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Note on the beginnings of sinusoidal testing methods
Tanner, R.I. The Korean Society of Rheology 2002 Korea-Australia rheology journal Vol.14 No.2
The measurement of the storage and loss moduli (G' and G" respectively) of materials as functions of frequency is now commonplace and is of wide utility. Yet il is not easy to trace the history of such measurements. and so this article discusses the genesis of this important experimental technique. We find that the technique grew out of a parallel technique for dielectric measurements (ca. 1900) and was developed in the mid-1930s by Philippoff and others. Important breakthroughs due to digital circuitry have occurred only in the last 20 years or so.r so.
Study of shear and elongational flow of solidifying polypropylene melt for low deformation rates
Tanner, R.I.,Kitoko, V.,Keentok, M. The Korean Society of Rheology 2003 Korea-Australia rheology journal Vol.15 No.2
An experimental technique was developed to determine the strain-rate in a tensile specimen. Then one can calculate the transient isothermal elongational viscosity. Both shear and elongational viscosities were measured to study the effect of shear and elongational fields on the flow properties. The comparison between these viscosities shows that the onset of rapid viscosity growth as crystallization solidification proceeds occurs at about the same value of time at very small deformation rates (0.0028 and 0.0047 $s^{-1}$). The comparison of these measured viscosities as functions of shear and elongational Hencky strains also reveals that the onset of rapid viscosity growths starts at critical Hencky strain values. The behaviour of steady shear viscosity as function of temperature sweep was also explored at three different low shear rates. Finally, the influence of changing oscillatory frequencies and strain rates was also investigated.
Modeling of flow-induced crystallization of colored polypropylene in injection molding
Rong Zheng,R. I. Tanner,D. Lee Wo,Xi-jun Fan,C. Hadinata,F.S. Costa,P.K. Kennedy,P. Zhu,G. Edward 한국유변학회 2010 Korea-Australia rheology journal Vol.22 No.3
We present a study on flow-induced crystallization of an injection-molded isotactic polypropylene (iPP) mixed with colorant additives. Two types of blue colorants were used in the study: one is the ultramarine Blue composed of Sodium Alumino Sulpho Silicate (UB) and the other is the PV Fast Blue composed of Cu-Phthalocyanine (CuPc). The CuPc colorant exhibits increased nucleation of both quiescent and flow-induced crystallization, and results in more oriented microstructures, causing a high degree of anisotropy in material properties and shrinkage of the injection molded parts. In contrast, the nucleating effect of the UB colorant is negligible under the quiescent condition, but becomes notable in the case of short-term shear treatment at high shear rates. The UB colorant does not significantly increase the degree of anisotropy as compared with the virgin iPP. A flow-induced crystallization kinetic model is used in the numerical simulation for the injection molding process, and predicted the colorant effects as observed in experiments.