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RISS 인기검색어
- 검색키워드
- 저자 : GAORONG HAN (검색결과 4 건)
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Controlled synthesis and characterization of BiVO4 dendrites via a hydrothermal method
Yonggang Wang,Linlin Yang,Xiaofeng Wang,Yujiang Wang,GAORONG HAN 한양대학교 세라믹연구소 2016 Journal of Ceramic Processing Research Vol.17 No.7
BiVO4 dendrites have been controllably synthesized by a hydrothermal method without any surfactants or templates. Thestructure and morphology of the obtained BiVO4 dendrites were characterized by X-ray powder diffraction, scanning electronmicroscope, transmission electron microscopy, and high-resolution transmission electron microscopy. The effect of the pHvalues, precursors, solution concentrations, reaction temperature, and reaction time on the morphology and structure of theBiVO4 dendrites was systematically studied for the first time. It is found that the morphologies of the obtained BiVO4crystallites can vary from cubic-like to dendritic shape. The BiVO4 dendrites can be successfully fabricated by thehydrothermal method at 150 oC and pH 7 when Bi2(CO3)3 and NH4VO3 were used as precursors The resultant dendriticstructure has four trunks which have ordered branches on the opposite sides of the trunks. A rational mechanism for theoriental growth of the BiVO4 dendrites is discussed. The preparation of BiVO4 dendrites with well-dened shapes may open newopportunities for wide applications of future nanodevices.
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JING ZHOU,GAOLING ZHAO,BIN SONG,WEIXIA DONG,JINJIAN YANG,GAORONG HAN 성균관대학교(자연과학캠퍼스) 성균나노과학기술원 2012 NANO Vol.7 No.2
One-dimensional (1D) single crystalline CdS nanostructures have been successfully synthesized via a diphenylthiocarbazone-assisted solvothermal route. The results revealed that the microstructure and optical absorption properties of 1D CdS nanostructures were temperature and time dependent owing to thermodynamically and kinetically controlled growth. Single crystalline CdS nanowires with a diameter of 80 nm and length of 20 μm were synthesized at 180°C for 96 h. At moderate temperature (180°C), the morphology of the products transformed from irregular short rods to uniform long rods as the reaction time prolonging in a kinetically controlled growth regime. Only nanorods were obtained at a temperature as low as 120°C even extending reaction time to 260 h due to thermodynamic limited growth. At high temperature (250°C in this system), the products were nanowires with larger diameter but lower aspect ratio since the growth rates on both lateral and axial directions were accelerated. Moreover, the optical absorption spectra revealed that the CdS nanowires showed a blue shift compared with bulk CdS. Two optical absorption peaks appeared due to the nanometer effect in the radial and lengthwise directions of CdS nanowires. The growth mechanism of 1D CdS nanostructures was discussed.
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Controlled synthesis of SrCO3 dendrites by a simple hydrothermal method
Yonggang Wang,Linlin Yang,Xiaofeng Wang,Yujiang Wang,GAORONG HAN 한양대학교 세라믹연구소 2015 Journal of Ceramic Processing Research Vol.16 No.2
In this paper, we report the controlled synthesis of SrCO3 crystals by a simple hydrothermal method without any surfactants and templates. The as-prepared samples were characterized by X-ray powder diffraction (XRD) and transmission electron microscopy (TEM). The effect of pH value, temperature, and reaction time on the formation of SrCO3 crystals was investigated. This novel route is proved to be simple and environment-friendly, which can be extended to the shape-controlled synthesis of other metal oxide nanocrystals.
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Jing Zhou,GAOLING ZHAO,Wangwei Lu,Lingtong Zhan,GAORONG HAN 성균관대학교(자연과학캠퍼스) 성균나노과학기술원 2019 NANO Vol.14 No.2
Nanocarrier-based biological fluorescent probes for ketamine and amphetamine have been prepared by conjugating red and green fluorescent nanoparticles (150-nm-sized) with anti-ketamine and anti-amphetamine antibodies, respectively, with the assistance of carbodiimide/N-hydroxysuccinimide. Biological fluorescent probes for ketamine and amphetamine could simultaneously detect these two drugs within a single fingermark by one-step test. Nanoparticles as carrier played dual-functional roles for not only fingermark visualization but also drug recognition. Latent fingermarks were visualized by the fluorescence signal generated from nanoparticles. The developed fingermarks clearly revealed ridge pattern and sufficient minutiae for individual identification. Ketamine and amphetamine were recognized by simply observing the colors of fluorescent images when the fingermark was checked in red and green channels. Detection limit of ketamine or amphetamine was 50 ng in fingermark. This work therefore provides a novel nanocarrier-based strategy of drug detection as well as personal identification with high selectivity, low background interference and fast testing, which can be further broadened to other drugs and molecules.
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