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배상은,조수길,이운식 한국산업융합학회 2019 한국산업융합학회 논문집 Vol.22 No.3
The walk-way means a passage installed on the deck of a ship so that a person can safely move under any circumstances. So, the walk-way has to maintain a temperature of 5°C or more for anti/de-icing even at an ambient temperature of -62°C, a temperature in polar region. At present, the walk-way with heating cable is used, but the anti/de-icing effect is insufficient due to low heat transfer efficiency. Also, it has a construction problem due to heavy weight. In this study, an walk-way with a CNT surface heating element is proposed for the high anti/de-icing effect and the heating value per unit volume. The international standard survey, conceptual design, and simulation for the structural safety and the heat transfer are performed for the development of the proposed walk-way. To enhance the performance, the case studies based on the simulation analysis are conducted. Finally, the final prototype, applying the optimum material and thickness (3.2t of SS400) based on the case study results, is fabricated and experimented
Si(111)-H 표면의 전기화학적 제조에 관한 전기화학적 주사터널링현미경법 연구
배상은,이치우,Bae, Sang-Eun,Lee, Chi-Woo 한국전기화학회 2002 한국전기화학회지 Vol.5 No.3
Electrochemical scanning tunneling microscopy was employed to study the evolution of surface morphology during electrochemical preparation of Si(111)-H from Si(111) oxide. Anodic dark current of cyclic voltammogram in 0.2M $NH_4F$ solution (pH 4.7) decreased as the number of cycles increased and remained nearly constant after the second cycle. Then, the Si(111) oxide was entirely stripped, which was followed by H termination on the Si(111) surface. Hydrides at kink and step sites were etched more rapidly than on the terrace, which remained triangle pits with [112] oriented steps where existed stable monohydride. Then, triangle pits deepened. During chronomamperometry at 0.4V anodic dark current shoulder appeared and decreased slowly, indicated the stripping of Si(111) oxide and the formation of stable (112) oriented steps with monohydride. Additionally, the etching mechanism of Si(111)-H in 0.2M $NH_4F(pH 4.7)$ solution at +0.4V was discussed. 묽은 불산용액에서 Si(111) 산화막 (SiOx) 표면을 전기화학적으로 에칭할 때 생성되는 Si(111)-H 표면변화를 전기화학적 주사터널링현미경을 사용하여 조사하였다. pH가 4.7인 0.2M $NH_4F$ 용액에서 순환전압전류곡선은 순환 횟수가 증가할수록 양극 암전류가 감소하였고 두 번 이상 순환한 시료의 암전류는 일정한 형태의 전압전류곡선을 나타냈다. 이때 표면은 모든 SiOx층이 벗겨져 수소말단화된 구조를 가졌으며, 그 이후 순환에서는 생성된 Si(111)-H 표면의 이중 수소결합이 없어지는 step-flow반응이 일어나, 표면이 단일수소결합을 가지는 [112]모서리의 안정한 삼각형 모양을 나타냈으며 또한 생성된 삼각형 흠의 깊이가 점차 깊어졌다. 일정전압법에서는 초기에 큰 양극 암전류 최고 값을 나타낸 후, 시간에 따라 양극 암전류가 감소하였다. 양극 암전류 최고 값 후. 표면의 모든 SiOx가 벗겨졌으며 이후 양극 암전류는 작은 값을 띠면 조금씩 더 낮아졌다. 이 낮아지는 양극 암전류 역시 이중수소 결합의 step-How반응에 안정한 단일수소결합의 [112]모서리 생성에 의해 나타난다. pH 4.7인 0.2M $NH_4F$용액중의 Si(111)-H표면에 +0.4V를 가할 때 진행되는 에칭반응의 메커니즘에 관해서 논하였다.
배상은,Mi-Kyung Oh,민남기,백세환,홍석인,이치우 대한화학회 2004 Bulletin of the Korean Chemical Society Vol.25 No.12
Electrochemical, in situ electrochemical scanning tunneling microscope (EC-STM), and attenuated total reflectance-FTIR (ATR-FTIR) spectroscopic methods were employed to investigate the preparation of atomically flat Si(111)-H surface in ammonium fluoride solutions. Electrochemical properties of atomically flat Si(111)-H surface were characterized by anodic oxidation and cathodic hydrogen evolution with the open circuit potential (OCP) of ca. −0.4 V in concentrated ammonium fluoride solutions. As soon as the natural oxide-covered Si(111) electrode was immersed in fluoride solutions, OCP quickly shifted to near −1 V, which was more negative than the flat band potential of silicon surface, indicating that the surface silicon oxide had to be dissolved into the solution. OCP changed to become less negative as the oxide layer was being removed from the silicon surface. In situ EC-STM data showed that the surface was changed from the initial oxidecovered silicon to atomically rough hydrogen-terminated surface and then to atomically flat hydrogenterminated surface as the OCP moved toward less negative potentials. The atomically flat Si(111)-H structure was confirmed by in situ EC-STM and ATR-FTIR data. The dependence of atomically flat Si(111)-H terrace on mis-cut angle was investigated by STM, and the results agreed with those anticipated by calculation. Further, the stability of Si(111)-H was checked by STM in ambient laboratory conditions.
배상은,이운식 한국산업융합학회 2019 한국산업융합학회 논문집 Vol.22 No.6
This study investigates the validity of applying new carbon nanotube (CNT, Carbon Nano Tube) surface heaters, which are applied in combination with various products, to the vessel’s materials, and proposes the commercializable products accordingly. In order to actually apply a CNT surface heating system technology to the ship’s equipment for the first time in Korea, we carried out the interview of experts in the technology field and the due diligence of the shipyard, and presented the technology road map for the selected three items. Finally, for “Heating System of Ship Fuel Tank” with the highest commercialization potential, we proposed a conceptual diagram to enable the final development of the product through the product analysis.