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Cao, Shiyu,Song, Shangbin,Xiang, Xing,Hu, Qing,Zhang, Chi,Xia, Ziwen,Xu, Yinghui,Zha, Wenping,Li, Junyang,Gonzale, Paulina Mercedes,Han, Young-Hwan,Chen, Fei The Korean Ceramic Society 2019 한국세라믹학회지 Vol.56 No.2
Recently, all-solid-state batteries (ASSBs) have attracted increasing interest owing to their higher energy density and safety. As the core material of ASSBs, the characteristics of the solid electrolyte largely determine the performance of the battery. Thus far, a variety of inorganic solid electrolytes have been studied, including the NASICON-type, LISICON-type, perovskite-type, garnet-type, glassy solid electrolyte, and so on. The garnet Li<sub>7</sub>La<sub>3</sub>Zr<sub>2</sub>O<sub>12</sub> (LLZO) solid electrolyte is one of the most promising candidates because of its excellent comprehensively electrochemical performance. Both, experiments and theoretical calculations, show that cubic LLZO has high room-temperature ionic conductivity and good chemical stability while contacting with the lithium anode and most of the cathode materials. In this paper, the crystal structure, Li-ion transport mechanism, preparation method, and element doping of LLZO are introduced in detail based on the research progress in recent years. Then, the development prospects and challenges of LLZO as applied to ASSBs are discussed.
( Xiang Xu Li ),( Sang Bong Lee ),( Ur Ryong Cho ) 한국고무학회 2019 엘라스토머 및 콤포지트 Vol.54 No.2
Four different polymer compounds were manufactured to make cable sheaths for the shipping industry. Two kinds of ethylene vinyl acetate (EVA) as the main matrix polymers and EVA-grafted maleic anhydride (EVA-g-MAH) as the coupling agent were selected for compounding with fire retardant, crosslinking agent, filler, plasticizer, and other additives. The properties of the four compounded materials were investigated with different contents of the fire retardant, silanecoated magnesium dihydroxide (S-MDH). In the rheology evaluation, the t90 and ΔT values increased with increasing SMDH contents. On the other hand, the tensile strength decreased with increasing S-MDH content due to a relative decrease in binder polymers. With increasing S-MDH content, fire resistance increased, but cold resistance showed no obvious enhancement due to the polar effect of vinyl acetate in EVA.
A Study on Property Change with Mixing Ratio in NBR/PVC Composites
( Xiang Xu Li ),( Hyung Seok Jeong ),( Ur Ryong Cho ) 한국고무학회 2018 엘라스토머 및 콤포지트 Vol.53 No.2
10, 20, 30, and 40% of polyvinyl chloride (PVC) were added to nitrile butadiene rubber (NBR) to modify the latter. The NBR/PVC composites containing pure NBR were synthesized to investigate properties, such as crosslinking density, hardness, tensile strength, abrasion resistance, heat resistance, solvent resistance, and filler dispersion. The experimental result revealed a decrease in crosslinking density and heat resistance with increase in the PVC content. In contrast, addition of PVC to NBR resulted in enhancement of hardness, tensile strength, solvent resistance, and filler dispersion.
( Xiang Xu Li ),( Sang Bong Lee ),( Ur Ryong Cho ) 한국고무학회 2019 엘라스토머 및 콤포지트 Vol.54 No.3
Herein, three polymer compounds were manufactured using three polymer combination methods, ethylene-vinyl acetate/ethylene-propylene-diene-copolymer (EPDM), ethylene-vinyl acetate (EVA)/polyethylene-A (PE-A; density: 0.870), and ethylene-vinyl acetate (EVA)/polyethylene-B (PE-B; density: 0.885), for making cable sheath for use in the shipping industry. In this study, EVA, EPDM, PE-A, and PE-B were used as matrix polymers, and EVA-grafted maleic anhydride was used as a coupling agent for compounding with various compounds such as a fire retardant, cross-linking agent, filler, and other additives, besides the plasticizer. ΔT, Mooney viscosity, and tensile strength increased in order of EPDM < PEA < PE-B, the probable reason is due to the different crosslinking effect. The three compounds showed similar results for fire resistance and aging resistance after compounding process, but they showed excellent cold resistance owing to the non-polarity of the polymers and sufficient plasticizer content.
Xu, Li Xiang,Sohn, Mi Hyun,Kim, Yu Soo,Jeong, Ye Rin,Cho, Ur Ryong The Korean Society Of SemiconductorDisplay Technol 2019 반도체디스플레이기술학회지 Vol.18 No.3
Styrene-butadiene rubber (SBR) composites, incorporated with graphene, molybdenum disulfide and their hybrid in different filling ratio, were fabricated by a two roll-mill. The dispersion states of all the samples' matrix were employed by carbon black dispersion tester. The curing properties of the pre-vulcanized rubber composites were investigated, after molding by heating press machine, the tensile strength, storage modulus, friction coefficient, the swelling property had also been tested according to ASTM. The composite G1M10 (filling with 1 phr graphene and 10 phr molybdenum) showed the best mechanical properties and viscoelastic properties in this research with a better filler dispersion state and more compact matrix structure.
