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      • KCI등재

        Preparation of Durable Antibacterial Cellulose with AgCl Nanoparticles

        Zhipeng Ma,Maoli Yin,Zhenming Qi,Xuehong Ren 한국섬유공학회 2018 Fibers and polymers Vol.19 No.10

        In this study, a facile method was developed to coat AgCl nanoparticles (NPs) onto knitted cotton fabrics. The AgCl NPs were characterized by ultraviolet absorption spectrum, X-ray diffraction (XRD) and dynamic laser light scattering (DLS). The AgCl NPs were coated onto cotton fabrics through a pad-dry-cure process with the assistance of 1,2,3,4- butanetetracarboxylic acid (BTCA). Fourier transform infrared spectroscopy (FTIR), scanning electron microscopy (SEM), ICP-OES analysis and energy-dispersive X-ray spectroscopy (EDX) confirmed that AgCl NPs were successfully coated onto cotton fabrics. The prepared cotton samples exhibited excellent antimicrobial activity against both Gram-positive S. aureus and Gram-negative K. pneumonia bacteria. Rat skin fibroblast cytotoxicity testing demonstrated the treated cotton fabrics to be non-toxic. The washing durability evaluation showed that the antimicrobial function of cotton fabrics was durable to washing. In addition, the wrinkle resistance of the coated cotton fabrics was improved and there was no obvious change in whiteness.

      • KCI등재

        Durable N-halamine Antibacterial Cellulose Based on Thiol-ene Click Chemistry

        Zhipeng Ma,Maoli Yin,Mengshuang Zhang,Zhenming Qi,Xuehong Ren,Tung-Shi Huang 한국섬유공학회 2019 Fibers and polymers Vol.20 No.2

        Antibacterial cotton fabrics were prepared with 3-allyl-5,5-dimethylhydantoin (ADMH) by UV photoinitiated thiol-ene click chemistry after 3-mercaptopropyltriethoxysilane (MPTES) was introduced on the surface of cotton fabrics. The treated cotton fabrics were characterized by SEM, FT-IR and EDS. After chlorination with diluted sodium hypochlorite, the treated samples showed good antibacterial efficacy against S. aureus and E. coli O157:H7. About 106 of S. aureus and E. coli O157:H7 could be completely inactivated within 1 min and 5 min of contact, respectively. Compared to the control samples, the antibacterial treatment method used in this study only had a minor effect on the tensile strength of cotton fabrics. Besides, the treated cotton fabrics showed good storage stability and 77 % of the active chlorine remained after 30 days. After exposure to bleach solution, almost all of the active chlorine was restored. The prepared antimicrobial cotton fabrics showed good washing and UV light stability.

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