaneous determination of six sweeteners (acesulfame-K, cyclamate, saccharin, sucralose, stevioside, aspartame) in children's favorite foods. The procedure involves an extraction of the six sweeteners with 50% methanol solution, sample clean-up using the Carrez clearing reagent and filtering with cartridge filter. The HPLC separation was performed on a Hypersil Gold (150 mm × 2.1 mm 5 um) column using the water/acetonitrile mobile phase (95:5). Mass spectrometric analysis was carried out using the TSQ Quantum Ultra operated in negative and positive ESI/SRM. With this method, good linear relationship, sensitivity and reproducibility were obtained. The spike recoveries of six sweeteners for 2 kinds of foods spiked into 0.4 mg/kg ranged from 87.4 to 114.7%. The detection limits were above 0.02 mg/kg. The method has been applied to determination of six sweeteners in children's favorite foods.
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박건용,정보경,김애경,박경애,조성자,곽재은,장민수,배청호,조남준 한국식품위생안전성학회 2004 한국식품위생안전성학회지 Vol.19 No.2
This study was performed to investigate 172 samples of fried food in fast food store. The free fatty acid value of 22 samples exceeded standard of fried-food. These samples were 10 fried chickens, 6 fried potatoes and 5 fried onions. Fatty acid composition differed from each company. The correlation between free fatty acid value and double bond index was very low. New standard of fried food in fast food store is needed for thorough hygiene management, because of being not existed standard. The fried potato containing many carbohydrate and fat appeared higher calory than fried chicken containing many protein. The fried food had high fat comparatively, so that attention in regard to excess intake is demanded. The trace materials were included Mg, Ca, Mn, Fe, Zn, Cu and Cr in order of quantity, and the harmful heavy metals - Pb, Hg and Cd - were included small quantity.
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