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전기화학적으로 제조한 CoPtP-X합금의 첨가제 효과에 따른 맞춤형 자기적 성질
박호동,이관희,김긍호,정원용,최동훈,이우영,Park, H.D.,Lee, K.H.,Kim, G.H.,Jeung, W.Y.,Choi, D.H.,Lee, W.Y. 한국전기화학회 2005 한국전기화학회지 Vol.8 No.2
본 연구에서는 CoPtP합금에 첨가원소로 Fe, Mn을 첨가하여 그에 따른 자기적 성질을 제어하고자 하였다. 우선 합금을 합성하기 위해서 용액 중 Fe, Mn의 농도를 변화시키면서 전기도금 방식을 이용하여 CoPtP-X (X=Fe, Mn) 합금을 제조하였다 Fe를 첨가한 합금박막에서는 X선 회절분석 견과 Fe함량이 증가함에 따라 CoPtP합금의 수직방향으로의 우선결정방향이 조밀육방정 [001]방향에서 [100] 방향으로 변화함을 관찰하였고, 이에 따라 결정 자기이방성이 변화하여 전형적인 경자성 특성에서 연자성 특성까지 자기적 특성을 제어할 수 있었다. 용액 중 첨가된 망간의 농도를 변화시켜 제조된 CopPtP-Mn 합금박막에서는 Mn의 농도가 0.0126M일 때 보자력(coercivity)과 각형비(squareness, Mr/Ms)가 각각 4630 Oe, 0.856의 매우 우수한 자기적 성질을 나타내었으며, 이는 Mn의 특정농도에서 CoPtP 합금박막의 우선결정 성장방향인 조밀육방정 c축이 박막면에 대하여 수직하게 놓이는 현상에서 기인된다는 것을 투과전자현미경 분석을 통해 확인하였다. Coptp films with the additive elements (X=Fe, Mn) of varying concentrations were prepared by in-situ electrodeposition, to tailor their magnetic properties. Alloys of CoPtP-X (X=Fe, Mn) were synthesized by changing the solution concentrations of Fe and Mn for electrodeposition. In the electrodeposited CoFePtP alloys, preferred orientation of the electrodeposited films changed from hexagonal (001) to (100) direction with increasing iron contents as revealed by X-ray diffraction, and these films exhibited various magnetic properties ranging from a typical hard magnetic to a soft magnetic property in accordance with microstructural variations. In the case of Mn addition, excellent hard magnetic property was observed at a specific Mn concentration of 0.0126 M in the electrolyte, with the coercivity of 4630 Oe and squareness of 0.856 and this was attributed to the fact that magnetization easy-axis (hexagonal c-axis) coincides with the preferred growth orientation of the film confirmed by transmission electron microscopy.
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전기도금 시 외부자기장이 CoPtP 합금의 자기 특성에 미치는 영향
정원용(W. Y. Jeung),박호동(H. D. Park) 한국자기학회 2005 韓國磁氣學會誌 Vol.15 No.5
We have investigated the effects of an external magnetic field on the growth direction and the grain size of electrochemically prepared CoPtP alloys. Electrodeposited CoPtP alloys were synthesized by appling an external magnetic field with 0 to 1 T to the perpendicular direction of the films. In the electrodeposited CoPtP alloys without external magnetic field, the growth direction of the alloys was mixed by fcc (111) and hcp (002), but only hcp (002) was observed in the alloys with 1 T external magnetic field. CoPtP alloys were grown as the columnar growth and the grain size increases with growing the alloys. With appling an external field, the grain size of the alloys was controlled less than 20 ㎚ which is smaller than single domain of Co, and the easy axis of alloys, hcp (002) direction, was grown perpendicular to the films up to 200 ㎚. We could obtain the optimal thickness of the alloys and electrodeposition condition from the above results. Coercivity and squareness of CoPtP alloys taken out-of-plane are 6.1 kOe and 0.9, respectively. The magnetic properties of CoPtP alloys were measured by VSM, and the microstructural characterization and crystalline orientation measurement of the alloys were carried out by TEM and XRD.
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김유일(Y.I. Kim),김귀순(K.S. Kim),김경천(K.C. Kim),하만영(M.Y. Ha),박호동(H.D. Park) 한국전산유체공학회 1995 한국전산유체공학회 학술대회논문집 Vol.1995 No.-
A computer code for solving the Reynolds averaged full Navier-Stokes equations has been developed for analysis of gas and steam turbine cascade flows with the option of using one of two types of turbulence model. One is the Baldwin-Lomax model and the other is standard k-ε model. The numerical integration is based on the explicit four stage Runge-Kutta scheme and finite volume method. To be verified, the resulting code is applied to VKI turbine cascade and compared with the previous experimental results. Finally, the flowfield around a steam turbine cascade is analyzed. Comparisons with experimental data show that present numerical scheme is an accurate Navier-Stokes solver and can give very good predictions for both gas and steam turbine cascade flow.
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