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강도형 ( Do Hyung Kang ),이재우 ( Jae W. Lee ) 한국화학공학회 2014 Korean Chemical Engineering Research(HWAHAK KONGHA Vol.52 No.6
4성분계 다중반응이 반응증류 탑 내에서 발생할 때 증류거동의 변화를 시각화 방법을 통해 분석하였다. 시각화 방법이란 단순 증류의 물질수지에 각 반응에 의한 벡터를 추가하고 이를 공간상에 표현하는 것으로 각 단에서 혼합물의 조성 변화 및 반응의 진척도를 직관적으로 알 수 있다. 또한 이를 통해 주어진 운전조건에서 필요한 총 단수 및 최적반응 단의 위치를 결정할 수 있다. 본 연구에서는 에틸렌글리콜(Ethylene glycol) 생산공정을 시각화 방법을 통해 분석하였다. 제안된 시각화 방법을 사용하여 복잡한 실험이나 공정모사 없이 4성분계 다중반응증류 공정에 대한 타당성 평가 및 분석이 가능하다. When multiple reactions of quaternary mixtures take place in a reactive distillation column, the behavior of composition trajectory is analyzed by a visual-aided method. By adding additional vectors of multiple reactions and visualizing them in composition space, the composition of each component and extent of each reaction on an arbitrary stage can be easily estimated in terms of the composition trajectory and reaction cascade difference points. Moreover, for a given operating conditions, the number of total stages and position of optimum reaction zone can be determined by the visual-aided method. In this study, ethylene glycol synthesis with a side reaction is taken as an example and analyzed by the proposed graphical method. Through this method, the quaternary reactive distillation with multiple reactions can be analyzed without numerous experiments and simulations.
박재현,신원모,이재우,Park, Jae Hyun,Shin, Won Mo,Lee, Jae W. 한국군사과학기술학회 2016 한국군사과학기술학회지 Vol.19 No.1
Over the decades, TNT has been produced indiscriminately to be utilized in many fields owing to its ability to manipulate the explosion. Yet, the proper technique for disposal of TNT and the waste residues had not been developed so that the large amount of TNT waste was being piled up. Upon the agreement to demilitarization of old weapon, a study on the disposal methods for TNT and the waste treatment have been raised for their dangerous nature. Since then, from burying in landfill to utilizing supercritical fluid-based oxidation, a lot of research is actively ongoing, but little progress has been made in Korea compared to developed countries. This review paper covers all the technologies developed for TNT and its waste disposal including the concept, advantage, and disadvantage of those technologies. Also, suggested here are the future research directions.