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류재정,홍종기,김세훈,도환석,홍무기,Young Han Jeong,Jeong Eun Ryu,Hae Young Kwon,Ji Yoon Jeong,Hye Jin Park,Soon Ho Lee 대한화학회 2008 Bulletin of the Korean Chemical Society Vol.29 No.5
Simultaneous determination of amitraz, bromopropylate, coumaphos, cymiazole and 2,4-dimethylaniline in 200 honey samples purchased in Korea was performed by reversed-phase high-performance liquid chromatography with multiple UV detection. 2% Acetone in hexane was used for a liquid-liquid extraction and 20-40% water in acetonitrile solutions were used as mobile phases. The LOD for the analytes varied between 0.4 and 1.5 m g/L and the recoveries were yielded between 64 and 94%. Relative standard deviation of the repeatability of the method is less than 15%. Amitraz was not present in amount above 10 m g/L and one for coumaphos and cymiazole and two for bromopropylate, and three for 2,4-dimethylanilne were detected in amount above 10 m g/L. Levels of the acaricide residues found were less than 50 m g/L.