( Xiang Xu Li ),( Ur Ryong Cho ) 한국고무학회 2018 엘라스토머 및 콤포지트 Vol.53 No.1
Styrene-butadiene Rubber (SBR) Latex composites, incorporated with cellulose/starch-silica hybrids synthesized by gel-adsorption method, were filled into rubber by the latex compounding method. The structure morphology, mechanical properties, and thermodynamic properties of gel-silica hybrids were characterized. The states of hybrids which used as fillers were also characterized by SEM. As the fillers ratio increased, the difference for storage modulus of samples had been morphology by rubber process analyzer (RPA). Then, as more fillers ratio was filled into the matrix, the best tensile strength result, and the largest modulus value were also proved by UTM and RPA. As for thermal stability, increase in the ratio of fillers led to higher initial decomposition temperature, which was also proved by TGA. The swelling ratio of samples has also been characterized. From the results of all the tests, cellulose-silica hybrid showed the best results as a filler, and the best filling ratio of this hybrid is about 10 phr, which has the best storage modulus and great tensile strength.
A Study on Surface Treatment for Rubber Materials with Low Friction Factor
( Xiang Xu Li ),( Ur Ryong Cho ) 한국고무학회 2016 엘라스토머 및 콤포지트 Vol.51 No.1
Multi-Surface (MS) treatment is a new technique of surface treatment to reduce the static friction factor on the surface of rubber. MS treatments include 4 methods which names are MS-V (UV-irradiation on the rubber surface), MSM (doing the chemical reaction with double bond of rubber), MS-Q (dilution of rubber surface by silicone surfactant), and MS-P (coating and heating of rubber surface). The experiment and test of every MS-treatment had been carried out using acrylonitrile-butadiene rubber (NBR), ethylene-propylene-diene rubber (EPDM), and chlorosulphonated rubber (CSM) as rubber materials. It had introduced the steps of every MS-treatment process and the result of the properties test. From the research, it was found that the best method was MS-V treatment because it suited all the samples and the effect was obviously.
Xu, Xiang,Li, Lv-mu,Li, Bin,Guo, Wen-jie,Ding, Xiao-ling,Xu, Fa-zhi Asian Australasian Association of Animal Productio 2017 Animal Bioscience Vol.30 No.10
Objective: This study investigated the effect of fermented biogas residue (FBR) of wheat on the performance, serum biochemical parameters, and meat quality in pigs. Methods: We selected 128 pigs (the mean initial body weight was $40.24{\pm}3.08kg$) and randomly allocated them to 4 groups (1 control group and 3 treatment groups) with 4 replicates per group and 8 pigs per pen in a randomized complete block design based on initial body weight and sex. The control group received a corn-soybean meal-based diet, the treatment group fed diets containing 5%, 10%, and 15% FBR, respectively (abbreviated as FBR5, FBR10, and FBR15, respectively). Every group received equivalent-energy and nitrogen diets. The test lasted 60 days and was divided into early and late stages. Blood and carcass samples were obtained on 60 d. Meat quality was collected from two pigs per pen. Results: During the late stage, the average daily feed intake and average daily gain of the treatment groups was greater than that of the control group (p<0.05). During the entire experiment, the average daily gain of the treatment groups was higher than that of the control group (p<0.05). Fermented biomass residue did not significantly affect serum biochemical parameters or meat quality, but did affect amino acid profiles in pork. The contents of Asp, Arg, Tyr, Phe, Leu, Thr, Ser, Lys, Pro, Ala, essential amino acids, non-essential amino acids, and total amino acids in pork of FBR5 and FBR10 were greater than those of the control group (p<0.05). Conclusion: These combined results suggest that feeding FBR could increase the average daily gain and average daily feed intake in pigs and the content of several flavor-promoting amino acids.
Xiang Xu Li(리시앙수),Ji Hwan Oh(오지환),Shin Hye Kang(강신혜),Sun Ho Jang(장선호),Dam Hee Lee(이담희),Ur Ryong Cho(조을룡) 한국고분자학회 2017 폴리머 Vol.41 No.5
스티렌-부타디엔 고무에 4가지 충전제(키토산, 뱀부차콜 분말, 술폰화된 뱀부차콜, 술폰화된 뱀부차콜-키토산 혼성체)를 사용하여 라텍스 컴파운드법으로 고무복합체를 제조하였다. 주사전자현미경과 카본블랙 분산 테스트를 통해서 균일하게 충전제가 고무 매트릭스 내에 분산되었음을 확인하였으며, 가황된 고무복합체의 인장강도, 저장 탄성률, 내마모성, 마찰 계수, 팽윤 특성, 산소 투과도를 조사하였다. 술폰화된 뱀부차콜-키토산 혼성체가 다른 충전제보다 고무 매트릭스에 분산된 입자가 더 작고 잘 분산된 상태를 보였다. 또한 좋은 소수성 성질과 균일한 분산도로 충전제 중 가장 우수한 보강 성능을 보였다. Styrene-butadiene rubber (SBR) composites, incorporated with four kinds of fillers (chitosan, bamboo charcoal powder, sulfonated bamboo charcoal and sulfonated bamboo charcoal-chitosan hybrid) with similar filling ratio, were fabricated by a latex compounding method. Field emission scanning electron microscopy and carbon black dispersion tests were employed to confirm the uniform dispersion of filler in the matrix. The tensile strength, storage modulus, abrasion resistance, friction coefficient, swelling property, and oxygen transmission rates of the vulcanized rubber composites were investigated. The sulfonated bamboo charcoal-chitosan hybrid (sBC-CS) showed a smaller particle size and a better dispersion state compared with those of other fillers. In addition, this compound exhibited the best mechanical reinforcing performance among the four fillers with its great hydrophobic property and good dispersion rate.