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- 저자 : ndola, R. B. (검색결과 2 건)
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Rodrí,guez-Gonzá,lez, V.,Domí,nguez-Espí,ndola, R. B.,Casas-Flores, S.,Patró,n-Soberano, O. A.,Camposeco-Solis, R.,Lee, S.-W. American Chemical Society 2016 ACS APPLIED MATERIALS & INTERFACES Vol.8 No.46
<P>Antifungal silver nanocomposites inspired by titanate nanotubes (AgTNTs) were successfully evaluated for the effective inactivation of the phytopathogenic fungus Botrytis cinerea within 20 min. One-dimensional H2Ti3O7 nanotubes functionalized with silver nanoparticles (AgNPs) exhibit unique surface and antifungal properties for the photoinactivation of B. cinerea. Nanostructured titanates were synthesized by the eco-friendly, practical, microwave-induced, hydrothermal method followed by a highly monodispersive AgNP UV-photo deposition. Protonated nanotubes of similar to 11 nm in diameter and four-layers displayed high surface areas, 300 m(2)/g, with a size functionalization of 5 nm for the AgNPs. UV-vis DRS and XPS allowed the characterization and/or quantification of surface reactive species and cytotoxic silver species such as Ag degrees, Ag+. The effective biocidal properties of the nanocomposites were confirmed by using the well-known Gram-negative bacteria Escherichia coli, and then proceeding to the effective inactivation of the phytopathogenic fungus under visible light. The photo assisted inactivation mechanism was examined by HAADF-STEM, HRTEM, and FESEM electronic microscopies. A plasmalemma invagination due to oxidative stress caused by reactive oxygen, silver cytotoxicity species, and AgTNT sharp morphology damage expands the conidia to induce the cell death. The impact of the eco-friendly inactivation is significant because of the ease with which it is carried out and the possibility of being performed in situ with plants like tomato and grapes, which are ranked among the most valuable agricultural products worldwide.</P>
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Structural and optical characterization of wurtzite type ZnS
J. Díaz-Reyes,R.S. Castillo-Ojeda,R. Sánchez-Espíndola,M. Galván-Arellano,O. Zaca-Morán 한국물리학회 2015 Current Applied Physics Vol.15 No.2
ZnS films were grown on (001) GaAs substrates at different temperatures by RF magnetron sputtering. The ZnS chemical stoichiometry was determined by Energy-dispersive X-ray spectroscopy (EDS), besides it allowed to find the residual impurities, mainly oxygen. The X-ray diffraction (XRD) analysis and Raman scattering reveal that ZnS deposited thin films showed hexagonal wurtzite crystalline phase. The films average crystallite size range was from 8.15 to 31.95 nm, which was determined using the Debye eScherrer equation for the peak W(101). Besides an experimental study of first- and second-order Raman scattering of ZnS films is made. An energy level diagram involving oxygen traps and interstitial sulphur ions is used to explain the origin of the radiative transitions observed in the room temperature photoluminescence (PL) spectra.
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