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        Effect of moisture content on dense-phase conveying of pulverized coal at high pressure

        Xu Pan,Chen Xiaoping,Liang Cai,Xu Guiling,Liu Daoyin,Zhao Changsui 한국화학공학회 2011 Korean Journal of Chemical Engineering Vol.28 No.10

        In dense-phase pneumatic conveying, the solid moisture content can significantly influence the conveying process, but there are very few studies in the open literature. In this study, the conveying experiments of two pulverized coals with various moisture contents were carried out at a 4MPa high pressure and dense-phase pneumatic conveying facility. Results show that the whole conveying system can be stably and controllably operated under the condition that moisture content below ~8%. With the increase of moisture content up to ~8%, the mass flow rate of 280 μm pulverized coal increases at first and then decreases, while that of 55 μm pulverized coal decreases continuously. The method of solid friction factor correlation is used to investigate pressure drop of the horizontal pipe, and non-dimensional parameters--Fr number, moisture content M and solid loading ratio μ--are investigated. The pressure drop predictions by this correlation are in good agreement with the experimental data. The solid friction factor correlations indicate that the fine coal is more sensitive to M, and μ plays a more important role for the coarse coal.

      • KCI등재

        Experimental investigation and stability analysis on dense-phase pneumatic conveying of coal and biomass at high pressure

        Liang Cai,Cai Jiaying,Xu Guiling,Xu Pan,Chen Xiaoping,Zhao Changsui 한국화학공학회 2013 Korean Journal of Chemical Engineering Vol.30 No.2

        Conveying characteristics and flow stability are very important for design and control of a conveying system at high pressure. The influences of operating parameters and material properties on conveying characteristics were investigated in an experimental test facility with a conveying pressure up to 4MPa. Wavelet transform and Shannon entropy analysis were applied to analyzing pressure drops through horizontal pipe in order to obtain the stability criterion. Results indicated that the mass flow rate of biomass decreased, while the mass flow rate of pulverized coal increased at first and then decreased with the increase in fluidization velocity. Solid loading ratios for four kinds of powders decreased with the increase in fluidization velocity. Conveying phase diagrams and pressure drops through different test sections of pulverized coal and biomass at high pressure were obtained and analyzed. The influences of coal category,fracture characteristics and particle size on conveying characteristics were determined.

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        Preparation of N-Doped Graphene by Hydrothermal Method and Interpretation of N-Doped Mechanism

        Yan Shang,Huizhu Xu,Mingyue Li,Guiling Zhang 성균관대학교(자연과학캠퍼스) 성균나노과학기술원 2017 NANO Vol.12 No.2

        Nitrogen-doped graphene (NG) was generated by hydrothermal method, using GO as the raw material and formamide as the reducing-doping source. The composite material was characterized by Fourier transform infrared (FTIR) spectrum, X-ray diffraction (XRD) spectrum, X-ray photoelectron spectroscopy (XPS). The results showed that Nitrogen was successfully doped in the graphene. Through regulating the reaction temperature, time and the ratio of graphite oxide and formamide, the different nitrogen contents were obtained, the highest nitrogen content was 5.67%. NG was also synthesized by urea or ammonia, characterizing by XPS. The characterization results showed that for taking urea and ammonia as nitrogen source, pyrrolic-N was the main form of nitrogen existing, taking formamide as a nitrogen, pyridinic-N was the main form of nitrogen existing. Based on these experimental results by different nitrogen source, the N-doped graphene mechanism was interpreted.

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        Experimental and Modeling Analysis of Hydrogen Motion Behavior in Welding Zone of 2.25Cr–1Mo–0.25 V Steel Welded Joint with Hydrogen Corrosion

        Changdong Yin,Dongdong Ye,Zhou Xu,Jianjun Chen,Yiwen Wu,Houli Liu,Xin Ge,Qiang Liu,Guiling Zeng 대한금속·재료학회 2023 METALS AND MATERIALS International Vol.29 No.8

        Understanding and solving the problem of hydrogen damage due to the degradation of service performance of high-strengthsteel caused by hydrogen penetration is a milestone for the reliability improvement of high-end hydrogen energy equipment. From the perspective of microscopic hydrogen movement behavior, this study investigated the permeability of hydrogenin base metal (BM) and welded metal (WM) of 2.25Cr–1Mo–0.25 V steel welded joint through electrochemical hydrogenpermeation test, and the analytical models of hydrogen penetration and hydrogen diffusion in the welding zone were established,and the effect of adding hydrogen-resistant coatings (HRCs) on hydrogen movement behavior in steel substrate wasstudied. The results showed that the diffusivity of hydrogen in WM of the welded joint was significantly lower than thatin BM, and the hydrogen concentration in BM was higher than that in WM at the beginning of hydrogenation without theaddition of HRCs protection, while it tended to be consistent at the later stage. However, the hydrogen concentration in WMwas lower than that in BM after adding HRCs and would be always higher than that in BM after a certain period of time,and the difference was directly related to the hydrogen resistance of the coatings. Additionally, the difference between theintermediate and outer layers for the welding zone steel substrate with and without HRCs presented a trend of rapid increasefollowed by a slow decrease. These findings could provide an important reference value for hydrogen damage protectionmeasures and related researches on HRCs.

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